NO168810B - PROCEDURE AND DEVICE FOR THE CREATION OF MIXED WASTE, AS HOUSEHOLD WASTE OR FRACTIONS THEREOF, FOR THE RECYCLING OF PLASTIC FILM MATERIALS - Google Patents
PROCEDURE AND DEVICE FOR THE CREATION OF MIXED WASTE, AS HOUSEHOLD WASTE OR FRACTIONS THEREOF, FOR THE RECYCLING OF PLASTIC FILM MATERIALS Download PDFInfo
- Publication number
- NO168810B NO168810B NO874940A NO874940A NO168810B NO 168810 B NO168810 B NO 168810B NO 874940 A NO874940 A NO 874940A NO 874940 A NO874940 A NO 874940A NO 168810 B NO168810 B NO 168810B
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- Prior art keywords
- liquid
- flow
- plastic
- flotation
- residue
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 32
- 239000002985 plastic film Substances 0.000 title claims description 32
- 229920006255 plastic film Polymers 0.000 title claims description 32
- 239000000463 material Substances 0.000 title claims description 19
- 238000004064 recycling Methods 0.000 title claims description 17
- 239000010812 mixed waste Substances 0.000 title claims description 6
- 239000010791 domestic waste Substances 0.000 title description 2
- 239000007788 liquid Substances 0.000 claims description 39
- 239000004033 plastic Substances 0.000 claims description 36
- 229920003023 plastic Polymers 0.000 claims description 36
- 238000005188 flotation Methods 0.000 claims description 31
- 238000000926 separation method Methods 0.000 claims description 20
- 239000011888 foil Substances 0.000 claims description 15
- 239000000126 substance Substances 0.000 claims description 13
- 230000005484 gravity Effects 0.000 claims description 12
- 238000012216 screening Methods 0.000 claims description 12
- 230000008021 deposition Effects 0.000 claims description 11
- 239000012071 phase Substances 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 238000011109 contamination Methods 0.000 claims description 6
- 229920006327 polystyrene foam Polymers 0.000 claims description 6
- 239000002023 wood Substances 0.000 claims description 6
- 239000000356 contaminant Substances 0.000 claims description 5
- 239000007791 liquid phase Substances 0.000 claims description 5
- 239000002184 metal Substances 0.000 claims description 5
- 239000010813 municipal solid waste Substances 0.000 claims description 5
- 239000006260 foam Substances 0.000 claims description 4
- 238000004062 sedimentation Methods 0.000 claims description 4
- 239000004575 stone Substances 0.000 claims description 4
- 230000000284 resting effect Effects 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 239000000725 suspension Substances 0.000 claims description 3
- 239000002562 thickening agent Substances 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 238000000605 extraction Methods 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 22
- 239000000835 fiber Substances 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 239000002699 waste material Substances 0.000 description 5
- 238000011084 recovery Methods 0.000 description 3
- 238000005352 clarification Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 210000004905 finger nail Anatomy 0.000 description 2
- 230000009969 flowable effect Effects 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 239000013502 plastic waste Substances 0.000 description 2
- 238000007873 sieving Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 229920000426 Microplastic Polymers 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 239000010893 paper waste Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 239000002984 plastic foam Substances 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B9/00—General arrangement of separating plant, e.g. flow sheets
- B03B9/06—General arrangement of separating plant, e.g. flow sheets specially adapted for refuse
- B03B9/061—General arrangement of separating plant, e.g. flow sheets specially adapted for refuse the refuse being industrial
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
- B29B17/02—Separating plastics from other materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
- B29B17/02—Separating plastics from other materials
- B29B2017/0203—Separating plastics from plastics
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
- B29B17/02—Separating plastics from other materials
- B29B2017/0213—Specific separating techniques
- B29B2017/0217—Mechanical separating techniques; devices therefor
- B29B2017/0251—Hydropulping for converting the material under the influence of water into a slurry, e.g. for separating laminated plastic from paper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2025/00—Use of polymers of vinyl-aromatic compounds or derivatives thereof as moulding material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2027/00—Use of polyvinylhalogenides or derivatives thereof as moulding material
- B29K2027/06—PVC, i.e. polyvinylchloride
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
- B29K2105/04—Condition, form or state of moulded material or of the material to be shaped cellular or porous
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
- B29K2105/06—Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts
- B29K2105/065—Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts containing impurities
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2705/00—Use of metals, their alloys or their compounds, for preformed parts, e.g. for inserts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2709/00—Use of inorganic materials not provided for in groups B29K2703/00 - B29K2707/00, for preformed parts, e.g. for inserts
- B29K2709/08—Glass
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2711/00—Use of natural products or their composites, not provided for in groups B29K2601/00 - B29K2709/00, for preformed parts, e.g. for inserts
- B29K2711/12—Paper, e.g. cardboard
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
- B29K2711/00—Use of natural products or their composites, not provided for in groups B29K2601/00 - B29K2709/00, for preformed parts, e.g. for inserts
- B29K2711/14—Wood, e.g. woodboard or fibreboard
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
- B29L2007/00—Flat articles, e.g. films or sheets
- B29L2007/008—Wide strips, e.g. films, webs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/52—Mechanical processing of waste for the recovery of materials, e.g. crushing, shredding, separation or disassembly
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/62—Plastics recycling; Rubber recycling
Landscapes
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Mechanical Engineering (AREA)
- Separation Of Solids By Using Liquids Or Pneumatic Power (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
Description
Foreliggende oppfinnelse vedrører en fremgangsmåte og en innretning for oppredning av blandede avfall, som søppel eller fraksjoner derav, for adskilt gjenvinning av på den ene side papir og på den andre siden plastfoliematerialer, spesielt i resirkuleringsanlegg. The present invention relates to a method and a device for sorting out mixed waste, such as rubbish or fractions thereof, for separate recycling of on the one hand paper and on the other hand plastic foil materials, especially in recycling facilities.
