KR960003886B1 - Sterilization method of spice - Google Patents

Sterilization method of spice Download PDF

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KR960003886B1
KR960003886B1 KR1019900018970A KR900018970A KR960003886B1 KR 960003886 B1 KR960003886 B1 KR 960003886B1 KR 1019900018970 A KR1019900018970 A KR 1019900018970A KR 900018970 A KR900018970 A KR 900018970A KR 960003886 B1 KR960003886 B1 KR 960003886B1
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minutes
spices
spice
pepper
coriander
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KR920009328A (en
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최춘언
윤종훈
박완규
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오뚜기식품주식회사
함태호
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10Natural spices, flavouring agents or condiments; Extracts thereof

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  • Life Sciences & Earth Sciences (AREA)
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Abstract

The spice is sterilized by 1) soaking whole black pepper in 350-400 ppm NaOCl soln. for 3-5 min., soaking cinnamon bark in 400-500 ppm NaOCl soln. for 3-4 min., soaking whole red pepper in 500-600 ppm NaOCl soln. for 3-5 min., and soaking whole coriander in 200-400 ppm NaOCl soln. for 3-5 min., 2) dehydrating the soaked spices with 10-50 mesh sieve, and 3) drying the dehydrated spices at 60-80 deg. C for 30 min-1 hr. to obtain the final product contg. 15% or less moisture.

Description

향신료의 살균방법How to Sterilize Spices

이 발명은 향신료의 살균, 특히 후추, 계피, 고추 및 코리안더의 살균에 있어 품질의 열화나 유독성물질의 생성등의 부작용이 없이 향신료에 부착되어 있는 대장균군 등을 사멸시킴으로써 식품위생상 안정한 향신료의 살균방법에 관한 것이다.This invention sterilizes spices that are stable for food hygiene by killing coliforms attached to spices without degrading quality or producing toxic substances in the sterilization of spices, especially pepper, cinnamon, red pepper and coriander. It is about a method.

일반적으로 향신료라 함은 요리나 조미가공식품등에 필수불가결한 양념으로 후추, 고추, 생강, 계피, 코리안더, 겨자, 정향, 강황, 육두구, 소두구, 회향, 쿠민, 훼네그릭, 샐러리씨 등 그 종류는 상당히 많으며, 주산지는 열대, 아열대지방이다.In general, spices are indispensable spices for cooking and seasoned foods, such as pepper, pepper, ginger, cinnamon, coriander, mustard, cloves, turmeric, nutmeg, soybean paste, fennel, cumin, fenegrik and celery seeds. Are quite numerous, and the main regions are tropical and subtropical.

향신료는 재배, 유통등의 과정에서 대단히 많은 미생물에 오염될 가능성이 있어, 그 처리가 매우 중요하다.Spices can be contaminated with a large number of microorganisms in the process of cultivation and distribution, and their treatment is very important.

그중에서도 대장균군은 포유동물의 분변과 밀접한 관계가 있으므로, 식품위생상 대장균의 소장은 대단히 큰 의미를 가지고 있다.Among them, Escherichia coli group is closely related to feces of mammals, so the small intestine of Escherichia coli has a great meaning in food hygiene.

종래의 향신료의 살균방법에서는 가열살균, 자외선조사, 마이크로웨이브처리, 에틸렌옥사이드나 프로필렌옥사이드와 같은 훈증제처리등의 방법이 가장 많이 사용되고 있다.In the conventional method of sterilizing spices, methods such as heat sterilization, ultraviolet irradiation, microwave treatment, and fumigant treatment such as ethylene oxide or propylene oxide are most frequently used.

그중에서도 훈증제처리 방법이 가장 많이 사용되고 있는 방법이나, 발암물질의 생성 및 풍미 색상등의 변화 뿐만 아니라, 인화성 및 가연성이 있어 투약시 작업환경의 정비 및 밀폐된 훈종실이 있어야 하는 불편이 있다.Among them, the fumigant treatment method is the most widely used method, but not only the generation of carcinogens and the change of flavor color, but also the flammability and flammability, so there is inconvenience of maintaining a working environment and administering a closed fumigation chamber during administration.

