MX2019010520A - Metodo de sintesis continua de cristales de zeolita. - Google Patents

Metodo de sintesis continua de cristales de zeolita.

Info

Publication number
MX2019010520A
MX2019010520A MX2019010520A MX2019010520A MX2019010520A MX 2019010520 A MX2019010520 A MX 2019010520A MX 2019010520 A MX2019010520 A MX 2019010520A MX 2019010520 A MX2019010520 A MX 2019010520A MX 2019010520 A MX2019010520 A MX 2019010520A
Authority
MX
Mexico
Prior art keywords
zeolite crystals
continuous
continuous synthesis
composition
reynolds number
Prior art date
Application number
MX2019010520A
Other languages
English (en)
Inventor
Dubois Jean-Luc
Lutz Cécile
Nicolas Serge
Lecomte Yvan
Original Assignee
Arkema France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France filed Critical Arkema France
Publication of MX2019010520A publication Critical patent/MX2019010520A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/023Preparation of physical mixtures or intergrowth products of zeolites chosen from group C01B39/04 or two or more of groups C01B39/14 - C01B39/48
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/14Type A
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/20Faujasite type, e.g. type X or Y
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/20Faujasite type, e.g. type X or Y
    • C01B39/22Type X
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/26Mordenite type
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/30Erionite or offretite type, e.g. zeolite T
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C01B39/38Type ZSM-5
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46Other types characterised by their X-ray diffraction pattern and their defined composition

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

La presente invención se refiere a un método para la preparación continua de cristales de zeolita, que comprende la introducción continua de una composición capaz de generar cristales de zeolita en al menos una zona de reacción de cristalización sometida a medios de agitación, proporcionando a la composición un flujo caracterizado por un número relativo de Reynolds Rer comprendido entre 40 y 50000, y la recuperación continua de los cristales formados según un flujo caracterizado por un número neto de Reynolds Ren comprendido entre 1 y 1500.
MX2019010520A 2017-03-17 2018-03-12 Metodo de sintesis continua de cristales de zeolita. MX2019010520A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1752196A FR3063993B1 (fr) 2017-03-17 2017-03-17 Procede de synthese en continu de cristaux de zeolithe
PCT/FR2018/050568 WO2018167414A1 (fr) 2017-03-17 2018-03-12 Procédé de synthèse en continu de cristaux de zéolithe

Publications (1)

Publication Number Publication Date
MX2019010520A true MX2019010520A (es) 2019-10-17

Family

ID=59253648

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019010520A MX2019010520A (es) 2017-03-17 2018-03-12 Metodo de sintesis continua de cristales de zeolita.

Country Status (11)

Country Link
US (1) US11040884B2 (es)
EP (1) EP3596010A1 (es)
JP (1) JP6910462B2 (es)
KR (1) KR102292496B1 (es)
CN (1) CN110446683B (es)
EA (1) EA039224B1 (es)
FR (1) FR3063993B1 (es)
MX (1) MX2019010520A (es)
TW (1) TWI672271B (es)
WO (1) WO2018167414A1 (es)
ZA (1) ZA201905751B (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117529451A (zh) * 2021-06-14 2024-02-06 巴斯夫欧洲公司 以脉动流态在连续流反应器中进行的沸石合成
CN113401919A (zh) * 2021-07-23 2021-09-17 南京工业大学 一种连续制备fau-lta共晶分子筛工艺
FR3141080A1 (fr) 2022-10-19 2024-04-26 Arkema France Procédé de synthèse de zéolithe zsm-5 en continu

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1357762A (fr) 1963-02-27 1964-04-10 Pernod & Ricard Perfectionnements aux procédés de préparation de jus de fruits et de légumes et notamment de jus de raisin
FR2398698A1 (fr) * 1977-07-29 1979-02-23 Ugine Kuhlmann Procede industriel de fabrication en continu de zeolithe a
US4368174A (en) * 1980-12-29 1983-01-11 Mobil Oil Corporation Apparatus for a continuous down-flow zeolite production
FR2552070B1 (fr) * 1983-09-21 1987-09-11 Rhone Poulenc Chim Base Procede d'obtention d'une zeolite par alimentation en continu d'une solution aqueuse de silicate de sodium et d'une solution aqueuse d'aluminate de sodium, produit obtenu et application du produit a la detergence
DE3728601C1 (de) 1987-08-27 1988-09-29 Daimler Benz Ag Zentralverriegelungsanlage fuer Tuer- und Deckelverschluesse eines Kraftfahrzeugs
FR2750893B1 (fr) 1996-07-12 1998-10-30 Elf Aquitaine Procede de synthese de zeolithe avec agitation homogene du milieu, dispositif et application
US6656447B1 (en) 1998-12-29 2003-12-02 Uop Llc Process for synthesizing and controlling the particle size and particle size distribution of a molecular sieve
US6521208B1 (en) * 1999-03-03 2003-02-18 Pq Corporation Process for preparing a modified zeolite
US6773694B1 (en) 1999-12-22 2004-08-10 Uop Llc Process for synthesizing molecular sieves
JP2002068731A (ja) * 2000-08-23 2002-03-08 Akio Henmi 人工ゼオライトの製造方法およびその製造装置
JP3502831B2 (ja) * 2000-12-15 2004-03-02 敏雄 霜田 接触反応管・回転ディスク反応器方式によるゼオライトの連続製造方法および連続製造装置
US7528089B2 (en) * 2003-12-30 2009-05-05 Exxonmobil Research And Engineering Company High solids materials processing
JP4580321B2 (ja) * 2005-10-07 2010-11-10 敏雄 霜田 高機能ゼオライトの連続合成方法
GB0523707D0 (en) 2005-11-22 2005-12-28 Nitech Solutions Ltd Improved apparatus and method for temperature controlled processes
KR101047626B1 (ko) 2010-12-31 2011-07-07 신완숙 인공 제올라이트 제조장치 및 제조방법
JP7134099B2 (ja) * 2016-06-17 2022-09-09 ビーエーエスエフ ソシエタス・ヨーロピア ゼオライト材料の連続合成のための方法
FR3063996B1 (fr) * 2017-03-17 2022-01-14 Arkema France Procede de synthese de cristaux de zeolithe avec agent d'ensemencement

Also Published As

Publication number Publication date
TW201838920A (zh) 2018-11-01
KR102292496B1 (ko) 2021-08-20
EA039224B1 (ru) 2021-12-20
FR3063993B1 (fr) 2022-02-04
EA201992194A1 (ru) 2020-02-05
ZA201905751B (en) 2021-01-27
JP2020510604A (ja) 2020-04-09
CN110446683B (zh) 2023-04-25
JP6910462B2 (ja) 2021-07-28
EP3596010A1 (fr) 2020-01-22
WO2018167414A1 (fr) 2018-09-20
US20200010330A1 (en) 2020-01-09
CN110446683A (zh) 2019-11-12
TWI672271B (zh) 2019-09-21
FR3063993A1 (fr) 2018-09-21
US11040884B2 (en) 2021-06-22
KR20190125378A (ko) 2019-11-06

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