Det dreier seg spesielt om våt adskillelse av papir og plastfolier fra blandede papir/plast-avfall, f.eks. fra et resirkuleringsanlegg for søppel. This particularly concerns wet separation of paper and plastic films from mixed paper/plastic waste, e.g. from a waste recycling facility.
I husholdningssøppel befinner det seg, avhengig av den geografisk plasseringen, 30-40$ papir samt 6-12$ plast-avfall. Begge materialer kan ved tilfredsstillende renhet gjenanvendes uten problemer i industrien. In household waste, depending on the geographical location, there is 30-40$ of paper and 6-12$ of plastic waste. Both materials can be reused without problems in industry if they are of satisfactory purity.
I resirkuleringsanlegg for søppel er tørre separasjons-fremgangsmåter, f.eks. luftsikting eller trommelsikting kjent for å utsortere papir og plast som adskilte fraksjoner. Fraksjonene kan deretter bearbeides i spesielle opprednings-prosesser til fiberstoff hhv. plastgranulat. En ulempe er de høye investerings- og driftskostnadene og til dels en dårlig adskillelsesskarphet for slike tørre separasjonsfremgangs-måter. Forurensningsgrader for fraksjonene på inntil 30$ eller høyere er kjente. In waste recycling facilities, dry separation methods, e.g. air sieving or drum sieving known to sort out paper and plastic as separate fractions. The fractions can then be processed in special preparation processes into fiber material or plastic granules. A disadvantage is the high investment and operating costs and partly a poor separation sharpness for such dry separation methods. Degrees of pollution for the fractions of up to 30$ or higher are known.
Dersom papiret tilbakevinnes i et resirkuleringsanlegg så er for det meste også et masseløsersystem og et klaringsanlegg til stede i den våte oppredningsprosessen. I denne prosess-delen utskilles papirfremmede bestanddeler, bl.a. også plastfolier, som uønsket materiale og kastes. Følgelig besto den oppgaven å også gjøre denne delen gjenanvendelig. If the paper is recovered in a recycling plant, then a pulp separation system and a clarification plant are also mostly present in the wet sorting process. In this process part, components foreign to paper are separated, i.a. also plastic foils, as unwanted material and thrown away. Consequently, the task consisted of also making this part reusable.
Til løsning av denne oppgaven foreslås ifølge oppfinnelsen, ved utvidelse av våt-oppløsningssystemet å adskille og forrense begge de verdifulle stoffene papir og plastfolier, slik at disse kan tilføres direkte til den videre oppredningsprosessen. To solve this problem, according to the invention, by expanding the wet-dissolving system, it is proposed to separate and pre-clean both the valuable substances paper and plastic foils, so that these can be supplied directly to the further straightening process.
Foreliggende oppfinnelse tilveiebringer en fremgangsmåte for oppredning av blandede avfall, som søppel eller fraksjoner derav, for gjenvinning av plast, spesielt i resirkuleringsanlegg, hvorved en forsortert fraksjon inneholdende plastfolier behandles i en masseløser (pulper), den oppnådde, spesielt papir-holdige suspensjonen fjernes ved hjelp av sikter, og forurensningsfasen, som utgjør sikteresten, inneholdende plastfolie avleires. Fremgangsmåten er kjennetegnet ved at det for utvinning av plastandelen samles en sikterest av forurensningsfasen, sikteresten føres ut fra masseløseren, findeles etter fjernelse av væske og deretter fraskilles plastfolieandelen fra en flytende fase. The present invention provides a method for the sorting of mixed waste, such as rubbish or fractions thereof, for the recycling of plastics, especially in recycling facilities, whereby a pre-sorted fraction containing plastic foils is processed in a pulping machine (pulpers), the obtained, especially paper-containing suspension is removed by using sieves, and the contamination phase, which constitutes the sieve residue, containing plastic foil is deposited. The method is characterized by the fact that for the recovery of the plastic part, a screening residue is collected from the contamination phase, the screening residue is taken out of the mass dissolver, crushed after removal of liquid and then the plastic foil part is separated from a liquid phase.
