NO20052709L - NIR spektroskopimetode for a analysere kjemiske prosesskomponenter - Google Patents
NIR spektroskopimetode for a analysere kjemiske prosesskomponenterInfo
- Publication number
- NO20052709L NO20052709L NO20052709A NO20052709A NO20052709L NO 20052709 L NO20052709 L NO 20052709L NO 20052709 A NO20052709 A NO 20052709A NO 20052709 A NO20052709 A NO 20052709A NO 20052709 L NO20052709 L NO 20052709L
- Authority
- NO
- Norway
- Prior art keywords
- nir
- chemical process
- probe
- spectrograph
- white light
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- 238000004497 NIR spectroscopy Methods 0.000 title abstract 3
- 238000001311 chemical methods and process Methods 0.000 title abstract 3
- 239000000523 sample Substances 0.000 abstract 4
- 238000004458 analytical method Methods 0.000 abstract 2
- 238000001228 spectrum Methods 0.000 abstract 2
- 238000003556 assay Methods 0.000 abstract 1
- 230000002596 correlated effect Effects 0.000 abstract 1
- 239000000835 fiber Substances 0.000 abstract 1
- 238000005259 measurement Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/359—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3563—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing solids; Preparation of samples therefor
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/84—Systems specially adapted for particular applications
- G01N21/85—Investigating moving fluids or granular solids
- G01N21/8507—Probe photometers, i.e. with optical measuring part dipped into fluid sample
Landscapes
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
En fremgangsmåte er beskrevet for å tilveiebringe raske online analyser av kjemiske sammensetninger slik som kjemiske prosesstrømmer, anvendende nær-infrarødt (NIR) spektroskopi i kombinasjon med kjemometri. I fremgangsmåten er en database tileveiebrakt for hver type av analyse som skal utføres, ved å analsyere en serie prøver anvendende standard laboratorium analytiske prosedyrer, anvendende resultatene som referanseverdier for å etablere kvantitative kalibreringsmodeller fra NIR-spektroskopi anvendende kjemometriske teknikker og ved å lagre denne informasjonen i en datamaskin database. Et NIR-spektroskopisk system er også tilveiebrakt som omfatter en transflektans eller en overføringssonde koblet via fiberoptiske kabler til en stabil hvit lyskilde og en spektrograf. Sonden settes inn i en testprøve eller kjemisk prosesstrøm som skal analyseres, et stabilt hvitt lys valgt fra et bølgelengdeområde stråles til sonden og spektrene oppnådd på spektrografen registreres. Til slutt blir de oppnådde spektrene korrelert til referansedata lagret i datamaskinen for å oppnå rask måling av den ønskede analysen.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US42397502P | 2002-11-06 | 2002-11-06 | |
PCT/CA2003/001575 WO2004042375A1 (en) | 2002-11-06 | 2003-10-15 | Nir spectroscopy method for analyzing chemical process components |
Publications (2)
Publication Number | Publication Date |
---|---|
NO20052709D0 NO20052709D0 (no) | 2005-06-06 |
NO20052709L true NO20052709L (no) | 2005-08-08 |
Family
ID=32312733
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO20052709A NO20052709L (no) | 2002-11-06 | 2005-06-06 | NIR spektroskopimetode for a analysere kjemiske prosesskomponenter |
Country Status (5)
Country | Link |
---|---|
US (1) | US7067811B2 (no) |
EP (1) | EP1563280A1 (no) |
CA (1) | CA2503610C (no) |
NO (1) | NO20052709L (no) |
WO (1) | WO2004042375A1 (no) |
Families Citing this family (62)
