NZ324190A - Method of labelling containers to facilitate de-labeling includes forming a frangible region on label - Google Patents
Method of labelling containers to facilitate de-labeling includes forming a frangible region on labelInfo
- Publication number
- NZ324190A NZ324190A NZ324190A NZ32419096A NZ324190A NZ 324190 A NZ324190 A NZ 324190A NZ 324190 A NZ324190 A NZ 324190A NZ 32419096 A NZ32419096 A NZ 32419096A NZ 324190 A NZ324190 A NZ 324190A
- Authority
- NZ
- New Zealand
- Prior art keywords
- label
- container
- labeling
- frangible region
- labeled
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C63/00—Lining or sheathing, i.e. applying preformed layers or sheathings of plastics; Apparatus therefor
- B29C63/0004—Component parts, details or accessories; Auxiliary operations
- B29C63/0013—Removing old coatings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/083—Removing scrap from containers, e.g. removing labels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B26—HAND CUTTING TOOLS; CUTTING; SEVERING
- B26F—PERFORATING; PUNCHING; CUTTING-OUT; STAMPING-OUT; SEVERING BY MEANS OTHER THAN CUTTING
- B26F3/00—Severing by means other than cutting; Apparatus therefor
- B26F3/002—Precutting and tensioning or breaking
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C63/00—Lining or sheathing, i.e. applying preformed layers or sheathings of plastics; Apparatus therefor
- B29C63/38—Lining or sheathing, i.e. applying preformed layers or sheathings of plastics; Apparatus therefor by liberation of internal stresses
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65C—LABELLING OR TAGGING MACHINES, APPARATUS, OR PROCESSES
- B65C3/00—Labelling other than flat surfaces
- B65C3/06—Affixing labels to short rigid containers
- B65C3/065—Affixing labels to short rigid containers by placing tubular labels around the container
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65C—LABELLING OR TAGGING MACHINES, APPARATUS, OR PROCESSES
- B65C9/00—Details of labelling machines or apparatus
- B65C9/0015—Preparing the labels or articles, e.g. smoothing, removing air bubbles
Landscapes
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Forests & Forestry (AREA)
- Labeling Devices (AREA)
Description
New Zealand No. 324190 International No. PCT/US96/19268
TO BE ENTERED AFTER ACCEPTANCE AND PUBLICATION
Priority dates: 04.12.1995;
Complete Specification Filed: 02.12.1996
Classification:^) B32B31/00; B32B35/00; B65C9/04; B26F1/24; B26D7/06
Publication date: 26 August 1998
Journal No.: 1431
NEW ZEALAND PATENTS ACT 1953
COMPLETE SPECIFICATION
Title of Invention:
Method of labeling containers to facilitate de-labeling
Name, address and nationality of applicant(s) as in international application form:
B&H MANUFACTURING COMPANY, INC., 3461 Roeding Road, Ceres, California, United States of America
I.
METHOD OF LABELING CONTAINERS TO FACILITATE DE-LABELING
Technical Field
The present invention relates to a method of 5 labeling containers with labels which are prepared to facilitate being stripped from the containers.
Background Art
Containers for products are labeled by various methods. One example of a container produced in high 10 volumes which has constantly been improved in its method of labeling is a soft drink container. These containers were originally formed of glass directly decorated with painting or printing. Soft drink cans were subsequently developed wherein labels were directly printed on the 15 surface of the cans by lithography. Due to environmental and cost considerations, directly decorating con-uainers such as glass bottles and cans has been supplanted by applying pre-printed labels to these containers. These labels can be produced and applied at low 20 cost to containers as part of a container filling line. Originally, these labels consisted of paper and were applied to the containers with glue. The paper labels were subject to degradation from moisture and other environmental factors.
The bottling industry improved paper labels by applying a thin layer of plastic over the paper for protection. Other labels developed include polystyrene foam labels and, more recently, film labels. Selection of labeling materials for various containers is influ-30 enced by factors such as cost, convenience of applicaPrinted from Mimosa 13:12:01
PCT AJS96/I9268
tion and use, and ability to reuse and recycle the containers.