Ifølge et fremdeles ikke offentliggjort forslag fra søkeren fjernes fordelaktig væske fra siktresten som er tatt ut av masseløseren i en hulltrommel, hvorved denne siktetrommelen spesielt delvis kan dykke ned i et bad av suspensjonsvæske. Fordelaktig er hulltrommelen utført som trinntrommel med volum som avtar i transportretningen og sentralutløp og oppviser spesielt en innerspiral og/eller pumpelommer, slik at sikteresten ikke bare føres videre i hulltrommelen, men også løpende løses opp og blandes, slik at små andeler, som steiner, glass- eller metalldeler, hardplastdeler og fremdeles ikke fraskilte papirfibre kan tre ut av hulltrommelen gjennom hullene. Hulltrommelen kan også være tildannet som konustrommel med innsnevring i transportretningen; videre kan aksen i hulltrommelen forløpe stigende i transportretningen. According to a still unpublished proposal from the applicant, liquid is advantageously removed from the screening residue that has been taken out by the pulp solver in a hole drum, whereby this screening drum can in particular partially dive into a bath of suspension liquid. Advantageously, the hole drum is designed as a stepped drum with a volume that decreases in the direction of transport and a central outlet and in particular has an inner spiral and/or pump pockets, so that the screening residue is not only carried forward in the hole drum, but also continuously dissolved and mixed, so that small proportions, such as stones, glass or metal parts, hard plastic parts and still unseparated paper fibers can exit the punching drum through the holes. The hole drum can also be formed as a cone drum with a narrowing in the transport direction; furthermore, the axis in the hole drum can run upwards in the direction of transport.
Fjernelse av væske fra siktresten kan foregå i flere trinn; følgelig kan f.eks. det materialet som er brakt ut av hulltrommelen deretter utpresses og fortettes i en presse, spesielt en skruetransportør. Removal of liquid from the sieve residue can take place in several steps; consequently, e.g. the material brought out of the hole drum is then extruded and densified in a press, especially a screw conveyor.
Deretter underkastes materialet hvorfra vannet er fjernet en deling, som minst har ett trinn. Fremfor alt har det vist seg hensiktsmessig først å findele materialet i i det vesentlige tørr tilstand til håndflatestørrelse, f.eks. i en vanlig findeler, deretter oppslemme i et beger med prosessvann under bevegelse, hvorved vedhengende forurensningsdeler fraløses og tunge stoffer synker til bunnen av begeret, samt at materialet på overflaten av væske fjernes og underkastes en fortrinnsvis våt findeling til ca. fingerneglstørrelse. The material from which the water has been removed is then subjected to a division, which has at least one stage. Above all, it has proven appropriate to first finely chop the material in an essentially dry state to the size of the palm of your hand, e.g. in a regular finer, then slurried in a beaker with process water while moving, whereby adhering particles of contamination are released and heavy substances sink to the bottom of the beaker, and that the material on the surface of the liquid is removed and subjected to a preferably wet finer division to approx. fingernail size.
Deretter fraskilles fordelaktig de lette andelene av dette materialet, dvs. stoffer som lett flyter opp, som tre eller polystyrenskum, fra fraksjonen som skal utvinnes, dvs. plastfolierester, hvis tetthet bare er lite mindre enn 1, dvs. at de flyter i vann med bare liten oppdrift. Dette foregår i et tyngdekraft-flotasjonsbeger, hvori en fallende strømning opprettholdes, hastigheten av denne strømningen er større enn oppflytningshastigheten for plastfolierestene, slik at disse medføres av strømningen, og fortrinnsvis over et bunnuttak, trer ut av beholderen sammen med prosessvann, mens de lette delene flyter opp og kan fjernes. The light parts of this material, i.e. substances that float easily, such as wood or polystyrene foam, are then advantageously separated from the fraction to be recovered, i.e. plastic film residues, whose density is only slightly less than 1, i.e. that they float in water with just a little buoyancy. This takes place in a gravity flotation cup, in which a falling flow is maintained, the speed of this flow is greater than the buoyancy speed of the plastic film residues, so that these are carried by the flow, and preferably via a bottom outlet, exit the container together with process water, while the light parts floats up and can be removed.
Et tilsvarende trekk ved fremgangsmåten ifølge oppfinnelsen er at den avvannede og findelte sikteresten, spesielt etter fraskillelse av tungstoffer, samt fortrinnsvis etter en ytterligere findeling, i et tyngdekraft-flotasjonsbeger befris for flytbare, lette andeler, som tre eller skumplast, spesielt polystyrenskum, med unntak av plastfolierester. A corresponding feature of the method according to the invention is that the dewatered and finely divided screening residue, especially after separation of heavy substances, as well as preferably after a further fine division, in a gravity flotation beaker is freed from flowable, light parts, such as wood or foam plastic, especially polystyrene foam, with the exception of plastic film residues.
