NZ286665A - Stout brewing process - Google Patents

Description

New Zealand No. 286665 International No. PCT/ TO BE ENTERED AFTER ACCEPTANCE AND PUBLICATION Priority dates: Complete Specification Filed: 24.05.1996 Classification:(6) C12C12/00 Publication date: 24 June 1997 Journal No.: 1417 NEW ZEALAND PATENTS ACT 1953 COMPLETE SPECIFICATION Title of Invention: A brewing process Name, address and nationality of applicant(s) as in international application form: VALDOSA LIMITED, an Irish company of 90 South Mall, Cork, Ireland 28 6 u o PATENTS FORM 5 Number: PATENTS ACT 1953 COMPLETE SPECIFICATION A BREWING PROCESS Dated: We, VALDOSA LTD of 90 South Mall, Cork, Ireland, an Irish company, do hereby declare the invention for which we pray that a patent may be granted to us, and the method by which it is to be performed, to be particularly described in and by the following statement. 286 w o - la - The invention relates to a stout brewing process.

Theire are considerable tachnical difficulties in producing high quality stout having desired properties. A complex series of variables are involved in the production process 5 and it is difficult to reproduce the production process from one production site to another.

One particular area of difficulty is in removing unwanted particulates from the stout. It is known to use centrifuges for this purpose. However, the capacity of 10 such centrifuges is limited and it is often difficult to optimise the operation of the centrifuges.

The invention is therefore directed towards providing an improved process for producing stout which will overcome at least some of these difficulties.

According to the invention, there is provided a stout brewing process comprising the steps of:- preparing malt by cleaning, weighing, and milling malt; preparing roasted barley by cleaning, weighing and 20 milling roasted barley; mixing the prepared malt, the prepared roasted barley and hot water in a mash tun to prepare a brew; preparing sweet wort by agitating the brew and allowing starch in the brew to convert to sugar by enzymatic activity; l~ * *x, *-6 JUN1996 V 28 6 6 <o n separating spent grains of malt and roasted barley from the sweet wort; boiling the sweet wort; adding hops to the boiling sweet wort to prepare 5 hopped wort; removing hop residues from the hopped wort; cooling the hopped wort; adding yeast and sterile air to the hopped wort and allowing the mixture thus formed to ferment to 10 produce stout; blending and storing the stout; monitoring the oxygen content of the stout; applying a precoat material to a plate filter; passing the stout through the precoated plate filter 15 to substantially clarify the stout by removing particulates from the stout and forming bright diluted stout; controlling the carbon dioxide content of the stout; controlling the nitrogen content of the stout; and storing the stout.

In a particularly preferred embodiment of the invention, the process includes the step of adding bodyfeed Serial to the stout in-line upstream of the prec©Sted pla4ei^, *-6 )UN1996*7 2.8 6 ^ ^ filter.

In a preferred embodiment of the invention, the process includes the steps of:- delivering the bright filtered stout into a bright 5 stout buffer tank prior to delivery to a main bright stout storage tank; and controlling the level of bright stout in the buffer tank to maintain a substantially constant pressure drop across the plate filter.

In this case, preferably the level of bright stout in the buffer tank is controlled by reducing the rate of flow of bright stout from the buffer tank if the level of bright stout drops below a preset level.

Preferably, the storage stout is delivered into an 15 unfiltered stout buffer tank upstream of the plate filter. In this case, preferably the process includes the step of controlling the level of unfiltered stout in the buffer tank to maintain a substantially constant pressure drop across the filter.

In a preferred arrangement, the amount of oxygen in the stout is monitored both upstream and downstream of the plate filter.

Preferably, the process includes the step of monitoring the alcohol content of the filtered bright stout and 25 injecting dilution water into the bright stout as required to achieve a desired alcohol content.

The invention will be more clearly understood from the *-6 1U U1996 '. \ 28 6o B ^ 4 - only, with reference to the accompanying drawings, in which:- Fig. 1 is a schematic block diagram of the process of the invention? and Fig. 2 is a schematic flow diagram illustrating filtration and associated steps in the process of the invention.

