NO840973L - Fremgangsmaate ved fremstilling av vannfritt aluminiumklorid fra aluminiumkloridhexahydrat som skriver seg fra syreutluting - Google Patents
Fremgangsmaate ved fremstilling av vannfritt aluminiumklorid fra aluminiumkloridhexahydrat som skriver seg fra syreutlutingInfo
- Publication number
- NO840973L NO840973L NO840973A NO840973A NO840973L NO 840973 L NO840973 L NO 840973L NO 840973 A NO840973 A NO 840973A NO 840973 A NO840973 A NO 840973A NO 840973 L NO840973 L NO 840973L
- Authority
- NO
- Norway
- Prior art keywords
- aluminum chloride
- ach
- liquid
- aluminum
- leaching
- Prior art date
Links
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 title claims description 105
- 238000000034 method Methods 0.000 title claims description 34
- JGDITNMASUZKPW-UHFFFAOYSA-K aluminium trichloride hexahydrate Chemical compound O.O.O.O.O.O.Cl[Al](Cl)Cl JGDITNMASUZKPW-UHFFFAOYSA-K 0.000 title claims description 10
- 239000002253 acid Substances 0.000 title description 13
- 230000007717 exclusion Effects 0.000 title description 2
- 229940009861 aluminum chloride hexahydrate Drugs 0.000 claims description 49
- 238000002386 leaching Methods 0.000 claims description 33
- 239000004927 clay Substances 0.000 claims description 32
- 239000007788 liquid Substances 0.000 claims description 30
- 229940063656 aluminum chloride Drugs 0.000 claims description 28
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 27
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 19
- 229910052782 aluminium Inorganic materials 0.000 claims description 19
- 239000013078 crystal Substances 0.000 claims description 19
- 239000003638 chemical reducing agent Substances 0.000 claims description 16
- 238000002425 crystallisation Methods 0.000 claims description 16
- 230000008025 crystallization Effects 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 16
- 238000004519 manufacturing process Methods 0.000 claims description 15
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 12
- 239000000460 chlorine Substances 0.000 claims description 12
- 229910052801 chlorine Inorganic materials 0.000 claims description 12
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 12
- 239000002002 slurry Substances 0.000 claims description 11
- 239000007787 solid Substances 0.000 claims description 11
- 239000007789 gas Substances 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 238000000926 separation method Methods 0.000 claims description 6
- 229910002091 carbon monoxide Inorganic materials 0.000 claims description 5
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000004411 aluminium Substances 0.000 claims description 3
- 239000002008 calcined petroleum coke Substances 0.000 claims description 3
- 239000001569 carbon dioxide Substances 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims 2
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 24
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 13
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 13
- 238000001354 calcination Methods 0.000 description 12
- 229910052742 iron Inorganic materials 0.000 description 12
- 230000002829 reductive effect Effects 0.000 description 12
- 238000005660 chlorination reaction Methods 0.000 description 10
- 238000002474 experimental method Methods 0.000 description 9
- 239000000047 product Substances 0.000 description 6
- 238000005868 electrolysis reaction Methods 0.000 description 5
- 239000012535 impurity Substances 0.000 description 5
- 239000012452 mother liquor Substances 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000003245 coal Substances 0.000 description 4
- MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- 239000011574 phosphorus Substances 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 238000005352 clarification Methods 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 238000011010 flushing procedure Methods 0.000 description 3
