MX2008007109A - Soap composition with encapsulates - Google Patents
Soap composition with encapsulatesInfo
- Publication number
- MX2008007109A MX2008007109A MXMX/A/2008/007109A MX2008007109A MX2008007109A MX 2008007109 A MX2008007109 A MX 2008007109A MX 2008007109 A MX2008007109 A MX 2008007109A MX 2008007109 A MX2008007109 A MX 2008007109A
- Authority
- MX
- Mexico
- Prior art keywords
- soap
- bar
- clause
- encapsulation
- density
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 38
- 239000000344 soap Substances 0.000 title claims description 38
- 230000002209 hydrophobic Effects 0.000 claims abstract description 4
- 238000005538 encapsulation Methods 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- 229940095696 Soap Product Drugs 0.000 claims description 14
- 239000004094 surface-active agent Substances 0.000 claims description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 8
- 150000001298 alcohols Chemical class 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 7
- TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims description 6
- QIQXTHQIDYTFRH-UHFFFAOYSA-N Stearic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 6
- 239000000049 pigment Substances 0.000 claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 5
- SZXQTJUDPRGNJN-UHFFFAOYSA-N Dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims description 4
- -1 lauryl disodium sulfosuccinate Chemical compound 0.000 claims description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 4
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 3
- 240000007170 Cocos nucifera Species 0.000 claims description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 3
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 3
- 108010010803 Gelatin Proteins 0.000 claims description 3
- 235000021360 Myristic acid Nutrition 0.000 claims description 3
- 235000021355 Stearic acid Nutrition 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 239000008273 gelatin Substances 0.000 claims description 3
- 229920000159 gelatin Polymers 0.000 claims description 3
- 235000019322 gelatine Nutrition 0.000 claims description 3
- 235000011852 gelatine desserts Nutrition 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 239000011780 sodium chloride Substances 0.000 claims description 3
- 239000000600 sorbitol Substances 0.000 claims description 3
- 235000010356 sorbitol Nutrition 0.000 claims description 3
- 239000008117 stearic acid Substances 0.000 claims description 3
- 235000000346 sugar Nutrition 0.000 claims description 3
- SVTBMSDMJJWYQN-UHFFFAOYSA-N 2-Methyl-2,4-pentanediol Chemical compound CC(O)CC(C)(C)O SVTBMSDMJJWYQN-UHFFFAOYSA-N 0.000 claims description 2
- ZQBJRVYLUFBBEQ-UHFFFAOYSA-N 2-[diamino(3-formamidopropyl)azaniumyl]acetate Chemical compound [O-]C(=O)C[N+](N)(N)CCCNC=O ZQBJRVYLUFBBEQ-UHFFFAOYSA-N 0.000 claims description 2
- FBPFZTCFMRRESA-KAZBKCHUSA-N D-Mannitol Natural products OC[C@@H](O)[C@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KAZBKCHUSA-N 0.000 claims description 2
- FBPFZTCFMRRESA-KVTDHHQDSA-N Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims description 2
- 239000004264 Petrolatum Substances 0.000 claims description 2
- 229940066842 Petrolatum Drugs 0.000 claims description 2
- HEBKCHPVOIAQTA-SCDXWVJYSA-N Xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims description 2
- 229960002675 Xylitol Drugs 0.000 claims description 2
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 2
- 229940110456 cocoa butter Drugs 0.000 claims description 2
- 235000019868 cocoa butter Nutrition 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- 229940051250 hexylene glycol Drugs 0.000 claims description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 2
- 239000000594 mannitol Substances 0.000 claims description 2
- 235000010355 mannitol Nutrition 0.000 claims description 2
- 239000011707 mineral Substances 0.000 claims description 2
- 235000019271 petrolatum Nutrition 0.000 claims description 2
- 229940057950 sodium laureth sulfate Drugs 0.000 claims description 2
- 159000000000 sodium salts Chemical class 0.000 claims description 2
- 150000008163 sugars Chemical class 0.000 claims description 2
- 239000000811 xylitol Substances 0.000 claims description 2
- 235000010447 xylitol Nutrition 0.000 claims description 2
- 239000012071 phase Substances 0.000 claims 6
- 229940057910 Shea butter Drugs 0.000 claims 2
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims 2
- 241001135917 Vitellaria paradoxa Species 0.000 claims 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N D-sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims 1
- CZMRCDWAGMRECN-GDQSFJPYSA-N Sucrose Natural products O([C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O1)[C@@]1(CO)[C@H](O)[C@@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-GDQSFJPYSA-N 0.000 claims 1
- 239000008384 inner phase Substances 0.000 claims 1
- 239000005720 sucrose Substances 0.000 claims 1
- 230000005484 gravity Effects 0.000 abstract description 6
- 238000009826 distribution Methods 0.000 abstract description 2
- 239000000725 suspension Substances 0.000 abstract 1
- 239000002585 base Substances 0.000 description 29
- 239000000047 product Substances 0.000 description 22
