PL2146B1 - The method of producing solid solutions of volatile bodies. - Google Patents

The method of producing solid solutions of volatile bodies. Download PDF

Info

Publication number
PL2146B1
PL2146B1 PL2146A PL214621A PL2146B1 PL 2146 B1 PL2146 B1 PL 2146B1 PL 2146 A PL2146 A PL 2146A PL 214621 A PL214621 A PL 214621A PL 2146 B1 PL2146 B1 PL 2146B1
Authority
PL
Poland
Prior art keywords
calcium lactate
solution
bodies
solutions
solid solutions
Prior art date
Application number
PL2146A
Other languages
Polish (pl)
Filing date
Publication date
Application filed filed Critical
Publication of PL2146B1 publication Critical patent/PL2146B1/en

Links

Description

Zrobiono godne uwagi spostrzezenie, ze roztwory mleczanu wapnia nadaja sie wy¬ smienicie do przyjmowania w siebie cial lotnych, jak np. aldehydu mrówkowego, jak równiez i cial pachnacych i aromatycznych, do zatrzymywania ich przy krzepnieciu i do oddawania przy ponownem rozpuszcze¬ niu. W ten sposób otrzymuje sie wiec przy pomocy mleczanu wapnia preparaty stale, w których cialo lotne zwiazane jest z mleczanem wapnia i moze byc latwo po¬ nownie wydzielone na wolnosc. Tego wiec rodzaju preparaty, wzglednie stale roztwo¬ ry, moga byc zastosowane do najrózniej¬ szych celów, zaleznie od rodzaju ciala lot¬ nego.W celu wytworzenia stalego preparatu z mleczanu wapnia i aldehydu mrówkowe¬ go, mozna postepowac, np. w sposób na¬ stepujacy: W 500 gramach roztworu aldehydu mrówkowego o zawartosci okolo 35% wa¬ gowych aldehydu mrówkowego, rozpuszcza sie mniej wiecej 600—700 g sproszkowa¬ nego mleczanu wapnia, przy ogrzewaniu pod chlodnica zwrotna. Temperatura nie powinna przy tern, o ile moznosci, przekra¬ czac 90° C. W ten sposób otrzymuje sie bezbarwny syropowaty plyn, który po wie- logodzinnem staniu w zimnem miejscu za¬ styga na twarda biala mase krystaliczna, która latwo rozpuszcza sie w wodzie, a w wodzie ogrzanej latwo odszczepia aldehyd mrówkowy. Zawartosc aldehydu mrówko-wego w tej masie w stanie swiezym- byla okreslona na okolo 12%.Mozna równiez postepowac w ten spo¬ sób, ze rozpuszcza sie mleczan wapnia w niewielkiej ilosci cieplej wody i nastepnie dodaje roztwór aldehydu mrówkowego.Wytwór ten, przechowywany w zamknie¬ tej butelce, trzyma sie dobrze i daje sie przerabiac w stanie sproszkowanym na najrozmaitsze preparaty, tak, np. w mie¬ szaninie z cukrem mlecznym, maka, wap¬ nem i podobnemi materjalami zapelniaja- cemi na tabletki lub pigulki, kóre moga byc stosowane jako wewnetrzny srodek de^ zynfekcyjny. Równiez dobrze wytwór mozna przerabiac na srodki dezynfekcyj¬ ne do uzycia zewnetrznego.Równiez naturalne i sztuczne ciala pach¬ nace i aromatyczne moga byc w ten spo¬ sób przeprowadzone w postaci stalych roz¬ tworów. Postepuje sie np. w ten sposób, ze rozpuszcza sie mleczan wapnia w gotu¬ jacej wodzie, dodaje sie podczas oziebia¬ nia niewielkie ilosci ciala pachnacego w odpowiednim roztworze (np. rozcienczony roztwór alkoholowy jononu, roztwory olej¬ ków eterycznych i esencji lub podobnych) i daje mieszaninie zakrzepnac. PLThe remarkable observation has been made that solutions of calcium lactate are brilliant for the ingestion of volatile bodies such as formaldehyde, for example, as well as fragrant and aromatic bodies, for retaining them in solidification and for giving them back upon redissolution. Thus, solid preparations are obtained with calcium lactate in which the volatile matter is bound to the calcium lactate and can easily be re-separated into the wild. Such preparations, or constant solutions, can therefore be used for a variety of purposes, depending on the type of volatile matter. In order to prepare a solid preparation from calcium lactate and formaldehyde, it is possible to proceed, for example, by Tapping: In 500 grams of a solution of formaldehyde containing about 35% by weight of formaldehyde, about 600-700 g of powdered calcium lactate are dissolved by heating under reflux. The temperature should not, if possible, exceed 90 ° C. In this way, a colorless syrupy liquid is obtained, which, after standing in a cold place for many hours, condenses to a hard white crystalline mass that easily dissolves in water. and in heated water it easily cleaves formaldehyde. The content of formaldehyde in this mass in the fresh state was determined at about 12%. It is also possible to dissolve calcium lactate in a little warm water and then add a solution of formaldehyde. This product, stored in in a closed bottle, it stays well and can be processed in a powdered state into a wide variety of preparations, for example in a mixture with milk sugar, flour, calcium and similar filling materials into tablets or pills, which can be used as an internal disinfectant. The product can also be processed into disinfectants for external use. Natural and artificial bodies, both fragrant and aromatic, can thus be made in the form of solid solutions. The procedure is, for example, to dissolve calcium lactate in boiling water, add small amounts of fragrant body in a suitable solution during cooling (for example, dilute alcohol ionic solution, solutions of essential oils and essences or the like). and makes the mixture clot. PL