For ytterligere rensing velges deretter den motsatte fremgangsmåten, nemlig en flotasjon av plastfolierester i prosessvann. Dette tjener fremfor alt til en endelig adskillelse av stoffer som synker og flyter, og spesielt til adskillelse av rester er vevde materialer, spesielt vevde rester av kunststoffvev, idet det har vist seg at disse er en tilsetning som for etterfølgende oppredning av plastfolierestene, hvorved vanligvis granulater oppnås, utgjør en ytterst uheldig og kvalitetsreduserende forurensning. For further purification, the opposite method is then chosen, namely a flotation of plastic film residues in process water. This serves above all for a final separation of substances that sink and float, and in particular for the separation of remnants of woven materials, especially woven remnants of plastic fabric, as it has been shown that these are an addition for the subsequent spreading of the plastic film remnants, whereby usually granules are obtained, constitute an extremely unfortunate and quality-reducing pollution.
Disse vevde restene viser ingen flytning som plastfolierestene, men medtas lett i det strømmende prosessvannet. These woven residues do not flow like the plastic film residues, but are easily included in the flowing process water.
Ifølge oppfinnelsen er det følgelig videre anordnet slik at den avvannede og findelte sikteresten behandles i et strøm-nings-f Iotas j onsbeger , hvori plastfolierestene stiger til overflaten av væsken under innvirkning av strømningen, spesielt spyles oppover, og fjernes fra overflaten. According to the invention, it is therefore further arranged so that the dewatered and finely divided sifting residue is processed in a flow-flow Iotas ion beaker, in which the plastic foil residues rise to the surface of the liquid under the influence of the flow, are especially flushed upwards, and are removed from the surface.
Dette strømnings-fIotasjonsbegeret er fordelaktig, i det minste strømningsmessig, oppdelt i en oppflytningssone med sedimentasjonstrakt for frasugning av raskt synkbare forurensninger og en hvile- hhv. frastrømningssone, hvorved det i oppflytningssonen opprettholdes en i det minste i det vesentlige horisontalt rettet væskestrømning, hvormed plastfolierestene stiger til væskeoverflaten. I hvile- hhv. frastrømningssonen omdirigeres strømning, fortrinnsvis 1 fallende retning, og medtar de vevde stoffene og restene av disse, hvorved den flytende fasen fra begge sonene fjernes, fortrinnsvis ved hjelp av bunnutløp. De oppflytende plastfolierestene fjernes fra væskeoverflaten og føres som rent produkt inn i plast-tilbakevinningen. This flow-flotation cup is advantageously, at least in terms of flow, divided into a flotation zone with a sedimentation funnel for extracting rapidly sinking contaminants and a resting or outflow zone, whereby an at least substantially horizontally directed liquid flow is maintained in the buoyancy zone, whereby the plastic film residues rise to the liquid surface. At rest - or from the outflow zone, flow is redirected, preferably in a downward direction, and includes the woven fabrics and their residues, whereby the liquid phase from both zones is removed, preferably by means of a bottom outlet. The floating plastic film residues are removed from the liquid surface and fed as a clean product into the plastic recovery.
Strømningshastigheten og retningen i hvile- hhv. avsetningssonen innstilles så lavt at de oppflytende plastfolierestene ikke medtas videre, men forblir på væskeoverflaten. The flow speed and direction at rest - respectively the deposition zone is set so low that the floating plastic film residues are not carried further, but remain on the liquid surface.
Oppfinnelsen skal i det følgende beskrives ved hjelp av et utførelseseksempel under henvisning til tegningen, hvori den for utvinning av plastfolierester rettede delen av en opparbeiding ifølge oppfinnelsen, fra på forhånd sortert papir/plastfraksjoner fra et søppeloppredningsanlegg, er angitt skjematisk. In the following, the invention will be described with the help of an embodiment with reference to the drawing, in which the part of a processing according to the invention, from pre-sorted paper/plastic fractions from a waste processing plant, aimed at extracting plastic film residues, is indicated schematically.
Den vanligvis til baller pressede papir/plastfraksjonen oppløses i en pulper, betegnet masseløser 1, med prosessvann som føres i kretsløp. Den oppnådde papirmassen fjernes via hullsikten og går til papirgjenvinning; plastfoliene bringes sammen med øvrige forurensninger som sikterest, etter som de dannes, ut fra pulperen 1, spyles spesielt ut, hvorved det hensiktsmessig etter vanntilsatsen foretas en kort massedan-nelse, og føres ved hjelp av transportspiraler inn i en trinntrommel 2. Trinntrommelen 2 er en vanlig hulltrommel, gjennom hvis hull på den ene siden tunge stoffer, som glass, metall, steiner osv., og på den andre siden fiber- og flytestoffer som prosessvann inneholdende medført papir, trer ut og samles i en under trinntrommelen 2 anordnet opp-fangningsbeholder 3. Herved kan væskenivået i oppfangnings-beholderen 3 være valgt på en slik måte at trinntrommelen delvis dykker ned i dette; på denne måten oppnås en god utvaskingseffekt. Vannet tilbakeføres fra oppfangningstanken 3 som prosessvann i pulperen 1, de tunge stoffene bringes ut ved hjelp av en skruetransportør 4 og samles som avfall. Trinntrommelen 2 oppviser et sentralt utløp og det utførte materialet som inneholder plastfoliene underkastes i en skruepresse 5 en