MY151233A - Production of iron orthophosphate - Google Patents

Production of iron orthophosphate

Info

Publication number
MY151233A
MY151233A MYPI2011003397A MY151233A MY 151233 A MY151233 A MY 151233A MY PI2011003397 A MYPI2011003397 A MY PI2011003397A MY 151233 A MY151233 A MY 151233A
Authority
MY
Malaysia
Prior art keywords
iron
iii
solution
phosphoric
orthophosphate
Prior art date
Application number
Inventor
Bühler Gunnar
Schwarz Kilian
Original Assignee
Chem Fab Budenheim Kg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Fab Budenheim Kg filed Critical Chem Fab Budenheim Kg
Publication of MY151233A publication Critical patent/MY151233A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/37—Phosphates of heavy metals
    • C01B25/375—Phosphates of heavy metals of iron
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Nanotechnology (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Compounds Of Iron (AREA)
  • Battery Electrode And Active Subsutance (AREA)

Abstract

A PROCESS FOR THE PRODUCTION OF IRON (III) ORTHOPHOSPHATE OF THE GENERAL FORMULA FePO4 X nH2O (n ? 2.5) IN WHICH A) AN AQUEOUS SOLUTION CONTAINING Fe²? IONS IS PRODUCED IN THAT OXIDIC IRON (II), IRON (III) OR MIXED IRON (II, III) COMPOUNDS SELECTED FROM HYDROXIDES, OXIDES, OXIDE HYDROXIDES, OXIDE HYDRATES, CARBONATES AND HYDROXIDE CARBONATES, TOGETHER WITH ELEMENTARY IRON, ARE INTRODUCED INTO A PHOSPHORIC ACID-BEARING AQUEOUS MEDIUM, AND Fe²? IONS ARE DISSOLVED AND Fe³? IS REACTED WITH ELEMENTARY Fe (IN A COMPROPORTIONATION REACTION) TO GIVE Fe²?, B) SOLIDS ARE SEPARATED FROM THE PHOSPHORIC-ACID AQUEOUS Fe²? SOLUTION, AND C) AN OXIDATION AGENT IS ADDED TO THE PHOSPHORIC-ACID AQUEOUS Fe²? SOLUTION TO OXIDISE IRON (II) IN THE SOLUTION AND IRON (III) ORTHOPHOSPHATE OF THE GENERAL FORMULA FePO4 X nH2O PRECIPITATES.
MYPI2011003397 2009-02-26 2010-02-19 Production of iron orthophosphate MY151233A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102009001204A DE102009001204A1 (en) 2009-02-26 2009-02-26 Production of iron orthophosphate

Publications (1)

Publication Number Publication Date
MY151233A true MY151233A (en) 2014-04-30

Family

ID=42288666

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI2011003397 MY151233A (en) 2009-02-26 2010-02-19 Production of iron orthophosphate

Country Status (16)

Country Link
US (1) US8574518B2 (en)
EP (1) EP2401228B1 (en)
JP (1) JP5748146B2 (en)
KR (1) KR101690141B1 (en)
CN (1) CN102333725B (en)
AU (1) AU2010217661B2 (en)
BR (1) BRPI1009769A2 (en)
CA (1) CA2747646C (en)
DE (1) DE102009001204A1 (en)
ES (1) ES2599972T3 (en)
IL (1) IL214044A (en)
MX (1) MX2011008607A (en)
MY (1) MY151233A (en)
RU (1) RU2530126C2 (en)
SG (1) SG172357A1 (en)
WO (1) WO2010097341A1 (en)

