NO163669B - CONTRACTOR FOR ULTRA SOUND DIAGNOSTICS CONTAINING MICROPARTICLES AND GAS Bubbles. - Google Patents
CONTRACTOR FOR ULTRA SOUND DIAGNOSTICS CONTAINING MICROPARTICLES AND GAS Bubbles. Download PDFInfo
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- NO163669B NO163669B NO841490A NO841490A NO163669B NO 163669 B NO163669 B NO 163669B NO 841490 A NO841490 A NO 841490A NO 841490 A NO841490 A NO 841490A NO 163669 B NO163669 B NO 163669B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K49/00—Preparations for testing in vivo
- A61K49/22—Echographic preparations; Ultrasound imaging preparations ; Optoacoustic imaging preparations
- A61K49/222—Echographic preparations; Ultrasound imaging preparations ; Optoacoustic imaging preparations characterised by a special physical form, e.g. emulsions, liposomes
- A61K49/223—Microbubbles, hollow microspheres, free gas bubbles, gas microspheres
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B17/00—Surgical instruments, devices or methods
- A61B17/22—Implements for squeezing-off ulcers or the like on inner organs of the body; Implements for scraping-out cavities of body organs, e.g. bones; for invasive removal or destruction of calculus using mechanical vibrations; for removing obstructions in blood vessels, not otherwise provided for
- A61B2017/22082—Implements for squeezing-off ulcers or the like on inner organs of the body; Implements for scraping-out cavities of body organs, e.g. bones; for invasive removal or destruction of calculus using mechanical vibrations; for removing obstructions in blood vessels, not otherwise provided for after introduction of a substance
- A61B2017/22089—Gas-bubbles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B90/00—Instruments, implements or accessories specially adapted for surgery or diagnosis and not covered by any of the groups A61B1/00 - A61B50/00, e.g. for luxation treatment or for protecting wound edges
- A61B90/39—Markers, e.g. radio-opaque or breast lesions markers
- A61B2090/3925—Markers, e.g. radio-opaque or breast lesions markers ultrasonic
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Abstract
Description
Fremgangsmåte til fremstilling av sukkerbelagte tørre kornprodukter (cerealier). Process for the production of sugar-coated dry cereal products (cereals).
Den foreliggende oppfinnelse angår et spiselig sukkertaelagt tørt kornprodukt (cereal) med redusert hygroskopisk evne og forbedede smaksegenskaper, og går nærmere bestemt ut på en fremgangsmåte til fremstilling av et slikt kornprodukt. Oppfinnelsen går ut på at der i sukkerbelegget anvendes en liten mengde av en sukkerfosfat-sammensetning som vil bli beskrevet i det etterfølgende. The present invention relates to an edible sugar-coated dry cereal product (cereal) with reduced hygroscopic ability and improved taste properties, and more specifically concerns a method for producing such a cereal product. The invention is based on the use of a small amount of a sugar-phosphate composition in the sugar coating which will be described below.
I de senere år har kornprodukter (cerealier) som er innkapslet i eller belagt med glaserte eller harde sukkerbelegg bare i begrenset grad vært gunstig mottatt av voksne forbrukere, til tross for at slike kornprodukter har ønskede bekvemmelig-hetsegenskaper, idet de kan spises tørre og hvis de anvendes med melk, fløte eller lignende, slik det er vanlig for de overalt anvendte frokost-kornprodukter, ikke krever noen ytterligere tilsetning av sukker. Grunnen til at disse kornprodukter ikke har oppnådd noen vesentlig tilslutning blant voksne personer er blant annet at de er tilbøyelige til å være for søte. Andre fremtredende ulemper som undertiden kan observeres ved sukkerbelagte kornprodukter, er (1) at produktene ofte er klebrige, (2) at de er hygroskopiske, (3) at de er seige å spise, og (4) at sukkerbelegget er tilbøyelig til å krystallisere. In recent years, cereal products (cereals) encased in or coated with glazed or hard sugar coatings have only been favorably received by adult consumers to a limited extent, despite the fact that such cereal products have desirable convenience properties, in that they can be eaten dry and if they are used with milk, cream or the like, as is usual for the ubiquitous breakfast cereal products, do not require any further addition of sugar. The reason why these cereal products have not achieved any significant approval among adults is, among other things, that they tend to be too sweet. Other prominent disadvantages that can sometimes be observed with sugar-coated cereal products are (1) that the products are often sticky, (2) that they are hygroscopic, (3) that they are chewy to eat, and (4) that the sugar coating tends to crystallize .