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US20060097173A1 (en) * | 2003-10-15 | 2006-05-11 | Sanofi-Aventis Deutschland | Method and device for the quantitative analysis of solutions and dispersions by means of near infrared spectroscopy |
US20050092941A1 (en) * | 2003-06-06 | 2005-05-05 | Aventis Pharma Deutschland Gmbh | Method and device for the quantitative analysis of solutions and dispersions by means of near infrared spectroscopy |
US7528950B2 (en) * | 2005-01-11 | 2009-05-05 | Duquesne University Of The Holy Spirit | Tunable laser-based process monitoring apparatus |
DE102005007755B4 (de) * | 2005-02-18 | 2007-10-18 | Betriebsforschungsinstitut VDEh - Institut für angewandte Forschung GmbH | Verfahren zur Analyse der Zusammensetzung einer flüssigen Metallschmelze |
CA2613873C (en) * | 2007-05-03 | 2008-10-28 | Imperial Oil Resources Limited | An improved process for recovering solvent from asphaltene containing tailings resulting from a separation process |
CA2592725C (en) * | 2007-06-26 | 2009-04-14 | Imperial Oil Resources Limited | A method for cleaning fouled vessels in the paraffinic froth treatment process |
CA2594205C (en) * | 2007-07-20 | 2009-11-24 | Imperial Oil Resources Limited | Use of a fluorocarbon polymer as a surface of a vessel or conduit used in a paraffinic froth treatment process for reducing fouling |
CA2595336C (en) * | 2007-07-31 | 2009-09-15 | Imperial Oil Resources Limited | Reducing foulant carry-over or build-up in a paraffinic froth treatment process |
CA2609419C (en) * | 2007-11-02 | 2010-12-14 | Imperial Oil Resources Limited | System and method of heat and water recovery from tailings using gas humidification/dehumidification |
CA2609859C (en) * | 2007-11-02 | 2011-08-23 | Imperial Oil Resources Limited | Recovery of high quality water from produced water arising from a thermal hydrocarbon recovery operation using vacuum technologies |
CA2610052C (en) * | 2007-11-08 | 2013-02-19 | Imperial Oil Resources Limited | System and method of recovering heat and water and generating power from bitumen mining operations |
CA2610463C (en) * | 2007-11-09 | 2012-04-24 | Imperial Oil Resources Limited | Integration of an in-situ recovery operation with a mining operation |
CA2610230C (en) * | 2007-11-13 | 2012-04-03 | Imperial Oil Resources Limited | Water integration between an in-situ recovery operation and a bitumen mining operation |
EP2232236B1 (en) * | 2007-12-21 | 2019-12-18 | Medico Kemiske Laboratorium ApS | Monitoring lubricant oil condition and/or quality, on-line or at-line, based on chemometric data analysis of flourescence and/or near infrared spectra |
US8357291B2 (en) * | 2008-02-11 | 2013-01-22 | Exxonmobil Upstream Research Company | Upgrading bitumen in a paraffinic froth treatment process |
US20090200210A1 (en) * | 2008-02-11 | 2009-08-13 | Hommema Scott E | Method Of Removing Solids From Bitumen Froth |
US8592351B2 (en) | 2008-03-20 | 2013-11-26 | Exxonmobil Upstream Research Company | Enhancing emulsion stability |
US8252170B2 (en) | 2008-06-27 | 2012-08-28 | Exxonmobil Upstream Research Company | Optimizing feed mixer performance in a paraffinic froth treatment process |
US8017910B2 (en) * | 2008-10-20 | 2011-09-13 | Nalco Company | Method for predicting hydrocarbon process stream stability using near infrared spectra |
CA2644821C (en) * | 2008-11-26 | 2013-02-19 | Imperial Oil Resources Limited | A method for using native bitumen markers to improve solvent-assisted bitumen extraction |
CA2650750C (en) | 2009-01-23 | 2013-08-27 | Imperial Oil Resources Limited | Method and system for determining particle size distribution and filterable solids in a bitumen-containing fluid |