vannfjernelse, og deles i en foroppdeler 6 til ca. håndflatestørrelse. Det på forhånd oppdelte materialet går deretter inn i et (flotasjons/avsetnings) adskil-lelsesbeger 7, hvor større synkbare stoffer fraskilles. Dette er spesielt metalldeler, ikke-findelte tekstiler, PVC og andre synkbare hardplastdeler, lær osv. For å forbedre adskillelsen kan det her også anvendes rørere eller andre innretninger som gir turbulens. Andelene som synker bringes ut ved hjelp av bunnåpning 8; de oppflytende delene, hvortil plastfolierestene hører, tas av fra væskeoverflaten ved hjelp av en åreinnretning 9, og når inn i en f infordelingsinn-retning 10, som fortrinnsvis er tildannet som en våt mølle, i denne findeles materialet til omtrent fingerneglstørrelse. Det findelte materialet går inn i et tyngdekraft-flotasjonsbeger 11, som tilføres findelt materiale og prosessvann ovenfra. Transporten av det findelte materialet til tyngde-kraf t-f Iotas jonsbegeret 11 foregår ved hjelp av en åreskrue 12, hvori forurensningsdelene slås løs. The paper/plastic fraction, which is usually pressed into balls, is dissolved in a pulper, called pulp dissolver 1, with process water that is circulated. The paper pulp obtained is removed via the hole sieve and goes to paper recycling; the plastic foils are brought together with other contaminants as sifted residue, as they are formed, from the pulper 1, rinsed out in particular, whereby a brief mass formation is carried out appropriately after the addition of water, and fed by means of transport spirals into a step drum 2. The step drum 2 is an ordinary perforated drum, through whose holes on the one hand heavy substances, such as glass, metal, stones, etc., and on the other hand fibrous and floating substances such as process water containing entrained paper, exit and are collected in a device arranged below the step drum 2 collection container 3. Hereby, the liquid level in the collection container 3 can be selected in such a way that the step drum partially dives into it; in this way, a good washing-out effect is achieved. The water is returned from the collection tank 3 as process water in the pulper 1, the heavy substances are brought out by means of a screw conveyor 4 and collected as waste. The step drum 2 has a central outlet and the processed material containing the plastic films is subjected to water removal in a screw press 5, and divided in a pre-divider 6 to approx. palm size. The previously divided material then enters a (flotation/deposition) separation cup 7, where larger sinkable substances are separated. These are especially metal parts, non-finely divided textiles, PVC and other sinkable hard plastic parts, leather, etc. To improve the separation, stirrers or other devices that produce turbulence can also be used here. The portions that sink are brought out by means of bottom opening 8; the floating parts, to which the plastic film residues belong, are removed from the liquid surface with the help of an oar device 9, and when they enter a fine distribution device 10, which is preferably designed as a wet mill, in this the material is crushed to approximately the size of a fingernail. The finely divided material enters a gravity flotation beaker 11, which is supplied with finely divided material and process water from above. The transport of the finely divided material to gravity-force t-f Iota's ion beaker 11 takes place with the aid of an auger 12, in which the contamination parts are loosened.
Materialet føres i tyngdekraft-fIotasjonsbegeret 11, sammen med prosessvann, i tyngdekraftens retning nedover og føres ut sentralt i bunnen av begeret; lette andeler som tre og plastskum, f.eks. polystyrenskum, stiger opp og fjernes fra væskeoverflaten. The material is fed into the gravity flotation beaker 11, together with process water, in the direction of gravity downwards and fed out centrally at the bottom of the beaker; light parts such as wood and plastic foam, e.g. polystyrene foam, rises and is removed from the liquid surface.
Deretter pumpes prosessvannet med de medførte plastfolierestene ved hjelp av en pumpe 13 inn i et strømnings-f lota-sjonsbeger 14 gjennom et innløp 15 på siden, hvorved det dannes en horisontal strømning. En skillevegg 16 i strøm-nings-f Iotas jonsbegeret 14 tjener på den ene siden til å omdirigere strømningen og på den andre siden til deling i en fIotasjonssone med sedimentasjonstrakt 17, og en hvile- hhv. avsetningssone 18. De av væskestrømmen medførte plastfolierestene flyter opp; prosessvannet som fremdeles inneholder flytstoffer og forurensninger pumpes av gjennom et bunnutløp 19. En del av prosessvannet føres bort fra sedimentasjons-trakten i oppflytningssonen ved hjelp av rennen 22, og tilføres sammen med den andre delen av væskefasen til buesikten 24. The process water with the entrained plastic film residues is then pumped by means of a pump 13 into a flow-flotation cup 14 through an inlet 15 on the side, whereby a horizontal flow is formed. A dividing wall 16 in the flow-f Iotas ion cup 14 serves on the one hand to redirect the flow and on the other side to divide into a flotation zone with sedimentation funnel 17, and a resting or deposition zone 18. The plastic film residues carried by the liquid stream float up; the process water, which still contains liquids and contaminants, is pumped off through a bottom outlet 19. Part of the process water is led away from the sedimentation funnel in the upwelling zone by means of chute 22, and is supplied together with the other part of the liquid phase to the arch screen 24.