En hensikt med den foreliggende oppfinnelse er å skaffe et spiselig sukkerbelagt tørt kornprodukt med reduserte hygroskopiske egenskaper og smaksegenskaper som er mere tilfredsstillende etter voksen smak. One purpose of the present invention is to provide an edible sugar-coated dry grain product with reduced hygroscopic properties and taste properties that are more satisfactory after adult taste.
En ytterligere hensikt med oppfinnelsen er å skaffe et spiselig sukkerbelagt tørt kornprodukt som er sprøere enn de hittil tilgjengelige produkter. A further purpose of the invention is to provide an edible sugar-coated dry cereal product which is crisper than the products available to date.
Det er overraskende blitt fastslått at der oppnås et spiselig sukkerbelagt tørt kornprodukt som har redusert hygroskopisk evne og forbedrede smaksegenskaper (smak og sprøhet er mer tilfredsstillende for voksne forbrukere), hvis en liten mengde av en sulckerfosfat-sammensetning tilsettes den vanlige sukkerbelegg-oppløsning før denne påføres kornproduktet. It has surprisingly been found that an edible sugar-coated dry cereal product having reduced hygroscopicity and improved taste properties (taste and crispiness are more satisfactory to adult consumers) is obtained if a small amount of a sulcker phosphate composition is added to the usual sugar coating solution prior to this is applied to the grain product.
Under uttrykket «sukkerfosfat-sammensetning» slik det anvendes i den foreliggende fremstiling, menes der en stoffsammensetning som består av en kompleksforbindelse av to bestanddeler a og b, idet bestanddelen a består av ett eller flere salter av ett eller flere sukkerfosfater, og bestanddelen b består av ett eller flere uorganiske fosfater hvis kation eller kationer er valgt fra de flerverdige metallkationer som vanligvis ville danne hovedsakelig vannuoppløselige fosfater, samtidig som den nevnte forbindelse er slik at minst 2 vektprosent av bestanddel b regnet på vekten av bestanddel a er oppløselig i vann ved omgivelsesforhold når det samlede opp-løste sukkerfosfat og uorganiske fosfat overstiger 5 vektdeler pr. 100 vektdeler vann. Under the term "sugar phosphate composition" as used in the present formulation, is meant a substance composition consisting of a complex compound of two components a and b, with component a consisting of one or more salts of one or more sugar phosphates, and component b consisting of one or more inorganic phosphates whose cation or cations are selected from the polyvalent metal cations which would normally form mainly water-insoluble phosphates, while the said compound is such that at least 2 percent by weight of component b calculated on the weight of component a is soluble in water at ambient conditions when the total dissolved sugar phosphate and inorganic phosphate exceeds 5 parts by weight per 100 parts by weight of water.
En slik stoffsammensetning og frem-gangsmåter til dens fremstilling er beskrevet i sørafrikansk patentskrift nr. 65/6046. Such a substance composition and methods for its production are described in South African patent document No. 65/6046.
Som beskrevet nærmere i det foran As described in more detail above
nevnte patentskrift kan den sukkerfosfat-sammensetning som anvendes ved fremgangsmåten ifølge den foreliggende oppfinnelse, fremstilles ved fosforylering av et sukker, fortrinnsvis sukrose, mais-sukker, glykose, fruktose, maltose eller laktose, resp. blandinger av disse sukre, i nærvær av en egnet base av det flerverdige metallion og gjenvinning av et produkt som inneholder sukkerfosfatsalter i kompleksforbindelse med et uorganisk fosfat av det flerverdige metallion. Et egnet fosforyler-ingsmiddel er fosfor-oksyklorid (vanligvis tilsatt i trikloreten-oppløsning), og et egnet flerverdig metallion er kalsium. said patent, the sugar phosphate composition used in the method according to the present invention can be produced by phosphorylating a sugar, preferably sucrose, corn sugar, glucose, fructose, maltose or lactose, resp. mixtures of these sugars, in the presence of a suitable base of the polyvalent metal ion and recovery of a product containing sugar phosphate salts in complex with an inorganic phosphate of the polyvalent metal ion. A suitable phosphorylating agent is phosphorus oxychloride (usually added in trichloroethene solution), and a suitable polyvalent metal ion is calcium.