One problem in recycling or reusing containers relates to the de-labeling or the removal of labels. 5 For example, paper labels which are pasted or glued on containers are frequently removed by immersing the labeled container into a washer of hot caustic solution. An example of a machine used to apply caustic solution to a labelled container is disclosed in U.S. Patent No. 10 4,044,783 issued to Babunovic, et al. However, caustic solution baths do not work well with plastic labels because plastic is impervious to moisture. Furthermore, the washer may become subject to label congestion as a large number of containers are fed through the washer in 15 a relatively short time.
Tough, axially oriented film labels are also difficult to remove from containers. If a durable film label is applied to a glass or plastic bottle, it can be difficult to remove the label without harming the 20 surface of the container. In particular, wher. an oriented film is applied to a polyethylene tetraphthal-ate (PET) bottle, the known processes for de-labeling containers can scratch or cut the underlying container. It has been proposed that PET containers could be reused 25 without remelting if they could be de-labeled and adequately sanitized without injury to the bottle.
Known de-labeling methods include mechanical de-labelers wherein fingers are used to scratch and tear the label from the container as it moves down a de-30 labeling line. For instance, U.S. Patent No. 4,122,734 issued to Hurst, discloses a label stripping machine utilizing a razor for cutting off the label from the
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container. Another approach to cutting the label is to use air or water jet knives. As disclosed in U.S. Patent No. 4,717,442 issued to Hopson, air jets are directed between the label and the container in order to 5 rupture the label.
A difficulty with either mechanical stripping fingers, razors, or jet knife de-labelers, is controlling the depth of the cut and the force used to remove the label in order to avoid scratching or cutting the 10 container. If a PET container is scratched or cut, it is unusable ana must be remelted before being recycled. Likewise, if a glass container is cut or scratched in the course of de-labeling, the container can be ruined, requiring it to be remelted and reformed into a new 15 bottle.
A pressure sensitive, price tag is shown in U.S. Patent No. 4,787,158 issued to Vitol. The disclosed label has a score line which is provided for the purpose of spliting the label if a consumer tries to 2 0 remove the price tag.
The prior art has not addressed the need for a bottle labeling method which facilitates automatic de-labeling without harming the containers as proposed by applicant below.
Summary Of The Invention
It is an object of the present invention to provide a method of labeling containers with a label that lends itself to being removed from the containers by automatic de-labeling equipment.
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97/20694
PCI7US96/19268
It is another object of the present invention no provide a method of labeling containers including the step of forming a frangible region on the label which facilitates de-labeling without unduly weakening the durability of the label.
It is yet another object of the present invention to provide a method of labeling containers with a label that is adapted to break in a frangible region causing it to flag thereby facilitating de-labeling.
According to the present invention a method of labeling containers is provided which facilitates automatic de-labeling of the containers after consumer use. The method includes preparing a container for labeling and preparing a label for application to the container. In the process of preparing the label, a frangible, or breakable, region is formed on the label which may, in some applications, extend across the label generally from the top to the bottom of the label. The label is ther. applied to the container. The labeled container may then be distributed to consumers for use. The containers are then collected from the consumers for reuse or recycling. A mechanical force is applied to the labeled container to break the label initially at the frangible region prior to separating the label from the container.
The present invention is applicable to a variety of labeling methods including the method wherein labels are fed from a roll which is cut off into label segments. Roll fed label segments are generally applied to the container by tacking the leading end of the label to the container and then wrapping the label around the
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container. The trailing end of the label is then secured to the container or the leading end of the label. The method is also applicable to labels that are supplied from a pre-cut stack of labels and applied to 5 the container in a similar manner. The method is even applicable to sleeve-applied labels wherein labels are formed into sleeves and then slid over one end of a container. In each method, the label is either perforated or scored prior to application to a container from 10 one edge to the other to form a substantially full height frangible region which permits the label to break from edge to edge. Upon the frangible region breaking, the label flags or extends outward from the container.