- 239000011859 microparticle Substances 0.000 description 8
- 239000004615 ingredient Substances 0.000 description 7
- 238000009472 formulation Methods 0.000 description 6
- 239000003906 humectant Substances 0.000 description 6
- 239000003349 gelling agent Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 3
- 239000000375 suspending agent Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 210000003491 Skin Anatomy 0.000 description 2
- 229920000591 gum Polymers 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- 230000000699 topical Effects 0.000 description 2
- 238000009827 uniform distribution Methods 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N Iron(III) oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L Sulphite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
- 229940029983 VITAMINS Drugs 0.000 description 1
- 229940021016 Vitamin IV solution additives Drugs 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 229910001508 alkali metal halide Inorganic materials 0.000 description 1
- 150000008045 alkali metal halides Chemical class 0.000 description 1
- 229910052936 alkali metal sulfate Inorganic materials 0.000 description 1
- 239000002280 amphoteric surfactant Substances 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 239000004599 antimicrobial Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000014121 butter Nutrition 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 238000001647 drug administration Methods 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N edta Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 229910000460 iron oxide Inorganic materials 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 150000004668 long chain fatty acids Chemical class 0.000 description 1
- 229960001855 mannitol Drugs 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 150000004667 medium chain fatty acids Chemical class 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L na2so4 Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000002335 preservative Effects 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000002285 radioactive Effects 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000005063 solubilization Methods 0.000 description 1
- 229960002920 sorbitol Drugs 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002194 synthesizing Effects 0.000 description 1
- 230000002588 toxic Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229930003231 vitamins Natural products 0.000 description 1
Abstract
A personal care composition comprising a product base with at least one encapsulate dispersed throughout is disclosed. The at least one encapsulate contains a hydrophobic internal phase comprising a density-modifying agent such that the specific gravity of the solution is adjusted to provide for suspension and distribution of the at least one encapsulate throughout the product base.
Description
COMPOSITION OF SOAP WITH ENCAPSULATED
CROSS REFERENCE TO RELATED REQUESTS
This application claims the priority of the United States provisional patent application serial number 60 / 752,345, filed on December 21, 2005, the contents of which are incorporated herein by reference.
BACKGROUND OF THE INVENTION
Liquid personal care compositions, including soaps and body cleansers, containing encapsulates, or suspended microparticles, are known in the art. These compositions containing suspended or encapsulated microparticles typically have a gel type rheology and are suspended in solution by a gelling agent or other suspending agent. These agents are used to provide a uniform distribution of the suspended or encapsulated microparticles within the product base. In addition to the suspension or gelling agent, adjustments can also be made in the viscosity of the liquid formulation to establish a uniform distribution. In non-liquid products, which are
Substantially solid at room temperature and liquids at higher temperatures, the product must remain molten and diluted to process and fill the product molds or castings, so the addition of a gelling agent to suspend the microparticles or encapsulates or the viscosity adjustment. When the microparticles or encapsulates are added to a molten product that does not contain a suspending or gelling agent, the microparticles will be added in the upper part or in the lower part of the solution, depending on the specific gravity.
Therefore, there is a need for a personal care composition comprising a microparticle or encapsulation that can be used in a molten product formulation wherein the specific gravity is such that the microparticle or encapsulation remains suspended in the product base and is distributed evenly throughout the formulation.
SYNTHESIS OF THE INVENTION
The present invention is a solid soap composition comprising a soap product base and encapsulates which are suspended in the product base of
soap, where the encapsulates have basically the same density as that of the soap product base. In one embodiment, the encapsulates contain a pigment, for example, a pigment derived from ore, which increases the density of the encapsulation. By adjusting the density ratio of the encapsulation to match the density of the soap product base, the encapsulates can be distributed throughout the product base.