Gjenvinning av produktet krever vanligvis utfelling med en alkohol, fortrinnsvis etanol, fulgt av vasking med etanol/vann for å fjerne det flerverdige metallionklorid. Den faste sukkerfosfat-sammensetning som gjenvinnes på denne måte, er sterkt oppløselig i vann for å danne oppløsnin-ger som inneholder en betydelig mengde oppløselig uorganisk fosfat (som vanligvis er vann-uoppløselig). Disse oppløsninger er stabile i lange tidsrom ved konsentrasjo-ner på mere enn 5 vektprosent av de samlede oppløste fosfater. Nedenfor vil der bli beskrevet en fremgangsmåte som ansku-eliggjør fremstillingen av en bestemt sukkerfosfat-sammensetning som egner seg for innlemmelse i sukkerbelegg-oppløsnin-gene i overensstemmelse med den foreliggende oppfinnelse. Recovery of the product usually requires precipitation with an alcohol, preferably ethanol, followed by washing with ethanol/water to remove the polyvalent metal ion chloride. The solid sugar phosphate composition thus recovered is highly soluble in water to form solutions containing a significant amount of soluble inorganic phosphate (which is usually water insoluble). These solutions are stable for long periods of time at concentrations of more than 5% by weight of the total dissolved phosphates. Below will be described a method which illustrates the production of a specific sugar phosphate composition which is suitable for incorporation into the sugar coating solutions in accordance with the present invention.
En oppløsning på 127 kilogram sukrose A solution of 127 kilograms of sucrose
i 63,5 liter vann ble blandet med 295 1 vann og 68 kilogram lesket kalk i et reaksjonskar. Ytterligere vann ble tilsatt for å innstille volumet på 591 1. Opp-løsningen ble avkjølet til 5°C og holdt på denne temperatur i 8 timer. I løpet av denne tid ble 54,5 kilogram fosfor-oksyklorid oppløst i 54,5 kilogram trikloreten og gradvis tilsatt under kraftig omrøring Etterat reaksjonen var avsluttet, ble blan-dingen sentrifugert for å fjerne suspen-derte faste stoffer og pumpet inn i en be-holder med glassforing, hvor 2000 1 denatu-rert absolutt alkohol ble tilsatt under om-røring for å utfelle produktet. Det utfeltc produkt ble fraskilt og lutet med fire ad-skilte mengder av 80 pst.'s etanol før det ble samlet i en sentrifuge og tørket til e1 fint hvitt pulver. in 63.5 liters of water was mixed with 295 1 of water and 68 kilograms of slaked lime in a reaction vessel. Additional water was added to adjust the volume to 591 L. The solution was cooled to 5°C and held at this temperature for 8 hours. During this time, 54.5 kilograms of phosphorus oxychloride was dissolved in 54.5 kilograms of the trichloroethene and gradually added with vigorous stirring. After the reaction was complete, the mixture was centrifuged to remove suspended solids and pumped into a be -holder with glass lining, where 2000 1 of denatured absolute alcohol was added with stirring to precipitate the product. The precipitated product was separated and leached with four separate amounts of 80 percent ethanol before being collected in a centrifuge and dried to a fine white powder.
Det faste produkt som ble fremstill The solid product that was produced
ved denne fremgangsmåte, ble analyserl og funnet å inneholde en kompleksforbindelse (som definert foran) av (a) kal- by this method, was analyzed and found to contain a complex compound (as defined above) of (a) cal-
sium-sukrose-fosfater og (b) et uorganisk kalsium-ortofosfat. sium sucrose phosphates and (b) an inorganic calcium orthophosphate.