Claims (3)

Zastrzezenia patentowe. 1. Sposób wytwarzania stalych roz¬ tworów cial lotnych, znamienny tern, ze zwiazuje sie te ciala z mleczanem wapnia.Patent claims. 1. A process for the production of volatile solids solutions characterized by the association of the bodies with calcium lactate. 2. Sposób, wykonania postepowania wedlug zastrz. 1, znamienny tern, ze roz¬ puszcza sie mleczan Wapnia w roztworze cial lotnych, celowo na cieplo, i daje roz¬ tworom zakrzepnac.2. The method of carrying out the procedure according to claim A method according to claim 1, characterized in that the calcium lactate is dissolved in a solution of volatile matter, expediently with heat, and the solutions are allowed to clot. 3. Sposób wykonania postepowania wedlug zastrz. 1, znamienny tern, ze wpro¬ wadza sie ciala lotne do roztworu mleczanu wapnia, celowo na cieplo, i daje zastygnac roztworowi. Chemische Fabrik auf Actien (vorm. E, Schering). Zastepca: Cz. Raczynski, rzecznik patentowy. bruk L. Boguslawskiego, Warszdwd. PL3. The method of performing the procedure according to claim A method according to claim 1, characterized in that volatiles are introduced into the calcium lactate solution, expediently under heat, and the solution is allowed to freeze. Chemische Fabrik auf Actien (vorm. E, Schering). Deputy: Vol. Raczynski, patent attorney. pavement of L. Boguslawski, Warszdwd. PL
PL2146A 1921-12-19 The method of producing solid solutions of volatile bodies. PL2146B1 (en)

Publications (1)

Publication Number Publication Date
PL2146B1 true PL2146B1 (en) 1925-06-30

Family

ID=

Similar Documents

Publication Publication Date Title
JPH0198443A (en) Stabilized fat-containing system and method for its manufacture
JPS5765151A (en) Preparation of food like ceram cheese
CN103100090A (en) Hard capsule shell material and production process thereof
Black Experiments upon magnesia alba, quick-lime, and other alcaline substances
CN103100091A (en) Compound seaweed gum and application thereof to capsule preparation
PL2146B1 (en) The method of producing solid solutions of volatile bodies.
CN105662927A (en) Infant camellia oil hip-protecting cream and preparation method thereof
NO148871B (en) PROCEDURE FOR THE MANUFACTURE OF SUGAR-FREE TUBBER GUM
CN106215186B (en) The preparation method of sore mouth virus live-vaccine heat-proof protective agent and its freeze-dried powder and the freeze-dried powder
SU1084006A1 (en) Method of preparing food emulsion
CN103006616A (en) Algal polysaccharide capsules and method for manufacturing same
de Camargo Biology of the spermatozoon of Apis mellifera. I. Influence of diluents and pH
US2194842A (en) Soft lecithin preparation
US1244141A (en) Salt brick and method of making same.
CN103041397A (en) Sodium alga acid capsule and production process thereof
US1513298A (en) Therapeutic product and process of preparing same
JP2022044833A (en) Method for producing granule, and granule
Holmes et al. The relationship between sugar in blood and lactic acid in brain
DE950751C (en) Process for the production of spontaneously and rapidly absorbing tampons from absorbable material
CN104208712B (en) A kind of infectious bursal disease yolk antibody heat-resisting lyophilized protecting agent and preparation method thereof
JPS608775B2 (en) Method for producing pollen extract
CN103932976B (en) A kind of injection-type directional sustained-release Paeonol thermo-sensitive gel and preparation method
CN102308976B (en) Method for extracting cartialgenous and coronet nourishing ingredient and health care food with same
CN103301471B (en) Lyophilized vaccine for porcine rotavirus (PRV)
Britton et al. Further experiments on cortico-adrenal extract: its efficacy by mouth