또한, 최근에는 감마선과 같은 방사선조사에 의한 방법등이 실용화되어 그 효과 및 안전성에 대해 인정받고 있으나 방사선조사방법은 일반 소비자들이 방사능이라는 물질을 심리적으로 선호하지 않으며, 그 설비투자 비용이 크다는 단점이 있다.In addition, recently, methods such as gamma rays have been commercialized, and their effects and safety have been recognized. However, the radiation method has a disadvantage in that the average consumer does not psychologically prefer radioactive substances and the cost of equipment investment is high. have.

따라서, 이 발명에서는 이러한 제문제점을 해결하기 위해서 식품위생학적으로 문제가 되고 있는 대장균의 효과적인 살균법에 대하여 연구한 것이다.Therefore, in this invention, in order to solve this problem, the study on the effective sterilization method of E. coli which is a food hygiene problem.

즉, 향신료로서 후추, 계피, 고추, 코리안더를 분쇄하지 않은 채로 200∼600ppm의 치아염소산나트륨(NaOCI) 수용액에서 2∼10분 정도의 단시간처리함으로써 대장균군을 살균하는 방법이다. 살균된 향신료 원두를 10∼50메쉬의 체망으로 걸러 건조온도 60∼80℃에서 30분∼1시간정도 건조하여 수분함량이 15%이하가 되도록 하는 것을 특징으로 한다.That is, it is a method of sterilizing E. coli group by short-time treatment for about 2 to 10 minutes in 200-600 ppm sodium sodium chlorate (NaOCI) solution without grinding pepper, cinnamon, red pepper, and coriander as spices. The sterilized spice beans are filtered through a mesh of 10 to 50 mesh and dried at a drying temperature of 60 to 80 ° C. for about 30 minutes to 1 hour so that the moisture content is 15% or less.

종래에 알려진 관련특허문헌은 다음과 같다.Related patent documents known in the art are as follows.

(1) 일본국 특허공보 소 56-54140(1981.12.23.공고, 발명자 越田大吉(외 4인) ; 카레분의 제조방법)에서는 카레분의 원료인 향신료 10∼55메쉬로 조분쇄하여 예비가열을 한후, 0.4∼2kg/cm²의 가압증기에 의해 습열가열처리를 하고, 냉각, 분쇄하는 것을 그 특징으로 하는 카레분의 제조방법에 대하여 기재되어 있고, (2) 일본국 특허공보 소 62-50101(1987.10.22.공고, 발명자 越田大吉(외 9인) ; 향신료의 살균방법)에서는 향신료를 분쇄하지 않고 약 100∼145℃의 온도에서 증기와 접촉시켜 600-1초간 유지한후 고온에서 단시간 건조한후 상법으로 냉각한후 필요에 따라 분쇄하는 것을 특징으로 하는 향신료의 살균방법에 대하여 기재되어 있으며, (3) 일본국 특허공보 소 62-50102(1987.10.22.공고, 발명자 越田大吉(외 9인) ; 향신료의 살균방법)에서는 향신료를 분쇄하지 않고 그 표면에 물을 충분히 습윤시킨 후, 100℃이상의 온도에서 살균 및 건조를 하여 습윤전의 수분함량과 동일한 수분함량이 되게 하고 후에 상법에 따라 냉각하는 것을 특징으로 하는 향신료의 살균방법에 의하여 기재되어 있다.(1) Japanese Patent Publication No. 56-54140 (published on December 23, 1981, the inventor, Yutada Yoshino (4 others); method for preparing curry powder) is preheated by coarsely pulverizing with 10-55 mesh of spices, which is the raw material of curry powder. The method for producing a curry powder, which is characterized in that the wet heat treatment is performed by 0.4 to 2 kg / cm² of pressurized steam, followed by cooling and pulverizing, (2) Japanese Patent Publication No. 62-50101 ( 1987.10.22.Information, the inventor 越 田大吉 (9 others); sterilization method of spices), without grinding the spice without contacting the steam at a temperature of about 100 ~ 145 ℃ for 600-1 seconds and dried for a short time at high temperature A method of sterilization of spices, which is characterized in that it is cooled and then pulverized as necessary. (3) Japanese Patent Publication No. 62-50102 (October 22, 1987); In the sterilization method of spices) Water is sufficiently wetted on the surface, sterilized and dried at a temperature of 100 ° C. or higher to obtain the same water content as the water content before wetting, and then cooled by a conventional method.