De kornproduktpartikler som kan belegges med belegningsoppløsninger i overensstemmelse med den foreliggende oppfinnelse, omfatter alle de ferdig tilberedte kornprodukter som vanligvis betegnes som «breakfast cereals». Disse kornprodukter kan videre foreligge i en hvilken som helst vanlig fysisk form, f. eks. som flak, korn, pulver, ekspanderte partikler (puffs) etc. Visse typiske kornprodukter som kan belegges, er: corn flakes, ekspandert mais, hvete eller ris, hveteflak og havre. The cereal product particles that can be coated with coating solutions in accordance with the present invention include all the ready-made cereal products that are usually referred to as "breakfast cereals". These cereal products can also be present in any common physical form, e.g. such as flakes, grains, powders, expanded particles (puffs) etc. Certain typical grain products that can be coated are: corn flakes, expanded corn, wheat or rice, wheat flakes and oats.
Sukkerbelegg-oppløsninger som er egnet for anvendelse ved utførelse av den Sugar coating solutions suitable for use in its execution
- foreliggende oppfinnelse, omfatter overveiende et spiselig sukker, som f. eks. suk-i rose, hydrolysert sukrose, dektrose, glykose, fruktose, laktose, honning eller blandinger av disse sukre, og en liten mengde - present invention, predominantly comprises an edible sugar, such as e.g. suk-i rose, hydrolysed sucrose, dextrose, glucose, fructose, lactose, honey or mixtures of these sugars, and a small amount
av den sukkerfosfat-sammensetning som er angitt foran og beskrevet i det foran nevnte patentskrift. I tillegg til sukkeret of the sugar-phosphate composition stated above and described in the aforementioned patent document. In addition to the sugar
og sukkerfosfat-sammensetningen kan be-•■ legningsoppløsningen inneholde mindre : mengder smaksstoffer, salt, natrium-ace-tat eller andre små mengder av bestanddeler som også tidligere har vært ansett som gunstige i lignende oppløsninger. Inn-. holdet av oppløsningsmiddel i belegnings-oppløsningen vil vanligvis ikke vesentlig overstige den mengde som er nødvendig and the sugar-phosphate composition, the coating solution may contain smaller quantities of flavourings, salt, sodium acetate or other small quantities of components which have also previously been considered beneficial in similar solutions. In-. the amount of solvent in the coating solution will usually not significantly exceed the amount necessary
for å oppløse sukkeret og sukkerfosfat-sammensetningen samt de øvrige bestanddeler, og vil vanligvis ligge i området fra 20 til 50 vektprosent regnet på den sam-i lede mengde av belegningsoppløsningen. En foretrukken belegningsoppløsning ; for anvendelse ifølge oppfinnelsen, vil om-; fatte 35 til 65 vektprosent av ett eller flere sukre, fra 20 til 50 vektprosent vann, fra , 0,1 til 15 vektprosent sukkerfosfat-sammensetning og forøvrig eventuelt salt og/ to dissolve the sugar and the sugar-phosphate composition as well as the other components, and will usually lie in the range from 20 to 50 percent by weight based on the combined amount of the coating solution. A preferred coating solution; for use according to the invention, will re-; contain 35 to 65 percent by weight of one or more sugars, from 20 to 50 percent by weight of water, from , 0.1 to 15 percent by weight of a sugar-phosphate composition and other possible salt and/
eller andre smaksstoffer. En sukkerbeleg-i ningsoppløsning som foretrekkes i enda . sterkere grad, vil omfatte sukker i form av sukrose og/eller mais-sukker, mens sukkerfosfat-sammensetningen vil foreligge i form av en blanding av kalsium-sukrose-fosfat og kalsium-ortofosfat, samtidig som vektforholdet mellom sukkeret og sukker-! fosfat-sammensetningen ligger i området fra 10:1 til 20:1, mens resten av oppløs-; ningen består av vann og mindre mengder ; (mindre enn 2 vektprosent) av smaksstoffer, salt og lignende. En særlig foretrukken ; belegningsoppløsning vil inneholde mel-; lom 1 og 8 vektprosent av sukkerfosfat-sammensetningen. or other flavorings. A sugar coating solution which is preferred in even . to a greater extent, will include sugar in the form of sucrose and/or corn sugar, while the sugar phosphate composition will be in the form of a mixture of calcium-sucrose-phosphate and calcium-orthophosphate, while the weight ratio between the sugar and sugar-! the phosphate composition lies in the range from 10:1 to 20:1, while the rest of the dissolve-; ning consists of water and smaller amounts; (less than 2% by weight) of flavourings, salt and the like. A particularly preferred one; coating solution will contain flour; between 1 and 8 percent by weight of the sugar phosphate composition.