The method of the present invention facili-15 tates de-labeling by means of de-labeling machines which include fluid jet knives, mechanical moving fingers or counter-rotating rollers. Regardless of the de-labeling method used, the method of labeling containers of the present invention improves the operation of the de-20 labeling machines and their effectiveness at removing labels from containers while minimizing or eliminating damage to the containers inflicted from the de-labeling machine.
Other objects and advantages of the present 25 invention will become more apparent in view of the attached drawings and in light of the following detailed description of the invention.
Brief Description Of The Drawings
FIGURE l is a flow chart illustrating the 3 0 steps of the process of the present invention;
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FIGURE 2 is a perspective view of a roll-fed labeling apparatus including a label cutter and a perforator,-
FIGURE 3 is a perspective view of a sleeve 5 label being applied to a container;
FIGURE 4 is a perspective view of a cut and stack label magazine applying the label to the container;
FIGURE 5 is a perspective view of a label 10 cutter and a perforator for forming a frangible region on a label;
FIGURE 6 is a perspective view of a fluid knife used to de-label a container at the frangible region on a label;
lb FIGURE 7 is a plan view of a de-labeling system wherein mechanical fingers are used to break a label at a frangible region and strip it from a contain-
e r; and
FIGURE 8 is a plan view of a bottle de-label-20 ing apparatus wherein counter-rotating rollers are used to first break the label at a frangible region after which a vacuum label separating device tears the flagging label from the container.
Best Modes For Carrying Out The Invention
2 5 Referring now to the drawings, in Figure 1,
the general steps of the present invention are shown diagrammatically with references to the other Figures as
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appropriate to illustrate the steps of the invention. As shown in Figure 1, the invention can be used to de-label containers labeled by roll-fed, sleeve-applied, or cut and stack labeling methods. The present invention 5 is not intended for UBe with pressure-sensitive type labels having adhesive adhering the entire label to the container since the inclusion of a frangible zone on the label would not appreciably improve automatic de-labeling operations.
Referring now to Figures 1 and 2, a roll-fed labeler 10 is shown wherein a roll of labels 12 are preprinted with label indicia and provided to the roll-fed labeler 10. A web 14 is advanced from the roll of labels 12 to a conventional label cutter 16. A perfora-15 tor 18 is provided to form a perforated or frangible region on the label. After the cutter 16 cuts individual segments from the web 14, the label segments are provided to a vacuum drum 20 and then applied directly to unlabeled containers 22 which are fed into the roll-20 fed labeler 10. The labels are coated on leading and trailing edges with an adhesive or other suitable solvent, paste or glue. The leading edge of the labels are then tacked to the unlabeled containers 22. The labels are then wrapped around the container with the 25 leading edge adhering to the container and the trailing edge adhering to the leading edge to form a labeled container 24. Cf course, the trailing edge could adhere directly or. the container. As can be appreciated, the present invention can also be used with spot or full-3 0 wrap labels provided these labels have extensive nonadherent portions which will flag out from the container upon breaking the label at the frangible region or zone.
Printed from Mimosa 13:12:01
Referring now to Figures 1 and 3, a sleeve applied label can also be provided with the present invention. A container 3 0 can be labeled with a sleeve 32 which includes a score line 34. Similarly to the frangible region, the score line 34 facilitates the de-labeling process.
Referring to Figure 4, another approach to labeling that can be used with the present invention is a cut and stack labeling machine. With a cut and stack labeling machine, a magazine 30 is provided with a stack of labels 40. The labels 40 have a frangible region 42 which is a score or perforated line. The frangible region 42 is formed on the labels 40 prior to being loaded into the magazine 38. Labels 40 are applied to containers 44 in accordance with conventional cut and stack labeling techniques.
