NO116966B - - Google Patents
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- Publication number
- NO116966B NO116966B NO158282A NO15828265A NO116966B NO 116966 B NO116966 B NO 116966B NO 158282 A NO158282 A NO 158282A NO 15828265 A NO15828265 A NO 15828265A NO 116966 B NO116966 B NO 116966B
- Authority
- NO
- Norway
- Prior art keywords
- drum
- glycol
- ethylene glycol
- condensation
- vessel
- Prior art date
Links
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 96
- 238000000034 method Methods 0.000 claims description 13
- 238000009833 condensation Methods 0.000 claims description 10
- 230000005494 condensation Effects 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 5
- 150000002148 esters Chemical class 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000000110 cooling liquid Substances 0.000 claims description 3
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 2
- 239000005977 Ethylene Substances 0.000 claims description 2
- 238000007790 scraping Methods 0.000 claims description 2
- 239000011343 solid material Substances 0.000 claims description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 32
- 238000006116 polymerization reaction Methods 0.000 description 7
- 238000011084 recovery Methods 0.000 description 7
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 229920000728 polyester Polymers 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- -1 polyethylene terephthalate Polymers 0.000 description 3
- 238000004064 recycling Methods 0.000 description 3
- MHCVCKDNQYMGEX-UHFFFAOYSA-N 1,1'-biphenyl;phenoxybenzene Chemical compound C1=CC=CC=C1C1=CC=CC=C1.C=1C=CC=CC=1OC1=CC=CC=C1 MHCVCKDNQYMGEX-UHFFFAOYSA-N 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000002198 insoluble material Substances 0.000 description 2
- 229920000139 polyethylene terephthalate Polymers 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000002195 soluble material Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
- C08G63/785—Preparation processes characterised by the apparatus used
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0003—Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
- B01D5/0024—Rotating vessels or vessels containing movable parts
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyesters Or Polycarbonates (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US37168964A | 1964-06-01 | 1964-06-01 | |
| US623857A US3376353A (en) | 1964-06-01 | 1967-03-17 | Recovery of glycols from polyester production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO116966B true NO116966B (ko) | 1969-06-16 |
Family
ID=27005476
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO158282A NO116966B (ko) | 1964-06-01 | 1965-05-31 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US3376353A (ko) |
| JP (1) | JPS4927847B1 (ko) |
| BE (1) | BE664692A (ko) |
| CH (1) | CH461451A (ko) |
| DE (1) | DE1570975A1 (ko) |
| GB (1) | GB1074619A (ko) |
| IL (1) | IL23644A (ko) |
| LU (1) | LU48718A1 (ko) |
| NL (1) | NL6506904A (ko) |
| NO (1) | NO116966B (ko) |
| SE (1) | SE315580B (ko) |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL135611C (ko) * | 1961-07-24 | |||
| CH487345A (de) * | 1965-11-11 | 1970-03-15 | Karl Fischer App Und Rohrleitu | Verfahren zur Förderung eines dampfförmigen Stoffes und Anwendung dieses Verfahrens |
| JPS5128197A (en) * | 1974-09-03 | 1976-03-09 | Mitsubishi Chem Ind | Horiesuteruno seizohoho |
| DE2449162A1 (de) * | 1974-10-16 | 1976-04-22 | Basf Ag | Verfahren zur kontinuierlichen herstellung von linearen polyestern |
| DE2734946B2 (de) * | 1977-08-03 | 1980-09-25 | Basf Ag, 6700 Ludwigshafen | Verfahren und Vorrichtung zum Entfernen von flüchtigen Anteilen, die bei der Extrusion von Kunststoffschmelzen aus diesen entweichen |
| US5578173A (en) * | 1995-04-03 | 1996-11-26 | Eastman Kodak Company | Removal of dimethylterephthalate from a methanolysis vapor stream |
| JP3088311B2 (ja) * | 1996-11-19 | 2000-09-18 | 山形日本電気株式会社 | 充填塔式集塵装置 |