Da de tørre bestanddeler er oppløselige, kan belegningsoppløsningen som skal anvendes ved oppfinnelsen, fremstilles rett og slett ved tilsetning av bestanddelene til vann eller et annet egnet oppløsningsmid-del uten omrøring eller med svak omrøring inntil hovedsakelig alle de faste stoffer er oppløst. Tilsetningen kan naturligvis også finne sted i omvendt rekkefølge, d.v.s. oppløsningsmiddelet kan tilsettes en for-håndsblanding av de tørre bestanddeler. Den rekkefølge som bestanddelene tilsettes i, er imidlertid ikke noe avgjørende trekk ved oppfinnelsen, og en hvilken som helst fremgangsmåte til oppløsning av de faste stoffer i oppløsningsmiddelet ligger derfor innenfor rammen for oppfinnelsen. As the dry components are soluble, the coating solution to be used in the invention can be prepared simply by adding the components to water or another suitable solvent without stirring or with slight stirring until essentially all the solids are dissolved. The addition can of course also take place in the reverse order, i.e. the solvent can be added to a premix of the dry ingredients. However, the order in which the components are added is not a decisive feature of the invention, and any method for dissolving the solids in the solvent is therefore within the scope of the invention.
Belegningsoppløsningen påføres kornproduktene på måter som er vel kjent for fagfolk. Kornproduktene kan f. eks. an-bringes i en belegningsmaskin med roterende trommel, og belegningsoppløsningen som f. eks. kan ha en sammensetning som angitt ovenfor og være oppvarmet til en forhøyet temperatur, kan langsomt dryp-pes ned på de roterende kornprodukter. Etterat tilstrekkelig oppløsning er tilsatt, kan maskinen fortsette å gå ytterligere et par minutter eller til produktet strømmer fritt. Eventuelt vann som opprinnelig er tilstede i belegningsoppløsningen, blir praktisk talt fjernet under omrøringen i belegningsmaskinen og/eller ved et etter-følgende tørketrinn. Foråt der skal oppnås fullstendig oppløsning av de faste stoffer og skaffes varme for fordampningen av vannet, blir belegningsoppløsningen ofte oppvarmet til i nærheten av kokepunktet, d.v.s. til 99—127°C før den tilsettes kornproduktet. Temperaturen av belegnings-oppløsningen har imidlertid ikke noen av-gjørende innflytelse på mulighetene for å gjennomføre fremgangsmåten ifølge oppfinnelsen, og variasjoner for tilpasning til forskjellige industrielle prosesser må an-ses å ligge innenfor rammen for oppfinnelsen. Etterat belegningsoppløsningen er påført kornproduktene, kan disse tørkes ved værelsetemperatur i 2—12 timer, men ved industriell drift er det vanligvis mere ønskelig å tørke ved høyere temperaturer, nærmere bestemt 38—82<C>C, i kortere tidsrom for å oppnå større sprøhet. The coating solution is applied to the cereal products in ways well known to those skilled in the art. The cereal products can e.g. placed in a coating machine with a rotating drum, and the coating solution such as can have a composition as indicated above and be heated to an elevated temperature, can be slowly dripped onto the rotating cereal products. After sufficient solution has been added, the machine may continue to run for another few minutes or until the product flows freely. Any water originally present in the coating solution is practically removed during the stirring in the coating machine and/or in a subsequent drying step. Before complete dissolution of the solids is to be achieved and heat provided for the evaporation of the water, the coating solution is often heated to near the boiling point, i.e. to 99-127°C before it is added to the grain product. However, the temperature of the coating solution does not have any decisive influence on the possibilities of carrying out the method according to the invention, and variations for adaptation to different industrial processes must be considered to lie within the scope of the invention. After the coating solution has been applied to the grain products, these can be dried at room temperature for 2-12 hours, but in industrial operation it is usually more desirable to dry at higher temperatures, specifically 38-82<C>C, for a shorter period of time to achieve greater brittleness .
