NO119795B - - Google Patents
Download PDFInfo
- Publication number
- NO119795B NO119795B NO54069A NO54069A NO119795B NO 119795 B NO119795 B NO 119795B NO 54069 A NO54069 A NO 54069A NO 54069 A NO54069 A NO 54069A NO 119795 B NO119795 B NO 119795B
- Authority
- NO
- Norway
- Prior art keywords
- silicic acid
- solution
- hydrolysis
- titanium
- pigments
- Prior art date
Links
- 239000000049 pigment Substances 0.000 claims description 35
- 235000012239 silicon dioxide Nutrition 0.000 claims description 35
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 34
- 239000002245 particle Substances 0.000 claims description 21
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 20
- 230000007062 hydrolysis Effects 0.000 claims description 18
- 238000006460 hydrolysis reaction Methods 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 16
- 230000029087 digestion Effects 0.000 claims description 15
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 8
- 239000010936 titanium Substances 0.000 claims description 7
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 229910052719 titanium Inorganic materials 0.000 claims description 6
- 239000004408 titanium dioxide Substances 0.000 claims description 6
- 238000007669 thermal treatment Methods 0.000 claims description 5
- 108010010803 Gelatin Proteins 0.000 claims description 4
- 229920000159 gelatin Polymers 0.000 claims description 4
- 239000008273 gelatin Substances 0.000 claims description 4
- 235000019322 gelatine Nutrition 0.000 claims description 4
- 235000011852 gelatine desserts Nutrition 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 150000002894 organic compounds Chemical class 0.000 claims description 3
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims description 3
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 2
- 239000012141 concentrate Substances 0.000 claims description 2
- 239000008394 flocculating agent Substances 0.000 claims description 2
- 239000003292 glue Substances 0.000 claims description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 1
- 150000002605 large molecules Chemical class 0.000 claims 1
- 239000000243 solution Substances 0.000 description 38
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 13
- 238000000926 separation method Methods 0.000 description 10
- 238000001354 calcination Methods 0.000 description 9
- 238000001914 filtration Methods 0.000 description 8
- 229910052742 iron Inorganic materials 0.000 description 6
- IYVLHQRADFNKAU-UHFFFAOYSA-N oxygen(2-);titanium(4+);hydrate Chemical compound O.[O-2].[O-2].[Ti+4] IYVLHQRADFNKAU-UHFFFAOYSA-N 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 238000005189 flocculation Methods 0.000 description 3
- 230000016615 flocculation Effects 0.000 description 3
- 159000000014 iron salts Chemical class 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000009036 growth inhibition Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical class Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 description 2
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 150000003112 potassium compounds Chemical class 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 229910021577 Iron(II) chloride Inorganic materials 0.000 description 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 238000000184 acid digestion Methods 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000001493 electron microscopy Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 230000005021 gait Effects 0.000 description 1
- 230000009422 growth inhibiting effect Effects 0.000 description 1
- 239000003966 growth inhibitor Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- VBLQNYINPWASGP-UHFFFAOYSA-M oxygen(2-) titanium(3+) chloride Chemical compound [O-2].[Ti+3].[Cl-] VBLQNYINPWASGP-UHFFFAOYSA-M 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- WRWQVSOJXAVREP-UHFFFAOYSA-J tetrachlorotitanium hydrochloride Chemical compound Cl.[Cl-].[Cl-].[Cl-].[Cl-].[Ti+4] WRWQVSOJXAVREP-UHFFFAOYSA-J 0.000 description 1
- 150000003608 titanium Chemical class 0.000 description 1
- BAKALPNAEUOCDL-UHFFFAOYSA-N titanium hydrochloride Chemical compound Cl.[Ti] BAKALPNAEUOCDL-UHFFFAOYSA-N 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
- C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/10—Particle morphology extending in one dimension, e.g. needle-like
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Silicon Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE1968T0035892 DE1667857B2 (de) | 1968-02-17 | 1968-02-17 | Verfahren zur herstellung von rutilpigmenten abgerundeter teilchenform aus titanchloridloesungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO119795B true NO119795B (en, 2012) | 1970-07-06 |
Family
ID=7559466
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO54069A NO119795B (en, 2012) | 1968-02-17 | 1969-02-12 |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE727467A (en, 2012) |
| DE (1) | DE1667857B2 (en, 2012) |
| ES (1) | ES363705A1 (en, 2012) |
| FI (1) | FI49702C (en, 2012) |
| NL (1) | NL165130C (en, 2012) |
| NO (1) | NO119795B (en, 2012) |
-
1968
- 1968-02-17 DE DE1968T0035892 patent/DE1667857B2/de active Granted
-
1969
- 1969-01-27 BE BE727467D patent/BE727467A/xx unknown
- 1969-02-12 NO NO54069A patent/NO119795B/no unknown
- 1969-02-12 FI FI43369A patent/FI49702C/fi active
- 1969-02-14 NL NL6902383A patent/NL165130C/xx not_active IP Right Cessation
- 1969-02-15 ES ES363705A patent/ES363705A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE1667857A1 (de) | 1971-06-24 |
| DE1667857B2 (de) | 1976-08-12 |
| FI49702C (fi) | 1975-09-10 |
| NL165130B (nl) | 1980-10-15 |
| FI49702B (en, 2012) | 1975-06-02 |
| NL6902383A (en, 2012) | 1969-08-19 |
| NL165130C (nl) | 1981-03-16 |
| ES363705A1 (es) | 1971-01-01 |
| BE727467A (en, 2012) | 1969-07-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4923682A (en) | Preparation of pure titanium dioxide with anatase crystal structure from titanium oxychloride solution | |
| US3862297A (en) | Manufacture of pigmentary titanium dioxide | |
| JPH08225324A (ja) | アナターゼ二酸化チタン及びその製法 | |
| US3091515A (en) | Method for producing titanium dioxide pigments | |
| NO854918L (no) | Fremgamgsmaate til fremstilling av titandioksyd. | |
| US4283377A (en) | Process for the preparation of basic zirconium carbonate of high purity | |
| JPH09188518A (ja) | アナターゼ型二酸化チタンの製法 | |
| US8268203B2 (en) | Method for producing microcrystalline titanium oxide | |
| US4014977A (en) | Process for the hydrolysis of titanium sulphate solutions | |
| JPS61168529A (ja) | 高品質二酸化チタンの製造方法 | |
| US3615204A (en) | Preparation of anatase titanium dioxide pigment | |
| NO119795B (en, 2012) | ||
| NO120990B (en, 2012) | ||
| US2406465A (en) | Titanium oxide pigment production | |
| CN106542573A (zh) | 一种制备颜料二氧化钛的方法 | |
| US2361987A (en) | Titanium pigment production | |
| US2771345A (en) | Preparation of titanium dioxide pigments | |
| US3617217A (en) | Preparation of anatase titanium dioxide pigment | |
| GB2291052A (en) | Production of rutile titanium dioxide | |
| US3565580A (en) | Process for the manufacture of rutile pigments with rounded-off particle from titanium chloride solutions | |
| US2290922A (en) | Preparation of titanium oxide | |
| WO2003055805A1 (fr) | Poudre d'oxyde de tantale ou d'oxyde de niobium et procede de production de celle-ci | |
| US4781911A (en) | TiO2 for ceramic frits and glazes | |
| US2034923A (en) | Manufacture of titanium pigments | |
| CN112875750A (zh) | 一种金红石型钛白粉煅烧晶种的制备方法及其应用 |