The invention therefore provides, in one embodiment, a soap bar of Formula I comprising:
(i) a soap product base; Y
(ii) at least one encapsulation comprising an internal phase with a density modifying agent in a hydrophobic phase, the internal phase being surrounded by an external phase;
wherein (i) the ratio of the density of at least one encapsulation and the density of the soap base is from 97: 100 to 103: 100, preferably 99: 100 and 101: 100; and (ii)
the at least one encapsulate is distributed in the soap product base.
The soap product base is preferably a clear or translucent composition. For example, in addition to soap (eg, potassium and / or sodium salts of long and medium chain fatty acids, eg, stearic acid, myristic acid and / or coconut acid), it may comprise: additional surfactants (e.g. , anionic, cationic, nonionic or sutionionic surfactants, for example, sulfate and / or sulfonate surfactants, for example, sodium lauryl sulfate, sodium laureth sulfate, lauryl disodium sulfosuccinate, as well as cocamidopropyl betaine), as well as water and humectants, example, polyhydric alcohols (for example, glycerol, propylene glycol, dipropylene glycol, sugar alcohols and sugars). See, for example, U.S. Patent 6,838,420 incorporated herein by reference.
The encapsulates have an average diameter of, for example, about 100 to about 2000 microns, for example about 600 and about 1000 microns. In one embodiment, the external phase of the encapsulation is gelatin gum, for example, a mixture of fish gelatin and Arabian gum, and the internal phase comprises a semi-solid oil,
preferably a substance that provides a benefit to the skin, for example, kapté butter, cocoa butter or petrolatum. The semi-solid oil can be mixed with the pigment
(for example, titanium dioxide where white is desired, ferric oxide where ro is preferred, ultramarine base for blue, etc.) before encapsulation to achieve the desired density. The encapsulation may optionally comprise other materials, for example, fragrances, vitamins, etc., provided that the final mixture is such that the density of the encapsulation is equal to that of the base during the manufacturing process.
DETAILED DESCRIPTION OF THE INVENTION
The present invention is directed to a soap composition comprising a soap product base and dispersed encapsulates within the product base. Adjustments are made in the specific gravity of the composition so that the encapsulates are dispersed throughout the product base.
The compositions as provided herein are described and claimed with reference to their ingredients, as is usual in the art. As will be evident to one with skill
in the art, the ingredients may sometimes react with one another, so that the authentic composition of the final formulation may not correspond exactly with the ingredients listed. Therefore, it should be understood that the invention extends to the product of the combination of the listed ingredients.
All the ingredients for use herein are preferably cosmetically acceptable. By "cosmetically acceptable" is meant suitable for use in a topical application formulation on human skin. A cosmetically acceptable excipient, for example, is an excipient that is suitable for external application in the amounts and concentrations provided in the formulations of this invention, and includes for example excipients that are "Generally Recognized as Safe" (GRAS) by Drug Administration. and Food from the United States. Preferably, heavy metals, radioactive elements and other materials that one skilled in the art would consider reasonably toxic for topical administration in the amounts envisaged are excluded.
The soap composition of the present invention comprises a product base and one or more encapsulates in the
product base. The soap product base is a soap-based composition containing soap, surfactants and water, and may include additional elements such as a humectant, an alcohol or desired aesthetic additives such as a fragrance or a humectant.
The encapsulates of the present invention have an internal hydrophobic phase. The internal phase contains a density modifying agent and a carrier agent to provide ease of distribution of the density modifying agent. Suitable density modifying agents include metal oxides and other pigments made from mineral powders, since they are relatively heavy. Titanium dioxide is a pigment used in the preferred embodiment as a density modifying agent. Other density modifying agents can be used in the composition, if such agents impart the desired density of the encapsulate and the specific gravity of the composition. By varying the amount of the density modifying agent in the encapsulation, the specific gravity is adjusted so that the encapsulation can be evenly distributed across the product base.
The product base of the present invention preferably comprises a soap, surfactant, structuring agent and water.
In one embodiment, the soap product base comprises salts of fatty acids selected from stearic acid, myristic acid and coconut acid. Examples of additional surfactants that may be present in the soap composition include anionic, amphoteric, nonionic and cationic surfactants. The amount of soap is about 3% to about 40% by weight, or about 10% to about 30%. The additional surfactant is present in the soap composition in an amount by weight of about 4% to about 40%.
