NL262812A - - Google Patents
Info
- Publication number
- NL262812A NL262812A NL262812DA NL262812A NL 262812 A NL262812 A NL 262812A NL 262812D A NL262812D A NL 262812DA NL 262812 A NL262812 A NL 262812A
- Authority
- NL
- Netherlands
- Prior art keywords
- nitro compound
- weight
- sulphuric acid
- solution
- nitro
- Prior art date
Links
- 150000002828 nitro derivatives Chemical class 0.000 abstract 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
- 239000000243 solution Substances 0.000 abstract 4
- 239000001117 sulphuric acid Substances 0.000 abstract 4
- 235000011149 sulphuric acid Nutrition 0.000 abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- 239000004215 Carbon black (E152) Substances 0.000 abstract 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 229930195733 hydrocarbon Natural products 0.000 abstract 3
- 150000002430 hydrocarbons Chemical class 0.000 abstract 3
- NJNQUTDUIPVROZ-UHFFFAOYSA-N nitrocyclohexane Chemical compound [O-][N+](=O)C1CCCCC1 NJNQUTDUIPVROZ-UHFFFAOYSA-N 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 2
- VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 abstract 2
- 238000006396 nitration reaction Methods 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- FEYJIFXFOHFGCC-UHFFFAOYSA-N 1-nitrohexane Chemical compound CCCCCC[N+]([O-])=O FEYJIFXFOHFGCC-UHFFFAOYSA-N 0.000 abstract 1
- BVALZCVRLDMXOQ-UHFFFAOYSA-N 1-nitropentane Chemical compound CCCCC[N+]([O-])=O BVALZCVRLDMXOQ-UHFFFAOYSA-N 0.000 abstract 1
- 239000008346 aqueous phase Substances 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000009903 catalytic hydrogenation reaction Methods 0.000 abstract 1
- 150000001924 cycloalkanes Chemical class 0.000 abstract 1
- 238000000354 decomposition reaction Methods 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 230000008014 freezing Effects 0.000 abstract 1
- 238000007710 freezing Methods 0.000 abstract 1
- 150000007529 inorganic bases Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 125000004971 nitroalkyl group Chemical group 0.000 abstract 1
- SKGLKPZSDNHVMF-UHFFFAOYSA-N nitrocyclooctane Chemical compound [O-][N+](=O)C1CCCCCCC1 SKGLKPZSDNHVMF-UHFFFAOYSA-N 0.000 abstract 1
- CJSZWOGCKKDSJG-UHFFFAOYSA-N nitrocyclopentane Chemical compound [O-][N+](=O)C1CCCC1 CJSZWOGCKKDSJG-UHFFFAOYSA-N 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/16—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/01—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to acyclic carbon atoms
- C07C205/02—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to acyclic carbon atoms of a saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/05—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US17482A US3035100A (en) | 1960-03-25 | 1960-03-25 | Process for the purification of nitrocyclohexane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NL262812A true NL262812A (show.php) |
Family
ID=21782828
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NL262812D NL262812A (show.php) | 1960-03-25 |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US3035100A (show.php) |
| GB (1) | GB916954A (show.php) |
| NL (1) | NL262812A (show.php) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3132183A (en) * | 1961-11-29 | 1964-05-05 | Commerical Solvents Corp | Process for the purification of nitrocyclohexane |
| WO2011049681A1 (en) * | 2009-10-20 | 2011-04-28 | Dow Global Technologies Inc. | Process for downstream recovery of nitroalkane using dividing wall column |
| US8415514B2 (en) * | 2009-10-20 | 2013-04-09 | Angus Chemical Company | Isothermal reactor for hydrocarbon nitration |
| JP5816184B2 (ja) | 2009-10-20 | 2015-11-18 | アンガス ケミカル カンパニー | ニトロ化反応器への水相のリサイクルによるニトロアルカン回収法 |
| CN102741217B (zh) | 2009-12-24 | 2015-04-15 | 陶氏环球技术有限责任公司 | 烃类进料灵活的高压硝化装置的设计 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2822393A (en) * | 1954-08-05 | 1958-02-04 | Olin Mathieson | Recovery of cyclohexanone oxime |
| US2822394A (en) * | 1954-08-05 | 1958-02-04 | Olin Mathieson | Recovery of cyclohexanone oxime |
-
0
- NL NL262812D patent/NL262812A/xx unknown
-
1960
- 1960-03-25 US US17482A patent/US3035100A/en not_active Expired - Lifetime
-
1961
- 1961-03-16 GB GB9692/61A patent/GB916954A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US3035100A (en) | 1962-05-15 |
| GB916954A (en) | 1963-01-30 |
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