Referring now to Figure 5, a method of forming a frangible region on a label with a label cutter 48 is shown. The label cutter 4 8 includes a vacuum drum 50 for supporting the labels. A conventional cutter knife 52 is adapted to cut labels supported by the vacuum drum 50 as it passes the label cutter 40. A perforator 54 is preferably disposed at a circumferentially spaced location from the cutter knife 52 in order to form a fairly long segment of label material having a frangible region between the adherent leading and trailing edges,
Referring now to Figure 1, after the frangible region is formed on the label, the label is applied to the container. Either new or recycled containers can be labeled with any one of the conventional labeling methods described. In many instances, labels are shrink-fitted to the container by applying heat. The
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1C
heat causes a film or foam label to contract forming a tight fit on the container.
After labeling, the containers are provided through distribution channels to consumers for consumption of the product. Upon consumption, consumers are encouraged to return the containers with deposits or the like for recycling.
The empty labeled containers are collected and supplied to an automatic de-labeling machine. As can be appreciated from the de-labeling methods shown in Figures 6, 7, and 8, various means of applying a mechanical force to break the label can be provided. In Figure 6, labeled containers 58 having labels including a frangible region 60 are provided to a de-labeler. The de-labeler consists of a fluid nozzle 62 which is used to strip the label from the labeled container 58. Fluid nozzle 62 may direct air or liquid such as water, toward the labeled container 58 with a force sufficient to break or rupture the frangible region 60 but with less force than would be required to split other portions of the label. Breaking frangible region 60 creates a flagging label end 64 which hangs loosely from the container. The label is then easily removed by a label separator. The function of the label separator will be described below.
Another de-labeling approach is shown in Figure 7. A labeled container 6 8 is fed by a conveyor to stripping finger wheels 70 which rotate against the labeled container 6 8 causing frangible region 72 to split resulting in flagging label ends 74. Again, the
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force applied to split the frangible region is less than the force required to split other portions of the label.
Referring now to Figure 8, labeled container bo may be provided to counter rotating rollers 82. Rollers 82 apply tension to the label by surface contact causing the frangible region 84 to break first resulting in flagging label ends 86. The flagging label ends 86 provide broad surface area upon which the vacuum label separator 88 may act to pull and strip the label from the container. After the label is separated from the container as shown in Figure 1, the label material can be removed and discarded or recycled. The de-labeled container may then be cleaned for reuse and provided again to the label application line to receive a fresh label.
It should be appreciated that a simple and effective method for labeling containers so that they may easily be de-labeled by automatic de-labeling equipment has been disclosed. Applicant has disclosed several different embodiments of the invention to illustrate the invention and to provide an enabling disclosure. The preceding description should not be read in a limiting sense. The present invention should be construed in accordance with the broad scope and spirit of the following claims.
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Claims (15)
1. A method of labeling and de-labeling a container, said method comprising the steps of: preparing the container for labeling; 5 preparing a label with an adherent portion and an extensive non-adherent portion for application to said container; forming a frangible region on said non-adherent portion of said label which extends across said 10 label sufficiently frangible to facilitate de-labeling without unduly weakening the durability of the label; applying said label to said container to form a labeled container; introducing said labeled container for distri-15 but ion to consumers for use and collection of said labeled container from consumers; applying a mechanical force to said labeled container only after completion of said introducing step, said mechanical force being sufficient to break 2 0 said label at said frangible region so that said nonadherent portion will flag out when said label breaks; and utilizing the flagged out portion of said nonadherent portion to facilitate the separation of said 25 label from said container.
2. The method of labeling the container of claim 1 wherein said step of preparing a label for application to said container further comprises printing said label as one of a plurality of labels in a roll of 30 label material.
3. The method of labeling the container of claim 2 wherein said step of forming a frangible region PCT/US 96/19268 I PEA/US 10JUN199? -12- comprises perforating said label transverse to the direction of label movement in a roll fed labeling machine and substantially completely across said label.
4. The method of labeling the container of 5 claim 2 wherein said step of forming a frangible region comprises scoring said label transverse to the direction of label movement in a roll fed labeling machine and substantially completely across said label.
5. The method of labeling the container of 10 claim 1 wherein said step of preparing a label for application to said container further comprises printing said label and forming said label into a sleeve.
6. The method of labeling the container of claim 5 wherein said step of forming a frangible region 15 comprises perforating said label substantially completely across the formed sleeve from one edge of said sleeve to the other.