Families Citing this family (44)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI466370B (en) 2008-01-17 2014-12-21 A123 Systems Inc Hybrid metal olivine electrode material for lithium ion battery
US9178215B2 (en) 2009-08-25 2015-11-03 A123 Systems Llc Mixed metal olivine electrode materials for lithium ion batteries having improved specific capacity and energy density
WO2011030786A1 (en) * 2009-09-09 2011-03-17 戸田工業株式会社 Ferric phosphate hydrate particle powder and process for production thereof, olivine-type lithium iron phosphate particle powder and process for production thereof, and non-aqueous electrolyte secondary battery
US9660267B2 (en) 2009-09-18 2017-05-23 A123 Systems, LLC High power electrode materials
TWI496737B (en) * 2009-09-18 2015-08-21 A123 Systems Llc Ferric phosphate and methods of preparation thereof
DE102011003125A1 (en) * 2011-01-25 2012-07-26 Chemische Fabrik Budenheim Kg Iron (III) orthophosphate-carbon composite
CN102263236B (en) * 2011-06-17 2013-07-31 山东轻工业学院 Preparation method of meso-porous spherical lithium iron phosphate/carbon in-situ composite material
KR101893955B1 (en) * 2011-12-16 2018-09-03 삼성에스디아이 주식회사 Metal doped crystalline iron phosphate, method for preparation thereof and lithium composite metal phosphorus oxide prepared using the same
DE102011056812A1 (en) * 2011-12-21 2013-06-27 Chemische Fabrik Budenheim Kg Metal phosphates and process for their preparation
DE102011056815A1 (en) 2011-12-21 2013-08-01 Chemische Fabrik Budenheim Kg Nutrient composition for biological systems
DE102011056816A1 (en) 2011-12-21 2013-08-01 Chemische Fabrik Budenheim Kg Manganese-containing metal phosphates and process for their preparation
CN102530905B (en) * 2011-12-22 2014-09-03 浙江天能能源科技有限公司 Preparation method of nano-FePO4 with controllable particle size
DE102012100128A1 (en) * 2012-01-10 2013-07-11 Chemische Fabrik Budenheim Kg Condensed iron (III) phosphates
CN102867954B (en) * 2012-09-13 2014-09-24 清华大学 Method for synthesizing lithium iron phosphate anode material by adopting emulsion liquid phase
CN103058160A (en) * 2012-11-06 2013-04-24 浙江南都电源动力股份有限公司 Preparation method of low cost battery level iron phosphate based on ferrous powder corrosion
DE102013206007A1 (en) 2013-04-04 2014-10-09 Chemische Fabrik Budenheim Kg Amorphized iron (III) phosphate
CN103274383B (en) * 2013-05-20 2015-07-15 南京大学 Shape-controlled battery grade iron phosphate and preparation method thereof
EP3114081B1 (en) * 2014-03-07 2021-12-29 A123 Systems LLC High power electrode materials
DE102014118907A1 (en) 2014-12-17 2016-06-23 Chemische Fabrik Budenheim Kg For the preparation of cathodes for Li-ion batteries suitable phosphate compounds
EP3377443A2 (en) * 2015-11-19 2018-09-26 Qatar Foundation For Education Science And Community Development Orthophosphate electrodes for rechargeable batteries
DE102017106912A1 (en) * 2017-03-30 2018-10-04 Chemische Fabrik Budenheim Kg Process for the preparation of Fe (II) P / Fe (II) MetP compounds
CN108101014A (en) * 2018-01-31 2018-06-01 贵州仁聚业科技股份有限公司 The method for preparing ferric phosphate with yellow phosphorus by-product ferrophosphorus slag
CN108557795A (en) * 2018-03-08 2018-09-21 蒋央芳 A kind of preparation method of LiFePO4
CN108529582A (en) * 2018-03-28 2018-09-14 纽迈（常州）新材料有限公司 A kind of clean preparation method of ferric orthophosphate
WO2019219250A1 (en) * 2018-05-15 2019-11-21 Sicpa Holding Sa Machine readable security features
CN109775679B (en) * 2019-04-01 2022-03-18 中钢集团南京新材料研究院有限公司 Preparation method of iron phosphate for high-purity high-compaction lithium iron phosphate
CN110342485A (en) * 2019-08-06 2019-10-18 贵州开瑞科技有限公司 A kind of battery-grade iron phosphate alkali-free formula production method
CN110294466B (en) * 2019-08-19 2020-11-17 四川轻化工大学 Preparation method of nano flaky iron phosphate
CN112408351A (en) * 2020-11-23 2021-02-26 中钢集团南京新材料研究院有限公司 Preparation method of high-compaction iron phosphate and lithium iron phosphate
CN112573497A (en) * 2020-11-23 2021-03-30 湖南雅城新材料有限公司 Method for preparing iron phosphate by using ferric oxide
CN113603071B (en) * 2021-07-23 2023-11-03 广东邦普循环科技有限公司 Nanosheet iron phosphate and preparation method and application thereof
CN113666351B (en) * 2021-08-31 2023-12-12 广东邦普循环科技有限公司 Method for preparing ferric phosphate by recycling ferronickel slag
CN115806279B (en) 2021-09-15 2024-10-11 贵州川恒化工股份有限公司 A method for preparing ferric phosphate using iron-containing waste
CN114162795B (en) * 2021-11-08 2023-07-11 江苏涛立电子新材料有限公司 Nanometer ferric phosphate for synthesizing lithium battery anode material and preparation method thereof
CN114702016A (en) * 2022-03-30 2022-07-05 昆明理工大学 Method for preparing iron phosphate by using phosphorus iron slag as by-product in yellow phosphorus production
CN116924365A (en) 2022-04-08 2023-10-24 黄冈林立新能源科技有限公司 Method for preparing ferric phosphate dihydrate by decomplexing ferric phosphate complex
CN115285959B (en) * 2022-07-06 2023-06-06 宜宾天原海丰和泰有限公司 Method for continuously producing ferric phosphate at low cost
CN115231538B (en) * 2022-07-06 2023-09-26 曲靖市德方纳米科技有限公司 Preparation method and application of ferrophosphorus source
CN115676790B (en) * 2022-10-28 2024-04-02 贵州川恒化工股份有限公司 Preparation method of high-tap-density spherical battery-grade ferric phosphate
CN115818603B (en) * 2022-12-02 2024-03-12 湖南顺华锂业有限公司 Method for preparing battery grade ferric phosphate from lithium iron phosphate anode powder containing copper, aluminum and graphite through oxidizing and extracting lithium from residue
CN115974029B (en) * 2023-02-18 2025-05-02 宜昌邦普循环科技有限公司 Anhydrous iron phosphate and preparation method thereof and lithium iron phosphate positive electrode material
CN116902946B (en) * 2023-09-14 2023-11-14 北京林立新能源有限公司 Method for preparing ferric phosphate from iron black
CN117623255A (en) * 2023-10-19 2024-03-01 贵州雅友新材料有限公司 Preparation method of flaky ferric phosphate
WO2026000062A1 (en) * 2024-06-25 2026-01-02 Nano One Materials Corp. Manufacture of high purity fepo4 from elemental iron and lifepo4 formed therefrom