Mengden av belegg som tilsettes det tørre kornprodukt, vil hovedsakelig avhen-ge av de egenskaper som ønskes i det fer-dige produkt. De sukkerbelagte kornprodukter som for tiden finnes i handelen, inneholder vanligvis mellom 15 og 60 pst. tørt beleggmateriale regnet på den samlede vekt av det belagte kornprodukt. Iføl-ge den foreliggende oppfinnelse foretrekkes det at sukkerbelegget utgjør mellom 30 og 55 vektprosent av det samlede produkt. Belegningsmengden kan ikke desto mindre varieres innen vide grenser, og fordelene ved oppfinnelsen vil fremtre også utenfor det ovenfor angitte foretrukne område. Den mengde belegningsoppløsning som kan anvendes, vil naturligvis være av-hengig av den mengde av belegg som skal påføres kornproduktet, samt den mengde oppløsningsmiddel som skal fordampes under påføringen av belegget. The amount of coating added to the dry grain product will mainly depend on the properties desired in the finished product. The sugar-coated cereal products currently available in the trade usually contain between 15 and 60 percent dry coating material calculated on the total weight of the coated cereal product. According to the present invention, it is preferred that the sugar coating constitutes between 30 and 55 percent by weight of the overall product. The amount of coating can nevertheless be varied within wide limits, and the advantages of the invention will appear also outside the preferred range stated above. The amount of coating solution that can be used will, of course, depend on the amount of coating to be applied to the grain product, as well as the amount of solvent that is to evaporate during the application of the coating.
De følgende spesielle eksempler er ment å skulle gi et bilde av de belagte kornprodukter som kan fremstilles ifølge den foreliggende oppfinnelse, og den måte de fremstilles på. The following special examples are intended to give an image of the coated cereal products that can be produced according to the present invention, and the way in which they are produced.
Eksempel 1. Example 1.
De nedenfor angitte bestanddeler i de angitte mengder ble anbragt i en blande-beholder av rustfritt stål og omrørt inntil der ble dannet en klar oppløsning. Den bestanddel som er betegnet som «sukkerfosfatsammensetning», ble fremstilt ved den foran angitte fremgangsmåte. The ingredients listed below in the quantities listed were placed in a stainless steel mixing container and stirred until a clear solution was formed. The component which is designated as "sugar phosphate composition" was produced by the method indicated above.
Prøveoppløsningen ble oppvarmet på en varm plate til 121°C, hvoretter den langsomt ble dryppet ned på 50 gram «corn flakes» som ble holdt under omrøring i en belegningsmaskin med roterende trommel. Etter tilsetning av 75 gram belegnings-oppløsning ble maskinen holdt igang i ytterligere 3 minutter inntil produktet ble fritt-strømmende. Produktet (glasert «cereal») ble deretter fordelt på en bordplate for å tørke (fjerning av hovedsakelig alt vann) i ca. 12 timer. Fremgangsmåten ble nøyaktig gjentatt for sammenligningsopp-løsningen. Det kornprodukt som var belagt med prøveoppløsningen, ble sammenlignet med det kornprodukt som var belagt med sammenligningsoppløsningen, idet begge produkter ble vurdert med hensyn til smaksegenskaper og hygroskopisk evne. Det kornprodukt som var belagt med prøve-oppløsningen, var mindre hygroskopisk, mørere (sprøere) å spise og var mindre søtt ved prøving av et prøveutvalg av voksne personer. Det kornprodukt som var belagt med prøveoppløsningen, var dess-uten mindre klebrig, og der var mindre til-bøyelighet til at belegget krystalliserte. The sample solution was heated on a hot plate to 121°C, after which it was slowly dripped onto 50 grams of "corn flakes" which were kept under stirring in a coating machine with a rotating drum. After adding 75 grams of coating solution, the machine was kept running for a further 3 minutes until the product became free-flowing. The product (glazed "cereal") was then spread on a table top to dry (removal of essentially all water) for approx. 12 hours. The procedure was exactly repeated for the comparison solution. The cereal product coated with the test solution was compared with the cereal product coated with the comparison solution, both products being assessed with regard to taste properties and hygroscopic ability. The cereal product coated with the sample solution was less hygroscopic, more tender (crunchier) to eat and less sweet when tested by a sample of adults. The grain product that was coated with the sample solution was, moreover, less sticky, and there was less tendency for the coating to crystallize.