A structurant can be used in the product base as a substance to make the soap composition harder. Structures such as alkali metal halides and alkali metal sulfates, including sodium chloride and sodium sulfate, are preferred. Structuring levels can be from 0% to around 5% by weight, or from around 0.5% to around 1.5%.
Optionally, a gelling agent can be used in the product base to increase the hardness of the bar.
A humectant can be added to the product base to aid in the solubilization of the soap. Such humectants include polyhydric alcohols such as propylene glycol, dipropylene glycol, glycepine, sorbitol, mannitol, xylitol and hexylene glycol.
Optional ingredients that may be present in the product base include fragrances, dyes, chelating agents such as EDTA, antimicrobial agents, humectants and preservatives.
The bars can be prepared by standard procedures. The bars are prepared by means of pressing (molding) or pouring (pouring) methods, for example, by placing a liquid in a mold.
The examples and other statements on preferred ingredients, formulations and utilities are intended to illustrate rather than limit the invention.
The percentages described in the examples below are percentages by weight based on the total formulation of the specific component of the soap composition as 100%. For example, in the example of the Product Base, the soap is present in an amount by weight of about 10 / a about 30% of the composition of the Product Base, not of the total composition of the product. j fertilizer
Therefore, the invention provides in a particular embodiment, a bar of soap according to Formula 1 above, as follows:
Soap Product Base comprising
Internal phase comprising
External phase comprising
Composition of the soap bar
fifteen
twenty
Examples of representative formulations are as follows
Claims (15)
1. A bar of soap that includes: (a) a soap product base; and (b) at least one encapsulation comprising an internal phase having a density modifying agent in a hydrophobic phase, the inner phase being surrounded by an external phase; wherein (i) the ratio of the density of the at least one encapsulation to the density of the soap base is from 97: 100 to 103: 100 and (ii) the at least one encapsulation is distributed on the basis of soap product.
2. The soap bar as claimed in clause 1, characterized in that at least one encapsulation independently has an average diameter of about 100 to about 2000 microns.
3. The bar of soap as claimed in clause 1, characterized because the external phase of the at least one encapsulation comprises gelatin and the internal phase contains a semi-solid oil.
4. The bar of soap as claimed in clause 3, characterized in that the semi-solid oil comprises an agent selected from the group consisting of shea butter, cocoa butter and petrolatum.
5. The bar of soap as claimed in clause 1, characterized in that the at least one encapsulation comprises a density modifying agent.
6. The bar of soap as claimed in clause 1, characterized in that the density-modifying agent is a mineral-based pigment.
7. The bar of soap as claimed in clause 1, characterized in that the density modifying agent comprises 5-10% by weight of the internal phase.
8. The bar of soap as claimed in clause 1, characterized in that the soap product base is transparent or translucent.
9. The bar of soap as claimed in clause 4, characterized in that the semi-solid oil comprises shea butter.
10. The bar of soap as claimed in clause 1, characterized in that the product base of j abón comprises: a) a sodium salt of a fatty acid selected from the group consisting of stearic acid, myristic acid and coconut acid, in an amount by weight of from about 10% to about 30%; b) additional surfactants, in an amount by weight of from about 10% to about 25%; c) polyhydric alcohols, in an amount by weight of about 15% to about 30%.
11. The bar of soap as claimed in clause 10, characterized in that the polyhydric alcohols comprise one or more polyhydric alcohols selected from the group consisting of glycerin, propylene glycol, dipropylene glycol, sorbitol, mannitol, xylitol, hexylene glycol, sugars and mixtures thereof.
12. The bar of soap as claimed in clause 11, characterized in that the polyhydric alcohols are selected from one or more of the group consisting of glycerin, propylene glycol, dipropylene glycol, sorbitol, sucrose and mixtures thereof.
13. The bar of soap as claimed in clause 10, characterized in that the additional surfactants comprise one or more surfactants selected from the group consisting of sodium laureth sulfate, cocamidopropyl betaine, lauryl disodium sulfosuccinate and mixtures thereof.
14. The bar of soap as claimed in clause 10, characterized in that the soap product base further comprises a structuring component in an amount of up to about 5% by weight.
15. The bar of soap as claimed in clause 13, characterized in that the structuring component comprises sodium chloride.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US60/752,345 | 2005-12-21 | ||
US11457520 | 2006-07-14 |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2008007109A true MX2008007109A (en) | 2008-09-02 |
Family
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