De oppflytende plastfolierestene transporteres fra oppflytningssonen, hvori strømningen er rettet langs væske-overf laten, evt. med understøttelse ved hjelp av prosessvann-stråler fra en stråleinnretning 20 ved væskeoverflaten, inn i hvilesonen, og fjernes der ved hjelp av en åreutføring 21. Plastfolierestene er nå praktisk talt frie for forurensninger og tilføres til et vanlig gjenvinningsanlegg, hvor de vanligvis bearbeides til et plastgranulat. Det oppnås renhetsgrader på over 97$. The floating plastic foil residues are transported from the floating zone, in which the flow is directed along the liquid surface, possibly with support using process water jets from a jet device 20 at the liquid surface, into the rest zone, and are removed there using a vein outlet 21. The plastic foil residues are now practically free of contaminants and fed to a regular recycling plant, where they are usually processed into a plastic granulate. Purities of over 97$ are achieved.
I hvile- og avsetningssonen 18 blir strømningen som opp-rinnelig er rettet langs væskeoverflaten omdirigert i retning nedover; strømningen medtar dermed alle flytende og synkbare andeler, spesielt tekstilfibrer og vevde rester av kunststoffvev, nedover til utløp 19; den flytende fasen pumpes ved hjelp av en pumpe 23 til en buesikt 26, og befris der for faststoffene. De faste stoffene går sammen med de fra bunnutløpet 18 i adskillelsesbegeret 7, og de som er fjernet fra overflaten i tyngdekraft-fIotasjonsbegeret 11 til en skruepresse 25, og føres etter fortetning og fjernelse av vann bort som avfallsfraksjon. In the rest and deposition zone 18, the flow which is originally directed along the liquid surface is redirected in a downward direction; the flow thus carries all floating and sinkable parts, especially textile fibers and woven remnants of plastic fabric, downwards to outlet 19; the liquid phase is pumped with the aid of a pump 23 to an arc sieve 26, and is then freed from the solids. The solids go together with those from the bottom outlet 18 in the separation beaker 7, and those removed from the surface in the gravity flotation beaker 11 to a screw press 25, and after densification and removal of water are removed as waste fraction.
Prosessvannet fra buesikten 24 ledes via en pumpe 26 inn i en samlebeholder 27 og tilbakeføres der på den ene siden til våtmøllen 10, og på den andre siden til tyngdekraft-flota-sjonsbegeret 11. The process water from the bow screen 24 is led via a pump 26 into a collecting container 27 and is returned there on one side to the wet mill 10, and on the other side to the gravity flotation cup 11.
Prosessvannet fra fiberoppredningen, skruepressen 5, adskillelsesbegeret 7, åreskruen 12 og plastoppredningsprosesen går inn i et klaringsanlegg med slamavvanning og tilbakeføres i klargjort tilstand til masseløser 1, til våtmølle 10, til stråledyseinnretning 20, til plastoppredningsprosessen og til fiberoppredningsprosessen. The process water from the fiber preparation, the screw press 5, the separation cup 7, the auger 12 and the plastic preparation process enters a clarification plant with sludge dewatering and is returned in a prepared state to the pulp dissolver 1, to the wet mill 10, to the jet nozzle device 20, to the plastic preparation process and to the fiber preparation process.
I flytskjemaet gjenkjennes videre vanlige, ikke nærmere omtalte vanlige transportinnretninger, som pumper, bånd- og skruetransportører, samt sluser, ventiler og regulerings-innretninger. The flowchart also recognizes common, not mentioned in detail, common transport devices, such as pumps, belt and screw conveyors, as well as sluices, valves and control devices.
Oppfinnelsen omfatter videre en innretning for oppredning av blandede avfall, som søppel eller fraksjoner derav, for adskilt gjenvinning av på den ene siden papir og på den andre siden plastfoliematerialer, spesielt i resirkuleringsanlegg, kjennetegnet ved at den omfatter en masseløser (pulper) for behandling av en forsortert fraksjon inneholdende papir og plastfolier, en væskefjernelsesinnretning, spesielt en hulltrommel, for sikteresten som bringes ut av masseløseren, en oppdelingsinnretning, evt. med forkoplet fortetter, for filterresten som er behandlet i væskefjernelsesinnretningen, samt minst en faststoff/væske-adskillelsesinnretning, spesielt en flotasjonsbeholder, for adskillelse av plastfolierestene som øvre fase. The invention further comprises a device for sorting out mixed waste, such as rubbish or fractions thereof, for the separate recycling of on the one hand paper and on the other hand plastic film materials, especially in recycling facilities, characterized by the fact that it comprises a pulp solver (pulpers) for the treatment of a pre-sorted fraction containing paper and plastic foils, a liquid removal device, in particular a hole drum, for the screening residue that is brought out of the pulp solver, a division device, possibly with a pre-connected thickener, for the filter residue that has been processed in the liquid removal device, as well as at least one solid/liquid separation device, in particular a flotation container, for separating the plastic film residues as the upper phase.