7. The method of labeling the container of claim 5 wherein said step of forming a frangible region 2 0 comprises scoring said label substantially completely across the formed sleeve from one edge of said sleeve to the other.
8. The method of labeling the container of claim 1 wherein said step of preparing a label for 25 application to said container further comprises printing said label and stacking said label in a magazine.
9. The method of labeling the container of claim 8 wherein said step of forming a frangible region AMCN0E0 SHfST PCT/US96/1926& IPEA/US i oJUN1997 -13- comprises perforating said label substantially completely across one edge of said label to the other.
10. The method of labeling the container of claim 8 wherein said step of forming a frangible region 5 comprises scoring said label substantially completely across one edge of said label to the other.
11. The method of labeling the container of claim l wherein said step of applying said label to said container comprises tacking a leading adherent end 10 portion of the label having said frangible region already formed thereon to said container and wrapping said label around said container and securing a trailing adherent edge portion of said label to the leading edge.
12. A method of labeling and de-labeling a 15 container, said method comprising the steps of: preparing the container for labeling; preparing a pre-formed sleeve label for application to said container; forming a frangible region on said sleeve 20 label sufficiently frangible to facilitate de-labeling without unduly weakening the durability of the label; sliding said sleeve label over one end of said container and shrinking said sleeve label to said container, said frangible region extending across said 25 sleeve label in the direction that said label is slid over said one end of said container; introducing said labeled container for distribution to consumers for use and collection of said labeled container from consumers with said frangible 30 region remaining intact; applying a mechanical force to said labeled container only after completion of said introducing AMfcNLiLi"' PCT/US 96/19268 1PEA/US iojuhs# -14- step, said mechanical force being sufficient to break said label at said frangible region causing flagging of a portion of said label; and utilizing the flagged out portion of said 5 label to facilitate the separation of said label from said container after said mechanical force has caused flagging of said portion of said label.
13. The method of labeling the container of claim 1 wherein said step of applying a mechanical force 10 to said labeled container comprises directing a fluid jet knife toward said label at said frangible region.
14. The method of labeling the container of claim 1 wherein said step of applying a mechanical force to said labeled container comprises contacting said 15 labeled container with mechanical moving fingers to break said label.
15. The method of labeling the container of claim 1 wherein said step of applying a mechanical force to said labeled container comprises contacting said 20 labeled container with counter rotating rollers on opposite sides of said frangible region to break said label. END OF CLAIMS
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US56700395A | 1995-12-04 | 1995-12-04 | |
PCT/US1996/019268 WO1997020694A1 (en) | 1995-12-04 | 1996-12-02 | Method of labeling containers to facilitate de-labeling |
Publications (1)
Publication Number | Publication Date |
---|---|
NZ324190A true NZ324190A (en) | 1998-08-26 |
Family
ID=24265353
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NZ324190A NZ324190A (en) | 1995-12-04 | 1996-12-02 | Method of labelling containers to facilitate de-labeling includes forming a frangible region on label |