CA2672004C (en) | 2009-07-14 | 2012-03-27 | Imperial Oil Resources Limited | Feed delivery system for a solid-liquid separation vessel |
US9222929B2 (en) | 2009-12-07 | 2015-12-29 | Exxonmobil Upstream Research Company | Solvent surveillance in solvent-based heavy oil recovery processes |
CA2693640C (en) | 2010-02-17 | 2013-10-01 | Exxonmobil Upstream Research Company | Solvent separation in a solvent-dominated recovery process |
CA2696638C (en) | 2010-03-16 | 2012-08-07 | Exxonmobil Upstream Research Company | Use of a solvent-external emulsion for in situ oil recovery |
CA2705643C (en) | 2010-05-26 | 2016-11-01 | Imperial Oil Resources Limited | Optimization of solvent-dominated recovery |
CN101915745B (zh) * | 2010-07-20 | 2012-02-29 | 浙江省交通工程建设集团有限公司 | 一种改性沥青中sbs改性剂含量的红外光谱分析方法 |
US8248612B2 (en) * | 2010-07-26 | 2012-08-21 | Ut-Batelle, Llc | Oxygen concentration sensors and methods of rapidly measuring the concentration of oxygen in fluids |
CA2714842C (en) | 2010-09-22 | 2012-05-29 | Imperial Oil Resources Limited | Controlling bitumen quality in solvent-assisted bitumen extraction |
CA2734811C (en) | 2011-03-29 | 2012-11-20 | Imperial Oil Resources Limited | Feedwell system for a separation vessel |
CA2738560C (en) | 2011-05-03 | 2014-07-08 | Imperial Oil Resources Limited | Enhancing fine capture in paraffinic froth treatment process |
ITMI20111262A1 (it) * | 2011-07-06 | 2013-01-07 | Eni Spa | "metodo di monitoraggio delle operazioni di lavaggio dei depositi asfaltenici nei pozzi petroliferi mediante spettrometria nir" |
CA3075552C (en) * | 2011-07-07 | 2021-12-07 | Cidra Corporate Services Inc. | Spectroscopic analysis of oil sands ore face for real time ore blend management |
CA2849326A1 (en) * | 2011-09-23 | 2013-03-28 | Dow Agrosciences Llc | Chemometrics for near infrared spectral analysis |
CA2783819C (en) | 2011-11-08 | 2014-04-29 | Imperial Oil Resources Limited | Dewatering oil sand tailings |
WO2013082248A1 (en) * | 2011-11-29 | 2013-06-06 | Cidra Corporate Services Inc. | Laser based system for bitumen content determination, e.g., using discrete wavelength spectroscopic analysis |
DE102012100794B3 (de) * | 2012-01-31 | 2013-02-28 | Airbus Operations Gmbh | Vorrichtung und Verfahren zum Erfassen von Kontaminationen in einem Hydrauliksystem |
US9041933B2 (en) * | 2012-03-01 | 2015-05-26 | Schlumberger Technology Corporation | System and method for characterizing crude oil fractions |
CA2780169C (en) | 2012-06-08 | 2019-08-27 | The Governors Of The University Of Alberta | Hyperspectral imaging for ore froth processing |
DE112013004743T5 (de) | 2012-09-26 | 2015-09-24 | Panalytical Inc. | Multi-Sensoranalyse eines komplexen geologischen Materials |
US10668408B2 (en) | 2012-11-30 | 2020-06-02 | Suncor Energy Inc | Measurement and control of bitumen-containing process streams |
CN103868882A (zh) * | 2012-12-13 | 2014-06-18 | 中国石油化工股份有限公司 | 测定沥青中各组分含量的方法 |
US9360425B2 (en) | 2013-05-02 | 2016-06-07 | Baker Hughes Incorporated | Method for characterizing the stability of foulants and/or efficacy of foulant inhibitors within petroleum-based fluids |
CN103868600B (zh) * | 2014-02-26 | 2016-05-04 | 燕山大学 | 沥青路面摊铺温度在线测量装置 |
WO2015176007A1 (en) * | 2014-05-15 | 2015-11-19 | Flint Hills Resources, Lp | Methods for reducing the precipitation propensity of asphaltenes in blended crude oils |
GB2528487A (en) * | 2014-07-23 | 2016-01-27 | Airbus Operations Ltd | Apparatus and method for testing materials |
GB2528488A (en) | 2014-07-23 | 2016-01-27 | Airbus Operations Ltd | Method and apparatus for testing materials |
CN104198429A (zh) * | 2014-09-12 | 2014-12-10 | 广西大学 | 红外色谱和凝胶渗透色谱联合分析鉴别沥青的方法 |