Ytterligere trekk ved innretningen ifølge oppfinnelsen, som kan være tilveiebrakt alene eller i kombinasjon, er følgende: Den omfatter en siktetrommel som delvis dykker ned i et vaske- hhv. oppslemmingsvæskebad. Further features of the device according to the invention, which can be provided alone or in combination, are the following: It comprises a sifting drum which partially dips into a washing or slurry bath.
I tilslutning til findelingsinnretningen for den avvannede sikteresten er det tilveiebrakt et oppflytnings/avsetnings-beger for gjenoppslemming av sikteresten og for adskillelse av tunge stoffer som steiner, metalldeler, hardplastdeler o.l. In addition to the comminution device for the dewatered sifting residue, a flotation/deposition beaker is provided for re-slurrying the sifting residue and for separating heavy substances such as stones, metal parts, hard plastic parts etc.
I tilslutning til oppflytnings/avsetningsbegeret er det tilveiebrakt en findelingsinnretning, evt. med forkoplet avvannings-fortetter, for den gjenoppslemmede sikteresten. In connection with the floating/settling beaker, a comminution device has been provided, possibly with a connected dewatering condenser, for the re-slurried sifting residue.
Foran faststoff/væske-adskillelsesinnretningen for adskillelse av plastfolierestene er det koplet et tyngdekraft-flotasjonsbeger for adskillelse av flytbare, lette andeler som tre eller skumplast, spesielt polystyrenskum, med unntak av plastfolierester. In front of the solid/liquid separation device for separating the plastic film residues, a gravity flotation cup is connected for the separation of flowable, light parts such as wood or foam plastic, especially polystyrene foam, with the exception of plastic film residues.
Som faststoff/væske-adskillelsesinnretning for adskillelse av plastfolierestene er det tilveiebrakt et strømnings-flotasjonsbeger, hvori plastfolierestene under strømnings-påvirkning foreligger som øvre fase, hvorved en utførelses-innretning for plastfolierestene er tilveiebrakt i området ved væskespeilet i strømnings-fIotasjonsbegeret. As a solid/liquid separation device for separating the plastic film residues, a flow flotation beaker has been provided, in which the plastic film residues under the influence of flow are present as the upper phase, whereby an execution device for the plastic film residues has been provided in the area of the liquid mirror in the flow flotation beaker.
I strømnings-flotasjonsbegeret er det tilveiebrakt et innløpsområde hvori det er anordnet minst ett innløp, samt eventuelt strømningsføringsinnretninger, slik at det dannes en oppflytningssone, hvori det i det minste kan dannes en i det vesentlige horisontalt rettet væskestrøm. In the flow-flotation cup, an inlet area is provided in which at least one inlet is arranged, as well as possibly flow guiding devices, so that a flotation zone is formed, in which at least an essentially horizontally directed liquid flow can be formed.
Det er tilveiebrakt en strømnings-omføringsinnretning i form av en begermellomvegg, som skiller oppflytningssonen fra en hvile- og avsetningssone. A flow diverting device is provided in the form of a cup partition, which separates the buoyancy zone from a rest and deposition zone.
Strømnings-fIotasjonsbegeret oppviser i hvile- og avsetningssonen et i det minste i det vesentlige i tyngdekraftretning forløpende vaeskeavløp. The flow-flotation cup exhibits in the rest and deposition zone a liquid drain which runs at least substantially in the direction of gravity.
Oppfinnelsen er ikke begrenset til den angitte utførelses-formen. Følgelig er f.eks. en annen prosessvannoppredning mulig, og forskjellige transportinnretninger kan utelates, som f.eks. åreskruen 12, slik at tyngdekraft-fIotasjonsbegeret 1 anbringes direkte over våtmøllen 10, samt våtmøllen direkte over utløpet fra oppflytnings/avsetningsbegeret 7. The invention is not limited to the specified embodiment. Consequently, e.g. another process water recovery possible, and different transport devices can be omitted, such as e.g. the propeller 12, so that the gravity flotation beaker 1 is placed directly above the wet mill 10, as well as the wet mill directly above the outlet from the buoyancy/deposition beaker 7.
Spesielt fordelaktig kan, som nevnt innledningsvis, oppfinnelsen anvendes i kombinasjon med et resirkuleringsanlegg hvor det allerede finnes en fiber-våtoppredning. Particularly advantageously, as mentioned at the outset, the invention can be used in combination with a recycling plant where there is already a fiber wet sorting.