(4) 일본국 공개특허공보 공개번호 소 58-67158(1983.4.21.공개, 발명자 足立由郞(외 2인) ; 향신료류의 살균방법)에서는 분쇄한 향신료 100에 대하여 에탄올 5∼15가 되도록 혼합한 것을 70∼60℃정도로 가온하는 향신료류의 살균방법에 대하여 기재되어 있다.(4) Japanese Laid-Open Patent Publication No. 58-67158 (published on April 21, 1983, inventor 足 立 由 郞 (two others); sterilization method of spices) to ethanol 5 to 15 with respect to 100 ground spices. It describes about the sterilization method of the spice which heats the mixed thing about 70-60 degreeC.

(5) 일본국 공개특허공보 공개번호 소 58-220666(1983.12.22.공개, 발명자 杉澤公(외 6인) ; 터메릭의 처리법)에서는 터메릭원두 및 분쇄물을 105∼200℃에서 1∼60분간 건열가열하여 분말화하는 것을 특징으로 하는 터메릭의 처리법에 대하여 기재되어 있다.(5) Japanese Laid-Open Patent Publication No. 58-220666 (published on Dec. 22, 1983, the inventor, Yushako (6 others); turmeric treatment method), in which the turmeric beans and ground products are carried out at 105 to 200 DEG C. It describes a turmeric treatment method characterized by dry heating for 60 minutes and powdering.

(6) 대한민국 공개특허공보 공고번호 86-1345(1986.9.16.공고, 발명자 조 한옥 ; 향신료의 안전한 장기저장벙법)에서는 일정량의 향신료를 틴(tin)등에 넣고 밀봉한 다음 60Co 감마선을 3∼7KGY 조사하여 실온에서 저장함을 특징으로 하는 향신료의 안전한 장기저장방법에 대하여 기재되어 있다.(6) In the Republic of Korea Patent Publication No. 86-1345 (announcement, inventor Cho Han-ok; safe long-term storage method of spices) put a certain amount of spices in a tin, etc. and sealed 60Co gamma rays 3-7KGY It describes a safe long-term storage method of spices characterized by irradiation and storage at room temperature.

위 관련특허에서 볼 때 이 발명은 위 인용 특허와 전혀 다르다는 것을 알 수 있다.In view of the above patents, it can be seen that the present invention is completely different from the above-cited patents.

따라서, 이 발명은 후추, 계피, 고추 코리안더의 향신료를 분쇄하지 않은 상태에서 차아염소산나트륨(NaOCI)200∼600ppm의 농도를 유지하면서 2∼10분 정도의 단시간내 대장균을 살균한 후 10∼50메쉬의 체망으로 향신료의 물기를 없애고, 건조온도 60∼80℃에서 30분∼1시간 건조하여 수분함량이 15% 이하가 되는 것을 특징으로 하는 방법이다.Therefore, the present invention sterilizes E. coli in a short time of 2 to 10 minutes while maintaining the concentration of 200 to 600 ppm of sodium hypochlorite (NaOCI) without grinding the spices of pepper, cinnamon and red pepper coriander, and then 10 to 50 mesh. This method is characterized by removing the moisture of spices with a sieve of net, drying for 30 minutes to 1 hour at a drying temperature of 60 ~ 80 ℃ to 15% or less.

이 발명의 결과를 알기 위해서, 코리안더를 시료로 하여 다음 표 1 과 같은 조건하에서 실험을 실시하였다.In order to know the result of this invention, the experiment was performed on the conditions shown in following Table 1 using a coriander as a sample.

[표 1]TABLE 1

차아염소산나트륨 농도 및 침지시간에 따른 대장균류의 소장Small Intestine of Coliform Fungi with Sodium Hypochlorite Concentration and Soaking Time

위 실험결과에 의하여 NaOCI 농도 200ppm부터 대장균의 살균효과를 얻을수 있었다.As a result of the above experiment, the bactericidal effect of E. coli was obtained from NaOCI concentration of 200ppm.

위 방법에 의하여 살균된 향신료를 10∼50메쉬의 체망에 걸러서 향신료의 물기를 제거하고, 건조온도 60∼80℃에서 30분∼1시간동안 건조하여 수분함량이 15%가 되도록 한다.The sterilized spices by the above method is filtered through a mesh of 10 to 50 mesh to remove the moisture of the spices, and dried at a drying temperature of 60 to 80 ° C. for 30 minutes to 1 hour so that the moisture content is 15%.

건조온도 및 건조시간에 따른 코리안더의 수분함량 변동추이는 표 2 와 같다.The change in moisture content of Coriander according to drying temperature and drying time is shown in Table 2.