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 230000003134 recirculating effect Effects 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000000638 solvent extraction Methods 0.000 description 3
- 239000002562 thickening agent Substances 0.000 description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- 235000012211 aluminium silicate Nutrition 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000012320 chlorinating reagent Substances 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 238000009837 dry grinding Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000003350 kerosene Substances 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical compound [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- ZTHNOZQGTXKVNZ-UHFFFAOYSA-L dichloroaluminum Chemical compound Cl[Al]Cl ZTHNOZQGTXKVNZ-UHFFFAOYSA-L 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000010881 fly ash Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- 229910052622 kaolinite Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000002006 petroleum coke Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 150000003335 secondary amines Chemical class 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 230000000153 supplemental effect Effects 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
- 238000003828 vacuum filtration Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
- C25C3/06—Electrolytic production, recovery or refining of metals by electrolysis of melts of aluminium
- C25C3/22—Collecting emitted gases
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/48—Halides, with or without other cations besides aluminium
- C01F7/56—Chlorides
- C01F7/58—Preparation of anhydrous aluminium chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Electrochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/400,198 US4465566A (en) | 1982-07-20 | 1982-07-20 | Method of producing anhydrous aluminum chloride from acid leach-derived ACH and the production of aluminum therefrom |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO840973L true NO840973L (no) | 1984-03-13 |
Family
ID=23582615
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO840973A NO840973L (no) | 1982-07-20 | 1984-03-13 | Fremgangsmaate ved fremstilling av vannfritt aluminiumklorid fra aluminiumkloridhexahydrat som skriver seg fra syreutluting |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4465566A (fr) |
| EP (1) | EP0113771B1 (fr) |
| AU (1) | AU1826883A (fr) |
| BR (1) | BR8307437A (fr) |
| CA (1) | CA1199473A (fr) |
| DE (1) | DE3390076T1 (fr) |
| GB (1) | GB2137607B (fr) |
| NO (1) | NO840973L (fr) |
| SE (1) | SE8401356L (fr) |
| WO (1) | WO1984000356A1 (fr) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4559215A (en) * | 1983-08-03 | 1985-12-17 | Atlantic Richfield Company | Production of anhydrous aluminum chloride from hydrated alumina |
| US4915930A (en) * | 1986-07-31 | 1990-04-10 | Aluminum Company Of America | Process for producing aluminum hydroxide of improved whiteness |
| CA2122364A1 (fr) * | 1992-08-04 | 1994-02-17 | Alexei A. Marakushev | Methode de production d'aluminium a partir de materiaux bruts alumineux |
| US7910012B2 (en) * | 2007-07-16 | 2011-03-22 | General Electric Company | Composition, membrane, and associated method |
| WO2012126092A1 (fr) | 2011-03-18 | 2012-09-27 | Orbite Aluminae Inc. | Procédés permettant de récupérer des éléments de terres rares à partir de matériaux renfermant de l'aluminium |
| US9410227B2 (en) | 2011-05-04 | 2016-08-09 | Orbite Technologies Inc. | Processes for recovering rare earth elements from various ores |
| EP2714594A4 (fr) | 2011-06-03 | 2015-05-20 | Orbite Aluminae Inc | Procédés d'obtention d'hématite |
| EP2755918A4 (fr) | 2011-09-16 | 2015-07-01 | Orbite Aluminae Inc | Procédés de préparation d'alumine et de divers autres produits |
| CA2875776A1 (fr) | 2012-01-10 | 2013-07-18 | Richard Boudreault | Procedes de traitement de boue rouge |
| WO2013142957A1 (fr) | 2012-03-29 | 2013-10-03 | Orbite Aluminae Inc. | Procédés de traitement de cendres volantes |