Claims (16)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT323186A AT389126B (en) | 1986-12-04 | 1986-12-04 | METHOD AND DEVICE FOR PROCESSING MIXED WASTE AS MUELL OR ITS FRACTIONS FOR RECOVERING PLASTIC |
Publications (4)
Publication Number | Publication Date |
---|---|
NO874940D0 NO874940D0 (en) | 1987-11-26 |
NO874940L NO874940L (en) | 1988-06-06 |
NO168810B true NO168810B (en) | 1991-12-30 |
NO168810C NO168810C (en) | 1992-04-08 |
Family
ID=3547415
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO874940A NO168810C (en) | 1986-12-04 | 1987-11-26 | PROCEDURE AND DEVICE FOR THE CREATION OF MIXED WASTE, AS HOUSEHOLD WASTE OR FRACTIONS THEREOF, FOR THE RECYCLING OF PLASTIC FILM MATERIALS |
Country Status (5)
Country | Link |
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AT (1) | AT389126B (en) |
FI (1) | FI875189A (en) |
GB (1) | GB2198662B (en) |
NO (1) | NO168810C (en) |
SE (1) | SE8704831L (en) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
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SE466387B (en) * | 1989-06-05 | 1992-02-10 | Rejector Ab | SETTING AND DEVICE TO TREAT WASTE |
FR2658751B1 (en) * | 1990-02-23 | 1992-08-07 | Inst Francais Du Petrole | DEVICE FOR PRE-TREATING PLASTIC WASTE BEFORE RECYCLING. |
US5115987A (en) * | 1991-02-19 | 1992-05-26 | Mithal Ashish K | Method for separation of beverage bottle components |
MX9201132A (en) * | 1991-03-14 | 1992-10-01 | Wellman Inc | METHOD AND APPARATUS FOR SEPARATING PLASTIC ARTICLES |
US5333797A (en) * | 1992-04-03 | 1994-08-02 | Becker John C | Commingled recyclables recovery and recycling process and related apparatuses |
US5257740A (en) * | 1992-09-29 | 1993-11-02 | Andritz Sprout-Bauer, Inc. | Apparatus and process for recycling scrap film |
TW221392B (en) * | 1992-09-29 | 1994-03-01 | Sprout Bauer Inc Andritz | Apparatus and process for washing and shredding film |
LU88408A1 (en) * | 1993-09-15 | 1995-04-05 | Quadra Holdings S A | Method and installation for sorting plastics from household and industrial waste |
US5603413A (en) * | 1994-09-01 | 1997-02-18 | Wellman, Inc. | Sortation method for transparent optically active articles |
ES2086264B1 (en) * | 1994-09-21 | 1997-01-16 | Montanes Carmelo Rivera | PROCEDURE FOR THE TREATMENT OF URBAN SOLID WASTE AND INSTALLATION TO CARRY OUT SUCH A PROCEDURE. |
US5609256A (en) * | 1995-01-04 | 1997-03-11 | Carpco, Inc. | Process for recovery of values from solid waste materials |
DE19644437A1 (en) * | 1996-10-25 | 1998-04-30 | Der Gruene Punkt Duales Syst | Process for the digestion of waste containing at least partially recyclable parts |
DE19745896A1 (en) * | 1997-10-17 | 1999-04-22 | Babcock Anlagen Gmbh | Waste treatment method and apparatus |
DE19949265C2 (en) * | 1999-10-12 | 2002-09-19 | Der Gruene Punkt Duales Syst | Process for minimizing the use of new water in the water cycle in a treatment plant |
CN107790277B (en) * | 2017-04-25 | 2024-01-30 | 永清环保股份有限公司 | Mineralized garbage fluidization sorting device and sorting process |
CN113771265A (en) * | 2021-09-06 | 2021-12-10 | 北京化工大学 | Waste disposable mask recovery process and separation tank device for separating mask fabric in process |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CH612707A5 (en) * | 1974-11-07 | 1979-08-15 | Ahlstroem Oy | Process for recovering fibres from fibre material, for example waste paper, and equipment for carrying out the process |
CS201120B1 (en) * | 1976-07-27 | 1980-10-31 | Svetozar Vagac | Method of and apparatus for reclaiming individual components of papermaking combined waste materials |
DE2900666C2 (en) * | 1979-01-10 | 1992-04-02 | Bahr, Albert, Prof. Dr.-Ing., 3392 Clausthal-Zellerfeld | Method and device for the separation of plastic waste of different density and shape |
DE3002061C2 (en) * | 1980-01-21 | 1982-02-11 | Herbert 5942 Kirchhundem Grünewald | Process for the separation of plastics and fibers from mixed waste |
EP0073609A3 (en) * | 1981-08-20 | 1984-07-18 | The Black Clawson Company | Rotary screening machine |
-
1986
- 1986-12-04 AT AT323186A patent/AT389126B/en not_active IP Right Cessation
-
1987
- 1987-11-20 GB GB8727191A patent/GB2198662B/en not_active Expired - Lifetime
- 1987-11-24 FI FI875189A patent/FI875189A/en not_active Application Discontinuation
- 1987-11-26 NO NO874940A patent/NO168810C/en unknown
- 1987-12-02 SE SE8704831A patent/SE8704831L/en not_active Application Discontinuation
Also Published As
Publication number | Publication date |
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FI875189A (en) | 1988-06-05 |
NO168810C (en) | 1992-04-08 |
NO874940L (en) | 1988-06-06 |
GB2198662B (en) | 1990-11-21 |
GB2198662A (en) | 1988-06-22 |
FI875189A0 (en) | 1987-11-24 |
NO874940D0 (en) | 1987-11-26 |
SE8704831D0 (en) | 1987-12-02 |
ATA323186A (en) | 1989-03-15 |
GB8727191D0 (en) | 1987-12-23 |
SE8704831L (en) | 1988-06-05 |
AT389126B (en) | 1989-10-25 |
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