MD3530F1 - Plant for flow transesterification of vegetable oils - Google Patents

Plant for flow transesterification of vegetable oils Download PDF

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Publication number
MD3530F1
MD3530F1 MDA20070020A MD20070020A MD3530F1 MD 3530 F1 MD3530 F1 MD 3530F1 MD A20070020 A MDA20070020 A MD A20070020A MD 20070020 A MD20070020 A MD 20070020A MD 3530 F1 MD3530 F1 MD 3530F1
Authority
MD
Moldova
Prior art keywords
transesterification
vessels
vessel
decanting
receiving device
Prior art date
Application number
MDA20070020A
Other languages
Romanian (ro)
Other versions
MD3530G2 (en
Inventor
Ion Habasescu
Valerian Cerempei
Original Assignee
Institutul De Tehnica Agricola "Mecagro"
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institutul De Tehnica Agricola "Mecagro" filed Critical Institutul De Tehnica Agricola "Mecagro"
Priority to MDA20070020A priority Critical patent/MD3530G2/en
Publication of MD3530F1 publication Critical patent/MD3530F1/en
Publication of MD3530G2 publication Critical patent/MD3530G2/en

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Abstract

Inventia se refera la o instalatie pentru transesterificarea in flux a uleiurilor vegetale pentru obtinerea combustibilului lichid pentru motoarelecu ardere interna si poate fi utilizata in industriile chimica, prelucratoare si alimentara. Instalatia pentru transesterificarea in flux a uleiurilor vegetale contine vase pentru ulei vegetal (14) si metanol catalizat (13), bloc de transesterificare, rezervoare de acumulare a esterului (33) si glicerinei (29), ejectoare (10, 19), pompe de inalta presiune (9, 18), traductoare de nivel (39, 40, 41, 42), de temperatura (26) si presiune (17, 25). Vasele pentru ulei vegetal (14) si metanol catalizat (13) sunt unite cu blocul de transesterificare, format din trei vase cilindrice coaxiale cu fund comun, vasele central (4) si extern (5) fiind predestinate pentru receptia si decantarea amestecului de reactie obtinut respectiv dupa prima si a doua trepte de transesterificare, in fiecare vas din cele doua mentionate sunt montate dispozitive de receptie (16, 24) si de evacuare a esterilor obtinuti (22, 31) si racorduri de evacuare a glicerinei, totodata fiecare dispozitiv de receptie este executat in forma de conducta, la capatul inferior al careia este montat un caus partial inchis, orientatcu fanta formata intre capacul si fundul lui spreperetele vasului de decantare, causul fiind amplasat mai sus de fundul vasului la 0,2 din inaltimealui. Dispozitivele de evacuare (22, 31) sunt montate astfel incat capetele lor deschise sunt amplasate mai jos de capacul blocului de transesterificare. Intre vasele de decantare (4, 5) este situat schimbatorul de caldura (6), in care sunt montate doua reactoare (7, 8) respectiv al primei si al celei de a doua trepte de transesterificare, totodata intrarea in primul reactor (7) prin pompa (9),ejectorul (10) si robinetele (11, 12) este conectata cu vasele pentru metanol catalizat (13) si ulei vegetal (14), iar iesirea lui - cu dispozitivul de receptie (16), montat in vasul central de decantare (4). Intrarea in reactorul al doilea (8) prin pompa (18), ejectorul (19) si robinetele (20,21) este conectata cu vasul pentru metanol catalizat (13) si cu dispozitivul de evacuare (22), montat in vasul central de decantare (4), iar iesirea- cu dispozitivul de receptie (24), montat in vasul extern de decantare (5). Diametrul conductei dispozitivului de receptie in partea superioara estecu mult mai mic decat in partea inferioara langa caus. In fiecare vas de decantare sunt instalate cate doua traductoare de nivel al esterului (40, 42) si glicerinei (39, 41) pentru dirijarea vitezeide evacuare-receptie a lor.The invention relates to an installation for the transesterification in flow of vegetable oils for obtaining liquid fuel for internal combustion engines and can be used in the chemical, processing and food industries. The plant for the transesterification in flow of vegetable oils contains vessels for vegetable oil (14) and catalyzed methanol (13), transesterification block, storage tanks for ester (33) and glycerine (29), ejectors (10, 19), pumps high pressure (9, 18), level transducers (39, 40, 41, 42), temperature (26) and pressure (17, 25). The vegetable oil vessels (14) and catalyzed methanol (13) are joined by the transesterification block, consisting of three coaxial cylindrical vessels with a common bottom, the central (4) and external (5) vessels being predestined for receiving and decanting the reaction mixture obtained. respectively after the first and second transesterification steps, in each of the two mentioned vessels are installed receiving devices (16, 24) and evacuation of the obtained esters (22, 31) and connections for evacuating glycerin, at the same time each receiving device it is executed in the form of a pipe, at the lower end of which is mounted a partially closed case, oriented with the slit formed between the lid and its bottom the walls of the decanting vessel, the case being located above the bottom of the vessel at 0.2 height. The exhaust devices (22, 31) are mounted so that their open ends are located below the lid of the transesterification block. Between the decanting vessels (4, 5) is located the heat exchanger (6), in which two reactors (7, 8) respectively of the first and of the second transesterification stage are installed, at the same time the entrance to the first reactor (7). through the pump (9), the ejector (10) and the valves (11, 12) are connected with the vessels for catalyzed methanol (13) and vegetable oil (14), and its output - with the receiving device (16), mounted in the central vessel settling (4). The inlet to the second reactor (8) through the pump (18), the ejector (19) and the valves (20.21) is connected to the catalytic methanol vessel (13) and to the exhaust device (22), mounted in the central decanter vessel. (4), and the output - with the receiving device (24), mounted in the external decanting vessel (5). The diameter of the pipe of the receiving device in the upper part was much smaller than in the lower part near the cause. In each decanting vessel two two level transducers of ester (40, 42) and glycerine (39, 41) are installed to guide their speed of evacuation-reception.