Eksempel 2. Example 2.
Sukkerbelegningsoppløsninger ble fremstilt i overensstemmelse med den fremgangsmåte som er nevnt i eksempel 1, og Sugar coating solutions were prepared in accordance with the method mentioned in example 1, and
ble påført ekspandert ris. Sammenlignet was applied to expanded rice. Compared
med det kornprodukt som var belagt med with the grain product with which it was coated
sammenligningsoppløsningen var det kornprodukt som var belagt med den oppløsnin-gen som inneholdt sukkerfosfatsammensetningen, på samme måte som i eksempel 1 the comparison solution was the cereal product which was coated with the solution which contained the sugar phosphate composition, in the same way as in example 1
mindre hygroskopisk, mørere å spise og less hygroscopic, more tender to eat and
mindre søtt ved prøving av et prøveutvalg less sweet when trying a sample selection
av voksne personer. Det med prøveoppløs-ning belagte kornprodukt var likeledes of adults. The grain product coated with sample solution was likewise
mindre klebrig, og belegget var mindre til-bøyelig til å krystallisere. less sticky, and the coating was less prone to crystallisation.
Det har lenge vært kjent at visse uorganiske fosfater, f. eks. kalsium-ortofosfat, kan være nyttige for reduksjon av fore-komsten av karies i tenner. Belagte kornprodukter som inneholder et sukkerfosfat It has long been known that certain inorganic phosphates, e.g. calcium orthophosphate, can be useful for reducing the occurrence of caries in teeth. Coated cereals containing a sugar phosphate
i kompleksforbindelse med uorganisk fosfat, vil derfor sannsynligvis være mindre in complex connection with inorganic phosphate, will therefore probably be smaller
karies-frembringende enn vanlige sukkerbelagte kornprodukter. Det vil imidlertid caries-producing than usual sugar-coated cereal products. It will, however
forstås at man for å klarlegge nytten av it is understood that in order to clarify the usefulness of
oppfinnelsen ikke baserer seg på denne the invention is not based on this
mulige fordel. possible advantage.
Den foranstående detaljerte beskrivel-se tjener bare til å forklare oppfinnelsen, The foregoing detailed description serves only to explain the invention,
og ingen unødvendige begrensninger skal and no unnecessary restrictions shall
kunne utledes av beskrivelsen, idet modifi-kasjoner vil være innlysende for fagfolk. could be derived from the description, as modifications will be obvious to those skilled in the art.