US9678002B2 (en) * | 2014-10-29 | 2017-06-13 | Chevron U.S.A. Inc. | Method and system for NIR spectroscopy of mixtures to evaluate composition of components of the mixtures |
US10641758B2 (en) | 2015-09-01 | 2020-05-05 | Exxonmobil Upstream Research Company | Apparatus, systems, and methods for enhancing hydrocarbon extraction and techniques related thereto |
CN105699304B (zh) * | 2016-01-28 | 2018-08-14 | 深圳市芭田生态工程股份有限公司 | 一种获得光谱信息所代表的物质信息的方法 |
CN105606548B (zh) * | 2016-01-28 | 2018-06-19 | 深圳市芭田生态工程股份有限公司 | 一种数据库与运算服务器的工作方法 |
US20170314383A1 (en) * | 2016-04-28 | 2017-11-02 | New Mexico Tech Research Foundation | Situ method of analyzing mixed-phase flow compositions |
CA3123815A1 (en) | 2016-10-19 | 2018-04-19 | Fort Hills Energy L.P. | Near infrared (nir) monitoring in paraffinic froth treatment (pft) operations |
CA3014968A1 (en) | 2017-08-18 | 2019-02-18 | Canadian Natural Resources Limited | High temperature paraffinic froth treatment process |
CN108303393B (zh) * | 2018-01-31 | 2020-10-27 | 长安大学 | 一种测量sbs改性沥青中sbs改性剂含量的方法 |
CN111936844B (zh) * | 2018-03-20 | 2024-04-09 | Hte高通量实验公司 | 分析过程工艺料流的方法 |
CN108663338A (zh) * | 2018-05-09 | 2018-10-16 | 山东蓝星东大有限公司 | 在线监测聚合物多元醇产品质量的方法 |
EP3711852A1 (de) | 2019-03-21 | 2020-09-23 | Covestro Deutschland AG | Verfahren und vorrichtung zur quantitativen überwachung der zusammensetzung einer oligomer-/monomermischung |
CA3040649C (en) | 2019-04-18 | 2021-03-30 | Fort Hills Energy L.P. | Monitoring of residual metals in paraffinic froth treatment operations and process control |
CN110108865A (zh) * | 2019-04-28 | 2019-08-09 | 河海大学 | 一种废机油对沥青材料的改性机理研究方法 |
EP4290219A1 (en) | 2022-06-09 | 2023-12-13 | Lietuvos Agrariniu Ir Misku Mokslu Centras | Determination of the composition of biogas production by-product using a near-infrared spectroscopy method |
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JPS62110135A (ja) | 1985-11-08 | 1987-05-21 | Cosmo Co Ltd | アスフアルテン濃度定量方法および装置 |
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US5742064A (en) | 1996-04-24 | 1998-04-21 | Infante; David A. | System for detecting impurities contained in a flowing petroleum product |
US6281489B1 (en) * | 1997-05-02 | 2001-08-28 | Baker Hughes Incorporated | Monitoring of downhole parameters and tools utilizing fiber optics |
US6087662A (en) * | 1998-05-22 | 2000-07-11 | Marathon Ashland Petroleum Llc | Process for analysis of asphaltene content in hydrocarbon mixtures by middle infrared spectroscopy |
US6300633B1 (en) * | 1998-07-06 | 2001-10-09 | Bayer Corporation | In-line method for determining the residue content of an isocyanate and apparatus useful therefor |
US6507401B1 (en) * | 1999-12-02 | 2003-01-14 | Aps Technology, Inc. | Apparatus and method for analyzing fluids |
US6501072B2 (en) * | 2001-01-29 | 2002-12-31 | Schlumberger Technology Corporation | Methods and apparatus for determining precipitation onset pressure of asphaltenes |
-
2003
- 2003-10-15 WO PCT/CA2003/001575 patent/WO2004042375A1/en active Application Filing
- 2003-10-15 CA CA2503610A patent/CA2503610C/en not_active Expired - Lifetime
- 2003-10-15 EP EP03769100A patent/EP1563280A1/en not_active Withdrawn
- 2003-10-17 US US10/686,725 patent/US7067811B2/en not_active Expired - Lifetime
-
2005
- 2005-06-06 NO NO20052709A patent/NO20052709L/no not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
EP1563280A1 (en) | 2005-08-17 |
US20040084623A1 (en) | 2004-05-06 |
US7067811B2 (en) | 2006-06-27 |
CA2503610C (en) | 2011-08-02 |
NO20052709D0 (no) | 2005-06-06 |
CA2503610A1 (en) | 2004-05-21 |
WO2004042375A1 (en) | 2004-05-21 |
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