| US6538164B1 (en) * | 1999-09-30 | 2003-03-25 | E. I. Du Pont De Nemours And Company | Recovery process for volatile compounds from solids in aqueous solution |
| ES2540542T3 (es) * | 2000-12-07 | 2015-07-10 | Grupo Petrotemex, S.A. De C.V. | Procedimiento de poliéster de bajo coste que usa un reactor tubular |
| US6906164B2 (en) | 2000-12-07 | 2005-06-14 | Eastman Chemical Company | Polyester process using a pipe reactor |
| US7074879B2 (en) * | 2003-06-06 | 2006-07-11 | Eastman Chemical Company | Polyester process using a pipe reactor |
| US7135541B2 (en) | 2003-06-06 | 2006-11-14 | Eastman Chemical Company | Polyester process using a pipe reactor |
| US7332548B2 (en) * | 2004-03-04 | 2008-02-19 | Eastman Chemical Company | Process for production of a polyester product from alkylene oxide and carboxylic acid |
| US20080139780A1 (en) * | 2006-12-07 | 2008-06-12 | Debruin Bruce Roger | Polyester production system employing short residence time esterification |
| US7943094B2 (en) * | 2006-12-07 | 2011-05-17 | Grupo Petrotemex, S.A. De C.V. | Polyester production system employing horizontally elongated esterification vessel |
| US7649109B2 (en) * | 2006-12-07 | 2010-01-19 | Eastman Chemical Company | Polyester production system employing recirculation of hot alcohol to esterification zone |
| US7863477B2 (en) * | 2007-03-08 | 2011-01-04 | Eastman Chemical Company | Polyester production system employing hot paste to esterification zone |
| US7868130B2 (en) * | 2007-07-12 | 2011-01-11 | Eastman Chemical Company | Multi-level tubular reactor with vertically spaced segments |
| US7872089B2 (en) | 2007-07-12 | 2011-01-18 | Eastman Chemical Company | Multi-level tubular reactor with internal tray |
| US7868129B2 (en) * | 2007-07-12 | 2011-01-11 | Eastman Chemical Company | Sloped tubular reactor with spaced sequential trays |
| US7858730B2 (en) * | 2007-07-12 | 2010-12-28 | Eastman Chemical Company | Multi-level tubular reactor with dual headers |
| US7872090B2 (en) * | 2007-07-12 | 2011-01-18 | Eastman Chemical Company | Reactor system with optimized heating and phase separation |
| US7842777B2 (en) * | 2007-07-12 | 2010-11-30 | Eastman Chemical Company | Sloped tubular reactor with divided flow |
| US7829653B2 (en) * | 2007-07-12 | 2010-11-09 | Eastman Chemical Company | Horizontal trayed reactor |
| US7847053B2 (en) * | 2007-07-12 | 2010-12-07 | Eastman Chemical Company | Multi-level tubular reactor with oppositely extending segments |
| GB201317395D0 (en) * | 2013-10-01 | 2013-11-13 | Bulmer Duncan | Condenser |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2483254A (en) * | 1946-01-03 | 1949-09-27 | Atlas Powder Co | Production of dry sorbitol |
| US2793235A (en) * | 1954-09-27 | 1957-05-21 | Du Pont | Recovery of glycols from polyester production |
| US2883162A (en) * | 1955-12-13 | 1959-04-21 | Aluminium Lab Ltd | Condenser with rotary scraper |
| US3021831A (en) * | 1957-11-22 | 1962-02-20 | Jerome J Byrge | Furnace humidifier |
-
1965
- 1965-05-31 NO NO158282A patent/NO116966B/no unknown
- 1965-05-31 IL IL23644A patent/IL23644A/xx unknown
- 1965-05-31 LU LU48718D patent/LU48718A1/xx unknown
- 1965-05-31 BE BE664692D patent/BE664692A/xx unknown
- 1965-05-31 SE SE7099/65A patent/SE315580B/xx unknown
- 1965-06-01 JP JP40031982A patent/JPS4927847B1/ja active Pending
- 1965-06-01 NL NL6506904A patent/NL6506904A/xx unknown
- 1965-06-01 CH CH761965A patent/CH461451A/de unknown
- 1965-06-01 DE DE19651570975 patent/DE1570975A1/de active Pending
- 1965-06-01 GB GB23260/65A patent/GB1074619A/en not_active Expired
-
1967
- 1967-03-17 US US623857A patent/US3376353A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| LU48718A1 (ko) | 1965-12-01 |
| NL6506904A (ko) | 1965-12-02 |
| US3376353A (en) | 1968-04-02 |
| CH461451A (de) | 1968-08-31 |
| GB1074619A (en) | 1967-07-05 |
| DE1570975A1 (de) | 1970-02-19 |
| SE315580B (ko) | 1969-10-06 |
| IL23644A (en) | 1969-12-31 |
| JPS4927847B1 (ko) | 1974-07-22 |
| BE664692A (ko) | 1965-11-30 |
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