Claims (4)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3313947A DE3313947A1 (en) | 1983-04-15 | 1983-04-15 | MICROPARTICLES AND GAS BUBBLES CONTAINING ULTRASONIC CONTRASTING AGENTS |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO841490L NO841490L (en) | 1984-10-16 |
| NO163669B true NO163669B (en) | 1990-03-26 |
| NO163669C NO163669C (en) | 1990-07-04 |
Family
ID=6196666
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO841490A NO163669C (en) | 1983-04-15 | 1984-04-13 | CONTRACTOR FOR ULTRA SOUND DIAGNOSTICS CONTAINING MICROPARTICLES AND GAS Bubbles. |
Country Status (12)
| Country | Link |
|---|---|
| EP (1) | EP0123235B1 (en) |
| JP (1) | JPS59205329A (en) |
| AT (1) | ATE36959T1 (en) |
| AU (1) | AU569072B2 (en) |
| CA (1) | CA1232837A (en) |
| DE (2) | DE3313947A1 (en) |
| DK (1) | DK165622C (en) |
| FI (1) | FI81265C (en) |
| IE (1) | IE57197B1 (en) |
| NO (1) | NO163669C (en) |
| NZ (1) | NZ207854A (en) |
| ZA (1) | ZA842800B (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4277367A (en) * | 1978-10-23 | 1981-07-07 | Wisconsin Alumni Research Foundation | Phantom material and method |
| US4265251A (en) * | 1979-06-28 | 1981-05-05 | Rasor Associates, Inc. | Method of determining pressure within liquid containing vessel |
| ATE17311T1 (en) * | 1980-11-17 | 1986-01-15 | Schering Ag | PREPARATION FOR GENERATING MICROBUBBLES. |
| DE3141641A1 (en) * | 1981-10-16 | 1983-04-28 | Schering Ag, 1000 Berlin Und 4619 Bergkamen | ULTRASONIC CONTRAST AGENTS AND THEIR PRODUCTION |
| DE3313946A1 (en) * | 1983-04-15 | 1984-10-18 | Schering AG, 1000 Berlin und 4709 Bergkamen | MICROPARTICLES AND GAS BUBBLES CONTAINING ULTRASONIC CONTRASTING AGENTS |
-
1983
- 1983-04-15 DE DE3313947A patent/DE3313947A1/en not_active Withdrawn
-
1984
- 1984-02-20 DK DK079084A patent/DK165622C/en not_active IP Right Cessation
- 1984-04-05 IE IE836/84A patent/IE57197B1/en not_active IP Right Cessation
- 1984-04-11 CA CA000451729A patent/CA1232837A/en not_active Expired
- 1984-04-12 FI FI841463A patent/FI81265C/en not_active IP Right Cessation
- 1984-04-12 JP JP59071940A patent/JPS59205329A/en active Granted
- 1984-04-13 ZA ZA842800A patent/ZA842800B/en unknown
- 1984-04-13 DE DE8484104211T patent/DE3473829D1/en not_active Expired
- 1984-04-13 AU AU26806/84A patent/AU569072B2/en not_active Ceased
- 1984-04-13 NO NO841490A patent/NO163669C/en not_active IP Right Cessation
- 1984-04-13 AT AT84104211T patent/ATE36959T1/en not_active IP Right Cessation
- 1984-04-13 NZ NZ207854A patent/NZ207854A/en unknown
- 1984-04-13 EP EP84104211A patent/EP0123235B1/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FI81265C (en) | 1990-10-10 |
| EP0123235B1 (en) | 1988-09-07 |
| ZA842800B (en) | 1984-11-28 |
| FI81265B (en) | 1990-06-29 |
| CA1232837A (en) | 1988-02-16 |
| NO163669C (en) | 1990-07-04 |
| NZ207854A (en) | 1988-01-08 |
| IE840836L (en) | 1984-10-15 |
| FI841463A0 (en) | 1984-04-12 |
| DK165622C (en) | 1993-06-01 |
| AU2680684A (en) | 1984-10-18 |
| EP0123235A3 (en) | 1986-11-20 |
| EP0123235A2 (en) | 1984-10-31 |
| DK165622B (en) | 1992-12-28 |
| JPH0417164B2 (en) | 1992-03-25 |
| ATE36959T1 (en) | 1988-09-15 |
| DK79084A (en) | 1984-10-16 |
| IE57197B1 (en) | 1992-06-03 |
| FI841463L (en) | 1984-10-16 |
| DK79084D0 (en) | 1984-02-20 |
| JPS59205329A (en) | 1984-11-20 |
| DE3473829D1 (en) | 1988-10-13 |
| AU569072B2 (en) | 1988-01-21 |
| NO841490L (en) | 1984-10-16 |
| DE3313947A1 (en) | 1984-10-18 |
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