PE20221570A1 - Metodo para la determinacion de la autenticidad y adulteracion de hidrocarburos de petroleo marcados - Google Patents

Metodo para la determinacion de la autenticidad y adulteracion de hidrocarburos de petroleo marcados

Info

Publication number
PE20221570A1
PE20221570A1 PE2022000995A PE2022000995A PE20221570A1 PE 20221570 A1 PE20221570 A1 PE 20221570A1 PE 2022000995 A PE2022000995 A PE 2022000995A PE 2022000995 A PE2022000995 A PE 2022000995A PE 20221570 A1 PE20221570 A1 PE 20221570A1
Authority
PE
Peru
Prior art keywords
alkyl
sample
petroleum hydrocarbon
authenticity
hydrogen
Prior art date
Application number
PE2022000995A
Other languages
English (en)
Inventor
Martin Zuhlke
Daniel Riebe
Toralf Beitz
Thomas Tiller
Gejo Juan Lopez
Unige Laskay
Original Assignee
Sicpa Holding Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sicpa Holding Sa filed Critical Sicpa Holding Sa
Publication of PE20221570A1 publication Critical patent/PE20221570A1/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/003—Marking, e.g. coloration by addition of pigments
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26—Oils; viscous liquids; paints; inks
    • G01N33/28—Oils, i.e. hydrocarbon liquids
    • G01N33/2835—Oils, i.e. hydrocarbon liquids specific substances contained in the oil or fuel
    • G01N33/2882—Markers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B45/00—Other details
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B57/00—Other carbonising or coking processes; Features of destructive distillation processes in general
    • C10B57/04—Other carbonising or coking processes; Features of destructive distillation processes in general using charges of special composition
    • C10B57/06—Other carbonising or coking processes; Features of destructive distillation processes in general using charges of special composition containing additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M127/00—Lubricating compositions characterised by the additive being a non- macromolecular hydrocarbon
    • C10M127/06—Alkylated aromatic hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M171/00—Lubricating compositions characterised by purely physical criteria, e.g. containing as base-material, thickener or additive, ingredients which are characterised exclusively by their numerically specified physical properties, i.e. containing ingredients which are physically well-defined but for which the chemical nature is either unspecified or only very vaguely indicated
    • C10M171/007—Coloured or dyes-containing lubricant compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/16—Hydrocarbons
    • C10L1/1608—Well defined compounds, e.g. hexane, benzene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/22—Organic compounds containing nitrogen
    • C10L1/222—Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond
    • C10L1/223—Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond having at least one amino group bound to an aromatic carbon atom
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2230/00—Function and purpose of a components of a fuel or the composition as a whole
    • C10L2230/16—Tracers which serve to track or identify the fuel component or fuel composition
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/06—Well-defined aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/04—Ethers; Acetals; Ortho-esters; Ortho-carbonates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
    • C10M2215/068—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings having amino groups bound to polycyclic aromatic ring systems, i.e. systems with three or more condensed rings
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/42—Flashing oils or marking oils

Abstract

La presente invencion proporciona un metodo para la determinacion de la autenticidad de un hidrocarburo de petroleo que comprende supuestamente al menos un marcador quimico especifico, en donde dicho marcador quimico se selecciona de i) un compuesto de formula (I), donde R1 a R12 son H, alquilo C1-C4, entre otros; ii) un compuesto de formula (II) donde Ra-Re, Ra'-Re', Ra''- Re'' y Ra'''-Re''' son hidrogeno o alquilo C1-C4; L es -CR13=CR14-; R13 y R14 son hidrogeno o metilo; R15 a R24 son hidrogeno o alquilo C1-C4; n es un numero entero entre 2 y 6; iii) un compuesto aromatico sustituido mediante uno o mas grupos amino disustituidos por N,N, en donde los sustituyentes de los uno o mas grupos amino disustituidos por N,N se seleccionan de alquilo C1-C6 o los dos sustituyentes de un grupo amino disustituido por N,N tomados en conjunto forman un residuo -(CH2)p-, en donde p es un numero 15 entero entre 2 y 6; y iv) un compuesto aromatico sustituido mediante al menos un grupo seleccionado de alquiloxi C1-C4; en donde dicho metodo comprende las siguientes etapas: a-1) adquirir una muestra del hidrocarburo de petroleo; b-1) vaporizar dicha muestra para proporcionar una muestra gaseosa; c-1) iluminar la muestra gaseosa con una luz laser pulsada de una longitud de onda predeterminada de entre aproximadamente 300 nm y 25 aproximadamente 370 nm, produciendo, de ese modo, iones gaseosos; y d-1) analizar los iones gaseosos obtenidos en la Etapa c-1) mediante espectrometria de movilidad de iones o espectrometria de masas para detectar la presencia o ausencia de dicho al menos un marcador quimico en el hidrocarburo de petroleo y determinar, de ese modo, la autenticidad de 30 dicho hidrocarburo de petroleo.
PE2022000995A 2019-12-03 2020-11-26 Metodo para la determinacion de la autenticidad y adulteracion de hidrocarburos de petroleo marcados PE20221570A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP19213124 2019-12-03
PCT/EP2020/083470 WO2021110525A1 (en) 2019-12-03 2020-11-26 Method for determining authenticity and adulteration of marked petroleum hydrocarbons

Publications (1)

Publication Number Publication Date
PE20221570A1 true PE20221570A1 (es) 2022-10-06

Family

ID=68766586

Family Applications (1)

Application Number Title Priority Date Filing Date
PE2022000995A PE20221570A1 (es) 2019-12-03 2020-11-26 Metodo para la determinacion de la autenticidad y adulteracion de hidrocarburos de petroleo marcados

Country Status (15)

Country Link
US (1) US20230103579A1 (es)
EP (1) EP4069807B1 (es)
AU (1) AU2020397410A1 (es)
BR (1) BR112022010452A2 (es)
CO (1) CO2022008791A2 (es)
CR (1) CR20220246A (es)
DO (1) DOP2022000113A (es)
ES (1) ES2968166T3 (es)
GE (1) GEP20247597B (es)
MA (1) MA57801B1 (es)
PE (1) PE20221570A1 (es)
PL (1) PL4069807T3 (es)
PT (1) PT4069807T (es)
RS (1) RS65023B1 (es)
WO (1) WO2021110525A1 (es)

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JPH1074479A (ja) * 1996-08-30 1998-03-17 Nkk Corp レーザーイオン化質量分析装置及び質量分析方法
DE10120335C2 (de) 2001-04-26 2003-08-07 Bruker Daltonik Gmbh Ionenmobilitätsspektrometer mit nicht-radioaktiver Ionenquelle
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Also Published As

Publication number Publication date
BR112022010452A2 (pt) 2022-09-06
CO2022008791A2 (es) 2022-06-30
MA57801B1 (fr) 2024-01-31
RS65023B1 (sr) 2024-01-31
WO2021110525A1 (en) 2021-06-10
PT4069807T (pt) 2024-01-02
US20230103579A1 (en) 2023-04-06
EP4069807B1 (en) 2023-10-04
DOP2022000113A (es) 2022-09-30
CR20220246A (es) 2022-08-19
AU2020397410A1 (en) 2022-07-14
ES2968166T3 (es) 2024-05-08
PL4069807T3 (pl) 2024-03-18
EP4069807A1 (en) 2022-10-12
GEP20247597B (en) 2024-02-26

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