MDA20070020A 2007-01-26 2007-01-26 Plant for flow transesterification of vegetable oils MD3530G2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
MDA20070020A MD3530G2 (en) 2007-01-26 2007-01-26 Plant for flow transesterification of vegetable oils

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
MDA20070020A MD3530G2 (en) 2007-01-26 2007-01-26 Plant for flow transesterification of vegetable oils

Publications (2)

Publication Number Publication Date
MD3530F1 true MD3530F1 (en) 2008-03-31
MD3530G2 MD3530G2 (en) 2008-10-31

Family

ID=39271501

Family Applications (1)

Application Number Title Priority Date Filing Date
MDA20070020A MD3530G2 (en) 2007-01-26 2007-01-26 Plant for flow transesterification of vegetable oils

Country Status (1)

Country Link
MD (1) MD3530G2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MD4165C1 (en) * 2010-11-22 2012-11-30 Государственный Университет Молд0 Plant for the production of biofuel on base of fatty acid methyl esters

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EA002043B1 (en) * 1997-11-24 2001-12-24 Энергеа Умвельттехнологи Гмбх Method for producing fattymethyl ester and equipmentfor realizing the same
MD2058G2 (en) * 2000-07-11 2003-06-30 Петру ПАЛАМАРЧУК Device for alarm signalling of water level in the pipe culverts of the railway embankment
AU2004223910A1 (en) * 2003-03-20 2004-10-07 Michael F. Pelly Method and apparatus for refining biodiesel
MD2830G2 (en) * 2004-01-14 2006-03-31 Зайфулла Хамит-Нагимо0 СУЛЕЙМАНОВ Installation for obtaining fatty acids of the methyl esters
MD2958C2 (en) * 2004-04-22 2006-11-30 Валериу ДОМИНАС Installation for obtaining biodiesel fuel from vegetal oils

Also Published As

Publication number Publication date
MD3530G2 (en) 2008-10-31

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FG4A Patent for invention issued
KA4A Patent for invention lapsed due to non-payment of fees (with right of restoration)
MM4A Patent for invention definitely lapsed due to non-payment of fees