Referring to the drawings, and initially to Fig. 1, there is illustrated a brewing process for stout according to 10 the invention. In the brewing process, malt and roasted barley are separately stored in silos and are then cleaned and subsequently weighed prior to milling. The malt and roasted barley are then mixed with hot water in a mash tun. The brew is. transferred to a lauter tun to separate 15 the sweet wort. Spent grains of malt and roasted barley are then removed. The sweet wort is then pumped to a wort copper where it is boiled and hops are added. The hopped wort is then pumped to a whirlpool where hop residues are drained away. At this stage, the sweet wort is still hot 20 and it is then pumped to a heat exchanger where it is cooled. The cooled sweet wort is then pumped to a fermentation vessel where yeast and sterile air are added and it is allowed to ferment to form stout. The stout is then blended and stored in a storage tank to allow it to 25 mature.

In the process of the invention, the stout is clarified as will be described in more detail below. The carbon dioxide and nitrogen levels in the stout are controlled and the stout is then stored, ready for delivery into 30 barrels, as required.

M <*-6 J J i.1996 280663 In the process of the invention, Murphy's Irish Stout Yeast having the following characteristics is added to the cooled sweet wort in the fermentation vessel.

TABLE 1 Microbiological plate No growth on Wort Agar @ characteristics 37°C, SDA+, Lys and Cu.

No Melibiase activity.

No killer yeast activity.

No Phenolic flavour production.

Fermentation Has some characteristics of characteristics both top and bottom fermenting yeasts.

After two days fermentation it floats on the liquid surface and at the end of the fermentation it settles rapidly.

Highly hydrophobic and flocculent ( ABS/min 0.8 - 1.0).

Dextrin degradation No activity.

Aroma profile Low S02 production. Slightly low ester production.

Slightly high production of higher alcohols. No 4 - VG or styrene production. t colony morphology 95% dark green malt colony type with pseudohyphale. 5% small white edged/green centre colony type.

O (2 U G 3 Referring to Fig. 2, in the process of the invention a plate filter 1 is used to substantially clarify the stout by removing particulates from the stout and forming bright diluted stout.

Stout to be clarified is stored in a storage beer vessel 2. The flow of beer from the vessel 2 is monitored by a flowmeter 3 and the oxygen content of the beer is monitored by an oxygen analyser 4. The beer is delivered into a balance tank 5 which is held at a pressure of 10 approximately 0.7 bar. The level of unfiltered stout in the balance tank 5 is controlled to maintain a substantially constant pressure drop across the filter 1. Bright diluted beer from the plate filter 1 is collected in a buffer vessel 7, held at approximately 0.5 bar 15 pressure. The oxygen content of the bright beer delivered into the buffer vessel 7 is monitored by a second oxygen analyser 8. The level of bright stout in the buffer tank is controlled to maintain a substantially constant pressure drop across the plate filter 1 and hence optimise 20 the operation of the filter 1. The level of bright stout in the buffer tank is controlled by reducing the rate of flow of bright stout from the buffer vessel 7 if the level of bright stout drops below a preset level. A control valve 10 with a feedback control loop to a level detector 25 is used to control the flow of bright stout from the buffer vessel 7.

The rate of flow of bright stout from the buffer vessel 7 is monitored by a flowmeter 11. The alcohol content of the stout is also monitored by an alcohol analyser 12. If 30 the amount of alcohol present in the bright stout is above a predetermined value, a control valve 13 on a dilution water flow line 14 is activated. The flow of dilution water is monitored by a further flow m^errlS.

X, •? ^ ^ -6 .1UN1996 •?- . .,<*v on C\ ! , ; ■ Cm O ^ ^ ^ In this way, the amount of dilution water added is closely controlled to achieve the desired alcohol content in the bright stout. The bright stout having, if necessary, been diluted with water to achieve a uniform desired alcohol 5 content is delivered into a storage vessel 18 for further processing.

The filter plates of the plate filter 1 are first coated by applying a precoat material to the filter plates from a make-up vessel 20 through a precoat delivery line 21. 10 Bodyfeed material is added to the stout in-line upstream of the precoated plate filter 1 through a body feed delivery line 22.