| US9290828B2 (en) | 2012-07-12 | 2016-03-22 | Orbite Technologies Inc. | Processes for preparing titanium oxide and various other products |
| BR112015006536A2 (pt) | 2012-09-26 | 2017-08-08 | Orbite Aluminae Inc | processos para preparar alumina e cloreto de magnésio por lixiviação com hcl de vários materiais. |
| US9534274B2 (en) | 2012-11-14 | 2017-01-03 | Orbite Technologies Inc. | Methods for purifying aluminium ions |
| WO2015176166A1 (fr) * | 2014-05-21 | 2015-11-26 | Orbite Technologies Inc. | Procédés de décomposition de chlorure d'aluminium en alumine |
| WO2016049777A1 (fr) * | 2014-10-03 | 2016-04-07 | Orbite Technologies Inc. | Procédés de purification d'ions d'aluminium |
| US11746021B2 (en) | 2019-04-18 | 2023-09-05 | Nextchem, Llc | High purity aluminum oxide via electrodialysis |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2249761A (en) * | 1938-08-05 | 1941-07-22 | Chemical Foundation Inc | Acid process for the extraction of alumina |
| US2376696A (en) * | 1942-06-10 | 1945-05-22 | Chemical Foundation Inc | Production of alumina |
| US3842163A (en) * | 1971-09-07 | 1974-10-15 | Aluminum Co Of America | Production of aluminum chloride |
| US3755099A (en) * | 1971-09-08 | 1973-08-28 | Aluminum Co Of America | Light metal production |
| US4039648A (en) * | 1975-12-12 | 1977-08-02 | Aluminum Company Of America | Production of aluminum chloride |
| US4235860A (en) * | 1979-06-07 | 1980-11-25 | Aluminum Company Of America | Chlorination of aluminous material at superatmospheric pressure |
| US4105752A (en) * | 1976-12-20 | 1978-08-08 | Aluminum Company Of America | Aluminum chloride production |
| DD130656A1 (de) * | 1977-04-18 | 1978-04-19 | Dieter Petzold | Verfahren zur herstellung von wasserfreiem aluminiumchlorid |
| US4151061A (en) * | 1977-11-15 | 1979-04-24 | Nippon Light Metal Company Limited | Aluminum electrolytic cell |
| DD147185A3 (de) * | 1978-04-24 | 1981-03-25 | Siegfried Ziegenbalg | Verfahren zur herstellung von reinem aluminiumoxid |
| AU528882B2 (en) * | 1978-09-26 | 1983-05-19 | Commonwealth Scientific And Industrial Research Organisation | Producing anhydrous aluminium chloride |
| NO147516C (no) * | 1979-02-13 | 1983-04-27 | Elkem Spigerverket As | Fremgangsmaate for utfelling av et rent aluminiumklorid fra loesninger som inneholder aluminium- og magnesiumioner. |
| NO790460L (no) * | 1979-02-13 | 1980-08-14 | Elkem Spigerverket As | Fremstilling av et rent aluminiumoksyd fra loesninger inneholdende opploeste aluminiumioner og jernioner |
| US4284607A (en) * | 1979-09-10 | 1981-08-18 | Aluminum Company Of America | Chlorination of aluminous materials using preselected solid reducing agents |
-
1982
- 1982-07-20 US US06/400,198 patent/US4465566A/en not_active Expired - Fee Related
-
1983
- 1983-07-13 DE DE19833390076 patent/DE3390076T1/de not_active Withdrawn
- 1983-07-13 EP EP83902549A patent/EP0113771B1/fr not_active Expired
- 1983-07-13 BR BR8307437A patent/BR8307437A/pt not_active IP Right Cessation
- 1983-07-13 WO PCT/US1983/001050 patent/WO1984000356A1/fr active IP Right Grant
- 1983-07-13 GB GB08406336A patent/GB2137607B/en not_active Expired
- 1983-07-13 AU AU18268/83A patent/AU1826883A/en not_active Abandoned
- 1983-07-19 CA CA000432741A patent/CA1199473A/fr not_active Expired
-
1984
- 1984-03-12 SE SE8401356A patent/SE8401356L/xx not_active Application Discontinuation
- 1984-03-13 NO NO840973A patent/NO840973L/no unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA1199473A (fr) | 1986-01-21 |
| SE8401356D0 (sv) | 1984-03-12 |
| AU1826883A (en) | 1984-02-08 |
| GB8406336D0 (en) | 1984-04-11 |
| EP0113771B1 (fr) | 1987-05-27 |
| GB2137607B (en) | 1986-04-30 |
| DE3390076T1 (de) | 1984-10-18 |
| SE8401356L (sv) | 1984-03-12 |
| EP0113771A4 (fr) | 1984-11-23 |
| EP0113771A1 (fr) | 1984-07-25 |
| WO1984000356A1 (fr) | 1984-02-02 |
| US4465566A (en) | 1984-08-14 |
| BR8307437A (pt) | 1984-07-17 |
| GB2137607A (en) | 1984-10-10 |
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