PL506B1 - Saponification of casein to obtain a product which bleaches the fabric without the use of soap. - Google Patents
Saponification of casein to obtain a product which bleaches the fabric without the use of soap. Download PDFInfo
- Publication number
- PL506B1 PL506B1 PL506A PL50620A PL506B1 PL 506 B1 PL506 B1 PL 506B1 PL 506 A PL506 A PL 506A PL 50620 A PL50620 A PL 50620A PL 506 B1 PL506 B1 PL 506B1
- Authority
- PL
- Poland
- Prior art keywords
- soap
- product
- casein
- fabrics
- general
- Prior art date
Links
- 239000000344 soap Substances 0.000 title claims description 9
- 239000004744 fabric Substances 0.000 title claims description 6
- 239000005018 casein Substances 0.000 title claims description 4
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 title claims description 4
- 235000021240 caseins Nutrition 0.000 title claims description 4
- 238000007127 saponification reaction Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 4
- 239000011347 resin Substances 0.000 claims description 4
- 229920005989 resin Polymers 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 238000004061 bleaching Methods 0.000 claims 3
- 239000002657 fibrous material Substances 0.000 claims 3
- 239000003513 alkali Substances 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000000047 product Substances 0.000 description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 5
- 239000000126 substance Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 241000246358 Thymus Species 0.000 description 2
- 235000007303 Thymus vulgaris Nutrition 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 239000001585 thymus vulgaris Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241000779819 Syncarpia glomulifera Species 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000010692 aromatic oil Substances 0.000 description 1
- QFKJCKFAYFUXRQ-UHFFFAOYSA-N barium;hydrate Chemical compound O.[Ba] QFKJCKFAYFUXRQ-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 1
- 239000001739 pinus spp. Substances 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 229940036248 turpentine Drugs 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Description
Wynalazek dotyczy produktu, którym mozna bielic tkaniny wszelkiego rodzaju: jedwabne, welniane, bawelniane i inne bez uzycia mydla.Produkt otrzymuje sie z emulsji kaze¬ iny.Wyrób jego wymaga nastepujacego szeregu postepowan: 1. Do naczynia wklada sie 1 kg kazeiny handlowej, w proszku, lub ziarnistej, do której wlewa sie potrochu okolo 1 i pól li¬ tra wody. Podczas wlewania wody ugnia¬ ta sie substancje, poczem zostawia sie ja' na pól godziny, by napeczniala. 2. Rozpuszcza sie az do nasycenia 1 kg. 200 gr weglanu sodu w 800 cm3 wody o temperaturze 60° do 70°C, nastepnie sie o- studza. Zamiast weglanu sodu mozna u- zyc weglanu potasu; mozna równiez wziasc amonjak, wodzian baru, lub inna zasade. 3. Substancje 1 i 2 miesza sie i ugniata tak dlugo, az nadmiar wody bedzie mógl byc oddzielony przez dekantowanie (od¬ lanie cieczy z osadu), poczem pozostawia sie je na dwie godziny. Zamiast przez de¬ kantowanie, moze byc woda oddzielona przez cedzenie. 4. W metalowem naczyniu rozpuszcza sie na wolnym ogniu 1 kg 500 g jasnej zy¬ wicy handlowej, która sie zmydla 750 cm3 lugu sodowego o 30° Be. Mydlo zy¬ wiczne moze byc zastapione przez kazde inne mydlo rozpuszczalne. Nastepnie do¬ daje sie plyn 3, ugniatajac ustawicznie, az otrzymamy mase. miekka, zupelnie jedno¬ lita. Nalezy uwazac, by temperatura nie podniosla sie do wrzenia. Otrzymana mase ochladza sie do 50°C.Wtedy dodaje sie substancje odcedzona 3, nie przestajac ugniatac, aby produkt bylzupelnie jednolity. Po ostudzeniu otrzyma sie nowy produkt, który twardniejac, two¬ rzy mase lekko ziarnista. Moze on byc u- zyty w tej formie, lub tez mozna mu na¬ dac forme podobna do mydla. Mozna mu równiez nadac postac zupelnie ziarnista przez dodanie dostatecznej ilosci sody zwyklej. Plastycznosc i plynnosc zaleza od ilosci wody, uzytej przy postepowaniu pierwszem; biorac 1 i pól litra wody (jak bylo wskazane), otrzymuje sie produkt staly; przy uzyciu trzech litrów wody o- trzyma sie mase miekka.Produkt, otrzymany w ten sposób, ma slaby zapach terpentyny. By zapach ten zagluszyc, wystarcza dodac w ostatecznej fazie fabrykacji kilka kropel jakiegokol¬ wiek oleju aromatycznego, jak tymianek, macierzanka, nitrobenzol i t. p. Produkt ten rozpuszcza sie w zimnej wodzie, posia¬ da wlasnosc czyszczenia i wywabiania plam z wszystkich materjalów wlókni¬ stych i tkanin, bez uzycia mydla. PLThe invention relates to a product that can be bleached all kinds of fabrics: silk, wool, cotton and others without the use of soap. The product is obtained from a casein emulsion. The product requires the following series of procedures: 1. 1 kg of commercial casein is put into the dish, a powder or granular powder into which a little about 1 1/2 liters of water is poured. When the water is poured in, the substances are kneaded, and it is then left for half an hour to swell. 2. Dissolve to saturation 1 kg. 200 g of sodium carbonate in 800 cm3 of water at 60 ° to 70 ° C, then cooled. Potassium carbonate may be used in place of sodium carbonate; You can also take ammonia, barium hydrate, or some other principle. 3. Substances 1 and 2 are mixed and kneaded until the excess water can be separated by decanting (draining the liquid from the sediment), then left for two hours. Instead of decanting, the water may be separated by a strainer. 4. 1 kg of 500 g of light commercial resin, which is saponified by 750 cm 3 of sodium liquor at 30 ° Be, is slowly dissolved in a metal vessel. Resin soap may be replaced by any other soluble soap. Then liquid 3 is added, kneading continuously until mass is obtained. soft, completely uniform. Be careful that the temperature does not rise to boiling point. The resulting mass is cooled to 50 ° C. Then the strained substance 3 is added, without ceasing to knead, so that the product is completely uniform. After cooling, a new product will be obtained which hardens to form a slightly grainy mass. It may be used in this form, or it may be given a form similar to soap. It can also be made completely grainy by adding enough regular soda. Plasticity and fluidity depend on the amount of water used in the first procedure; taking 1 1/2 liter of water (as indicated), you get a solid product; with three liters of water it sticks to a soft mass. The product obtained in this way has a slight turpentine smell. In order to suppress this smell, it is enough to add a few drops of any aromatic oil, such as thyme, thyme, nitrobenzol, etc., in the final stage of fabrication. fabrics, without the use of soap. PL
Claims (3)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL506B1 true PL506B1 (en) | 1924-09-30 |
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