EXAMPLE The stout was filtered using a ZHF/Z kieselguhr horizontal 15 plate filter available from Schenk Fiterbaum GmbH of Germany. The filter had the following features filter elements: approx. 46m2 spacing between elements: 35 mm sludge volume: 1,500 litres precoat material: approx 45.4 Kg of Celite 5C available from Celite Corporation Bodyfeed added to stout Dilution Target: approx. 45.4 Kg of Celite Standard 3UPERCEL mixed with approx. 22.7 Kg of Celite 577, both available from Celite Corporation. 9 .4°P 28 6 6 6 5 - 8 ' Time (Mins) Prefilter Pressure (Bar) Post Filter Pressure (Bar) Flow Rate through filter hl/hr Oxygen Content of Dilution Water (ppb) Alcohol Level (% vol) Total Filtered (hectalitres) 0 3.0 0.9 430.6 21 4.0 - 3 2.9 0.7 438.2 22 4.1 88.0 12 3.2 0.9 360.0 23 4.0 173.4 21 3.1 0.7 362.1 23 4.1 - 26 3.2 0.8 358.5 4.0 240.5 29 Chase Water Recirculation Time: 34 minutes Total Filtration Time: 29 minutes Run Out Time: 45 minutes Final Water Volume: 57.3 HL's Final Stout Volume: 276.3 HL's Total Volume to Bright Stout Tank: 333.6 HL's The bright stout thus produced had excellent properties of 25 uniform alcohol content, colour, pH, dissolved C02, visual clarity, yeast content, taste and aroma.

The foregoing describes preferred fozms of the invention and it is to be understood that the scope of the invention is not to be limited to the specific forms described. Modifications and variations as will be obvious to a person skilled in the art may be made to the invention without departing from the scope of the invention as defined in the attached claims. 28 6 'o 61.

Claims (11)

WHAT WE CLAIM IS:

1. A stout brewing process comprising the steps of:- preparing malt by cleaning, weighing, and milling malt; 5 preparing roasted barley by cleaning, weighing and milling roasted barley; mixing the prepared n<<xlt, the prepared roasted barley and hot water in a mash tun to prepare a brew; 10 preparing sweet wort by agitating the brew and allowing starch in the brew to convert to sugar by enzymatic activity; separating spent grains of malt and roasted barley from the sweet wort; 15 boiling the sweet wort; adding hops to the boiling sweet wort to prepare hopped wort; removing hop residues from the hopped wort; cooling the hopped wort; 20 adding yeast and sterile air to the hopped wort and allowing the mixture thus formed to ferment to produce stout; blending and storing the stout; * X.'Y- v o) -A ^ y -6 JUN1996 > 286u - 10 - monitoring the oxygen content of the stout; applying a precoat material to a plate filter; passing the stout through the precoated plate filter to substantially clarify the stout by 5 removing particulates from the stout and forming bright diluted stout; controlling the carbon dioxide content of the stout; controlling the nitrogen content of the stout; 10 and storing the stout.

2. A process as claimed in claim 1 including the step of adding bodyfeed material to the stout in-line upstream of the precoated plate filter. 15

3. A process as claimed in claim 1 or 2 including the steps ofs- delivering the bright filtered stout into a bright stout buffer tank prior to delivery to a main bright stout storage tank; and 20 controlling the level of bright stout in the buffer tank to maintain a substantially constant pressure drop across the plate filter.

4. A process as claimed in claim 3 wherein the level of bright stout in the buffer tank is controlled by 25 reducing the rate of flow of bright stout from the buffer tank if the le/el of bright^^fctft*"drops below A* •* *c\\ 1^1 —" ~ 1*1' C-6 )Utt1996 28 6 6 6 5 - ii - a preset level.

5. A process as claimed in any preceding claim wherein the storage stout is delivered into an unfiltered stout buffer tank upstream of the plate filter. 5

6 . A process, 'is claimed in claim 5 including the step of controlling the level of unfiltered stout in the buffer tank to maintain a substantially constant pressure drop across the filter.

7. A process as claimed in any preceding claim wherein 10 the amount of oxygen in the stout is monitored both upstream and downstream of the plate filter.

8. A process as claimed in any preceding claim including the step of monitoring the alcohol content of the filtered bright stout and injecting dilution water 15 into the bright stout as required to achieve a desired alcohol content.

9. A process as claimed in any preceding claim wherein the yeast added to the hopped wort has the characteristics set out in Table 1 herein. 2 0

10. A process according to claim 1 for producing stout substantially as hereinbefore described with reference to the accompanying drawings and examples.

11. Stout whenever produced by a process as claimed in any preceding claim.