MX165977B - Separaciones cromatograficas continuas en un lecho fluidizado magneticamente estabilizado - Google Patents

Separaciones cromatograficas continuas en un lecho fluidizado magneticamente estabilizado

Info

Publication number
MX165977B
MX165977B MX007308A MX730883A MX165977B MX 165977 B MX165977 B MX 165977B MX 007308 A MX007308 A MX 007308A MX 730883 A MX730883 A MX 730883A MX 165977 B MX165977 B MX 165977B
Authority
MX
Mexico
Prior art keywords
bed
mixture
components
fluidized bed
chromatographic separations
Prior art date
Application number
MX007308A
Other languages
English (en)
Inventor
Jeffrey H Siegell
Original Assignee
Exxon Research Engineering Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Exxon Research Engineering Co filed Critical Exxon Research Engineering Co
Publication of MX165977B publication Critical patent/MX165977B/es

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1807—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using counter-currents, e.g. fluidised beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/025—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with wetted adsorbents; Chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B01J8/42—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed subjected to electric current or to radiations this sub-group includes the fluidised bed subjected to electric or magnetic fields
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2215/00—Separating processes involving the treatment of liquids with adsorbents
    • B01D2215/02—Separating processes involving the treatment of liquids with adsorbents with moving adsorbents
    • B01D2215/021—Physically moving or fluidising the adsorbent beads or particles or slurry, excluding the movement of the entire columns
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/58—Conditioning of the sorbent material or stationary liquid the sorbent moving as a whole

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Combustion & Propulsion (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

La presente invención se refiere a un procedimiento para separar contínuamente una mezcla de alimentación que contiene por lo menos dos componentes, caracterizado por los pasos de: a) introducir la mezcla en un lecho movible que contiene partículas magnetizables, el lecho se fluidiza mediante un fluido protador que pasa a través del lecho de una manera ascendente transversal al flujo del lecho y que se estabiliza mediante medios magnéticos que tiene resistencia suficiente para suprimir el retromezclado de sólidos en el mismo. b) poner en contacto la mezcla con un adsorben en el lecho durante un período de tiempo necesario para separar por lo menos una porción de uno de los componentes de la mezcla, y c) recuperar por lo menos una corriente de producto de lecho movible a lo largo de la trayectoria del lecho, consistiendo la corriente de una porción del fluido portador y una porción de la mezcla de alimentación que contiene por lo menos una porción de uno de los componentes.
MX007308A 1982-02-02 1983-01-21 Separaciones cromatograficas continuas en un lecho fluidizado magneticamente estabilizado MX165977B (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/345,095 US4443231A (en) 1982-02-02 1982-02-02 Continuous chromatographic separations in a magnetically stabilized fluidized bed

Publications (1)

Publication Number Publication Date
MX165977B true MX165977B (es) 1992-12-14

Family

ID=23353494

Family Applications (1)

Application Number Title Priority Date Filing Date
MX007308A MX165977B (es) 1982-02-02 1983-01-21 Separaciones cromatograficas continuas en un lecho fluidizado magneticamente estabilizado

Country Status (8)