Country Status (12)
Country | Link |
---|---|
EP (1) | EP0869869A4 (en) |
JP (1) | JP2000502017A (en) |
CN (1) | CN1207705A (en) |
AR (1) | AR004358A1 (en) |
AU (1) | AU709810B2 (en) |
BR (1) | BR9611686A (en) |
CA (1) | CA2239316C (en) |
CZ (1) | CZ170998A3 (en) |
NZ (1) | NZ324190A (en) |
TR (1) | TR199801015T2 (en) |
WO (1) | WO1997020694A1 (en) |
ZA (1) | ZA9610069B (en) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19630690A1 (en) * | 1996-07-30 | 1998-02-05 | Kronseder Maschf Krones | Bottle or the like with a label encompassing the scope, method and device for producing this bottle |
US8020359B2 (en) | 2009-05-11 | 2011-09-20 | The Coca-Cola Company | Method of using temporary decoration to mass customize refillable glass vessels |
FR2945522B1 (en) * | 2009-05-14 | 2014-05-23 | Decomatic Sa | EASY OPENING SLEEVE. |
IT1397462B1 (en) * | 2009-12-30 | 2013-01-10 | Sacmi Labelling S P A Ora Sacmi Verona S P A | DEVICE FOR THE PRODUCTION OF A SLEEVE LABEL |
DE102014105485A1 (en) * | 2014-04-17 | 2015-10-22 | Krones Ag | Apparatus and method for providing containers with glued labels |
CN112249464B (en) * | 2020-10-02 | 2021-06-01 | 深圳市荣航供应链有限公司 | Subsides mark device with sweep sign indicating number function |
CN114671106B (en) * | 2022-05-26 | 2022-08-23 | 徐州金之泰包装新材料科技有限公司 | Automatic conveying machinery for production of metal packaging cans |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB765981A (en) * | 1953-12-16 | 1957-01-16 | Bror Henrik Hageltorn | Improvements in or relating to labelling bottles, cans, or like containers |
US3951727A (en) * | 1972-07-06 | 1976-04-20 | Greenberg William B | Delaminating method and apparatus |
US4325775A (en) * | 1980-02-04 | 1982-04-20 | Horst Moeller | Delabeler |
GB2141972B (en) * | 1983-06-21 | 1987-06-10 | Metal Box Plc | Methods and apparatus for removing labels or carriers for containers |
DE3723074A1 (en) * | 1986-08-16 | 1988-02-18 | Reemtsma H F & Ph | Bottle crate |
US5037499A (en) * | 1989-11-29 | 1991-08-06 | B & H Manufacturing Company, Inc. | Labeling machine combining a turret and a vacuum drum-roll on pad |
GB2257681B (en) * | 1991-07-16 | 1995-04-12 | Graham Labelling Systems Limit | Banding apparatus and method |
GB9412849D0 (en) * | 1993-08-02 | 1994-08-17 | Marketing Store Ltd | Package |
DE4342383A1 (en) * | 1993-12-11 | 1995-06-14 | Hoechst Ag | Environmentally friendly packaging |
-
1996
- 1996-11-29 ZA ZA9610069A patent/ZA9610069B/en unknown
- 1996-12-02 CA CA002239316A patent/CA2239316C/en not_active Expired - Fee Related
- 1996-12-02 WO PCT/US1996/019268 patent/WO1997020694A1/en not_active Application Discontinuation
- 1996-12-02 BR BR9611686A patent/BR9611686A/en not_active Application Discontinuation
- 1996-12-02 CN CN96199749A patent/CN1207705A/en active Pending
- 1996-12-02 EP EP96942133A patent/EP0869869A4/en not_active Withdrawn
- 1996-12-02 JP JP09521380A patent/JP2000502017A/en not_active Ceased
- 1996-12-02 CZ CZ981709A patent/CZ170998A3/en unknown
- 1996-12-02 AU AU11286/97A patent/AU709810B2/en not_active Ceased
- 1996-12-02 NZ NZ324190A patent/NZ324190A/en unknown
- 1996-12-02 TR TR1998/01015T patent/TR199801015T2/en unknown
- 1996-12-03 AR ARP960105473A patent/AR004358A1/en unknown
Also Published As
Publication number | Publication date |
---|---|
CN1207705A (en) | 1999-02-10 |
AR004358A1 (en) | 1998-11-04 |
CZ170998A3 (en) | 1999-05-12 |
CA2239316C (en) | 2005-03-15 |
AU1128697A (en) | 1997-06-27 |
BR9611686A (en) | 1999-03-02 |
JP2000502017A (en) | 2000-02-22 |
EP0869869A1 (en) | 1998-10-14 |
TR199801015T2 (en) | 1998-09-21 |
CA2239316A1 (en) | 1997-06-12 |
EP0869869A4 (en) | 2000-06-14 |
ZA9610069B (en) | 1997-06-23 |
WO1997020694A1 (en) | 1997-06-12 |
AU709810B2 (en) | 1999-09-09 |
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