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2414974A (en) * 1943-08-30 1947-01-28 Monsanto Chemicals Production of ferric orthophosphate
US3070423A (en) * 1960-10-17 1962-12-25 Chemetron Corp Preparation of white iron phosphate
US3407034A (en) 1965-06-16 1968-10-22 Pfizer & Co C White iron phosphate
SU670535A1 (en) * 1977-12-19 1979-06-30 Белорусский технологический институт им. С.М.Кирова Method of producing trisubstituted ferrum orthophosphate
SU1549916A1 (en) * 1986-12-10 1990-03-15 Белорусский технологический институт им.С.М.Кирова Method of obtaining iron iii hydrophosphates
US5437870A (en) * 1994-08-25 1995-08-01 W. Neudorff Gmbh Kg Ingestible mollusc poisons
EA000483B1 (en) * 1996-06-14 1999-08-26 Дзнеладзе, Давид Эльдарович Phosphate composition and its utilization
WO2000060679A1 (en) * 1999-04-06 2000-10-12 Sony Corporation Method for manufacturing active material of positive plate and method for manufacturing nonaqueous electrolyte secondary cell
CA2320661A1 (en) * 2000-09-26 2002-03-26 Hydro-Quebec New process for synthesizing limpo4 materials with olivine structure
FR2815027B1 (en) 2000-10-11 2002-12-27 Rhodia Chimie Sa PROCESS FOR THE PREPARATION OF AN IRON PHOSPHATE AND AN ALKALINE
US6645452B1 (en) * 2000-11-28 2003-11-11 Valence Technology, Inc. Methods of making lithium metal cathode active materials
US6498119B2 (en) * 2000-12-29 2002-12-24 University Of Chicago Chemically bonded phosphate ceramics of trivalent oxides of iron and manganese
US6835500B2 (en) * 2001-10-02 2004-12-28 Rutgers University Hydrated iron phosphate electrode materials for rechargeable lithium battery cell systems
US7690387B2 (en) * 2004-10-25 2010-04-06 Philip Morris Usa Inc. Synthesis and incorporation of high-temperature ammonia-release agents in lit-end cigarettes
FI119804B (en) * 2007-09-07 2009-03-31 Maping Ky L Huotari Method and device for making a folder
DE102007049757A1 (en) * 2007-10-16 2009-04-23 Chemische Fabrik Budenheim Kg Iron (III) orthophosphate for Li-ion batteries
CN101237043A (en) * 2008-01-31 2008-08-06 东北师范大学 Method for preparing lithium iron phosphate/carbon composite material with highly active disordered iron phosphate
CN100595949C (en) * 2008-02-26 2010-03-24 郑州瑞普生物工程有限公司 Method for making positive material positive ferric phosphate of lithium battery

Also Published As

Publication number Publication date
SG172357A1 (en) 2011-07-28
HK1164262A1 (en) 2012-09-21
CN102333725A (en) 2012-01-25
US8574518B2 (en) 2013-11-05
WO2010097341A1 (en) 2010-09-02
RU2011139174A (en) 2013-07-10
US20120039783A1 (en) 2012-02-16
DE102009001204A1 (en) 2010-09-02
EP2401228A1 (en) 2012-01-04
AU2010217661B2 (en) 2013-01-17
CN102333725B (en) 2014-04-09
ES2599972T3 (en) 2017-02-06
IL214044A (en) 2015-07-30
KR20110139190A (en) 2011-12-28
BRPI1009769A2 (en) 2016-03-15
IL214044A0 (en) 2011-08-31
JP2012518594A (en) 2012-08-16
KR101690141B1 (en) 2016-12-27
RU2530126C2 (en) 2014-10-10
MX2011008607A (en) 2011-09-09
CA2747646C (en) 2017-08-22
CA2747646A1 (en) 2010-09-02
JP5748146B2 (en) 2015-07-15
EP2401228B1 (en) 2016-09-14
AU2010217661A1 (en) 2011-09-08

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