Country Link
US (1) US4443231A (es)
EP (1) EP0086068B1 (es)
JP (1) JPS58146409A (es)
AU (1) AU558393B2 (es)
CA (1) CA1186246A (es)
DE (1) DE3373785D1 (es)
MX (1) MX165977B (es)
NO (1) NO160603C (es)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB8317228D0 (en) * 1983-06-24 1983-07-27 Exxon Research Engineering Co Magnetizable adsorbents
US4655796A (en) * 1983-09-30 1987-04-07 Exxon Research & Engineering Co. Continuous sorption process
US4675113A (en) * 1984-11-28 1987-06-23 University Patents, Inc. Affinity chromatography using dried calcium alginate-magnetite separation media in a magnetically stabilized fluidized bed
EP0203163A4 (en) * 1984-11-28 1987-09-10 University Patents Inc AFFINITY CHROMATOGRAPHY USING SEPARATING AGENTS BETWEEN MAGNETITE AND DRIED CALCIUM ALGINATE IN A FLUIDIZED AND MAGNETICALLY STABILIZED BED.
FR2575666B1 (fr) * 1985-01-04 1989-08-18 Centre Nat Rech Scient Procede et dispositif pour la separation chromatographique de macromolecules biologiques
US4668379A (en) * 1985-05-23 1987-05-26 Exxon Research And Engineering Company Process for magnetically stabilizing a fluidized bed containing nonmagnetizable particles and a magnetizable fluid
US4780113A (en) * 1987-10-16 1988-10-25 Exxon Chemical Patents Inc. Isomobility focusing in a magnetically stabilized fluidized bed
US4937001A (en) * 1988-11-22 1990-06-26 Exxon Research And Engineering Company Process for reducing axial dispersion in a magnetically stabilized fluidized bed
US5174979A (en) * 1989-10-06 1992-12-29 Uop Mixed ion-exchanged zeolites and processes for the use thereof in gas separations
WO1993009860A1 (en) * 1991-11-15 1993-05-27 University Of Michigan Continuous multicomponent focusing in a magnetically stabilized fluidized bed
CA2361545C (en) 1999-02-22 2009-01-27 Henry Kopf Purification of biological substances
US6214221B1 (en) 1999-02-22 2001-04-10 Henry B. Kopf Method and apparatus for purification of biological substances
JP2002147948A (ja) * 2000-11-10 2002-05-22 Japan Organo Co Ltd ガス分離装置及びガス分離方法
US7211703B2 (en) * 2005-04-27 2007-05-01 Calgon Carbon Corporation Method of separating E and Z isomers of an alkene alcohol and derivatives thereof
US20140260540A1 (en) * 2013-03-15 2014-09-18 Agilent Technologies, Inc. Sample inlet with multi-capillary liner for gas chromatography
GB2550390A (en) * 2016-05-18 2017-11-22 Anton Michel Continuous moving bed chromatography
IL254209A0 (en) * 2017-08-29 2017-10-31 Yissum Res Dev Co Of Hebrew Univ Jerusalem Ltd Magnetic separation of chiral substances

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1291137A (en) * 1916-09-18 1919-01-14 Charles J Reed Process of and apparatus for grading solid materials.
US3078647A (en) * 1960-05-12 1963-02-26 Cities Service Res & Dev Co Continuous gas chromatography
US3236092A (en) * 1962-02-21 1966-02-22 Monsanto Co Method and apparatus for continuous flow analysis
US3264801A (en) * 1962-11-13 1966-08-09 Union Oil Co Chromatographic apparatus and process
US3482376A (en) * 1968-06-26 1969-12-09 Atomic Energy Commission Apparatus for continuous chromatographic separations
US3527350A (en) * 1969-08-25 1970-09-08 Atomic Energy Commission Apparatus for continuous chromatography
US3843518A (en) * 1972-08-23 1974-10-22 Exxon Research Engineering Co Commercial chromatography for more than two components
US4132005A (en) * 1977-08-02 1979-01-02 Exxon Research & Engineering Co. Fluidization of permanently magnetic particle beds
US4254556A (en) * 1978-05-03 1981-03-10 Lello Anav Portable drafting device for drawing parallel lines, comprising a working plane of flexible plastic material, adapted to be rolled
US4283204A (en) * 1979-09-07 1981-08-11 Exxon Research & Engineering Co. Process for the separation of contaminants from feed streams using magnetic beds
US4247987A (en) * 1979-09-26 1981-02-03 Exxon Research & Engineering Co. Continuous countercurrent fluid-solids contacting process stabilized by a magnetic field

Also Published As

Publication number Publication date
EP0086068A3 (en) 1985-01-23
NO160603B (no) 1989-01-30
AU558393B2 (en) 1987-01-29
CA1186246A (en) 1985-04-30
EP0086068A2 (en) 1983-08-17
NO830341L (no) 1983-08-03
EP0086068B1 (en) 1987-09-23
DE3373785D1 (en) 1987-10-29
JPS58146409A (ja) 1983-09-01
AU1096283A (en) 1983-08-11
US4443231A (en) 1984-04-17
JPH0230282B2 (es) 1990-07-05
NO160603C (no) 1989-05-10

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