[표 2]TABLE 2

건조온도와 시간변화에 따른 향신료의 수분함량Moisture Content of Spices with Drying Temperature and Time

향신료의 건조온도가 80℃를 넘으면 향신료의 방향이 소실되므로 건조온도는 80℃가 넘지 않도록 한다.If the drying temperature of spices exceeds 80 ℃, the direction of spices is lost, so the drying temperature should not exceed 80 ℃.

향신료의 식품위생법상 수분규격은 15% 이하이므로 이 발명의 건조조건은 60℃ 30분으로 설정하였다.Since the moisture standard of the food hygiene method of the spice is 15% or less, the drying condition of the present invention was set to 60 ° C 30 minutes.

건조시간의 경우에 있어서, 대량생산의 경우에 건조효과를 충분히 유지하기 위하여 건조시간을 60분까지 하였다.In the case of the drying time, the drying time was up to 60 minutes in order to sufficiently maintain the drying effect in the case of mass production.

다음의 실시예에 따라 이 발명을 더 자세하게 설명한다.The invention will be described in more detail according to the following examples.

[실시예 1]Example 1

1. 분쇄하지 않은 후추를 200∼400ppm의 NaOCI 용액에 2분∼5분까지 침지시키면서 대장균소장 시험을 하였다.1. Coliform small intestine was immersed in a 200 ~ 400ppm NaOCI solution for 2 minutes to 5 minutes in uncrushed pepper.

위 시험결과에 의해 후추중 대장균의 사멸조건은 NaOCI농도 350ppm이상, 침지시간은 3분이상임을 알 수 있다.The above test results show that the killing condition of E. coli in pepper is NaOCI concentration over 350ppm and immersion time over 3 minutes.

2. 1)항에 의해 살균된 후추원두를 10∼28메쉬채로 걸러서 물기를 없앤후 건조온도 60∼70℃에서 20∼40분 건조하였다.2. Filter the pepper beans sterilized by 1) with 10-28 mesh and remove the water, and then dry for 20 to 40 minutes at the drying temperature of 60-70 ℃.

위 시험결과에 의해 수분함량 15%이하(보사부 규격)로 낮추기 위해서 건조온도 60℃이상 건조시간 30분이상 건조하여야 함을 알 수 있다.From the above test result, it can be seen that the drying temperature should be more than 30 ℃ and the drying time more than 30 minutes in order to lower the moisture content to 15% or less (compartment part standard).

[실시예 2]Example 2

1. 분쇄하지 않은 계피를 30∼40cm 길이로 잘라서 300∼500ppm의 NaOCI 용액에 2∼4분 정도 침지시키면서 대장균소장시험을 하였다.1. The uncrushed cinnamon was cut into 30 to 40 cm in length and subjected to the E. coli intestine test while immersing in 300 to 500 ppm NaOCI solution for 2 to 4 minutes.

위 시험결과에 의해 계피중 대장균의 사멸조건은 NaOCI농도 400ppm이상, 침지시간 3분이상임을 알 수 있다.The above test results show that the killing condition of E. coli in cinnamon is NaOCI concentration over 400ppm and immersion time over 3 minutes.

2. 1)항에 의한 살균된 계피를 꺼내어 물기를 없앤후 건조온도 60∼80℃에서 30∼60분 건조하였다.2. Remove the sterilized cinnamon according to 1), remove the water and dry for 30 to 60 minutes at a drying temperature of 60 ~ 80 ℃.

위 시험결과에 의해 수분함량 15%이하(보사부 규격)로 낮추기 위해 건조온도 60℃이상 건조시간 50분이상 건조하여야 함을 알 수 있다.From the above test results, it can be seen that the drying temperature should be over 60 ℃ and the drying time over 50 minutes in order to lower the moisture content to 15% or less.

[실시예 3]Example 3

1. 분쇄하지 않은 고추를 400∼600ppm의 NaOCI 용액에 2분∼5분까지 침지시키면서 대장균소장시험을 하였다.1. Colon bacillus test was performed by immersing uncrushed red pepper in 400-600 ppm NaOCI solution for 2-5 minutes.

위 시험결과에 의해 고추중 대장균의 사멸조건은 NaOCI농도 500ppm이상, 침지시간 2분이상임을 알 수 있다.The above test results show that the killing condition of E. coli in red pepper is NaOCI concentration over 500ppm and immersion time over 2 minutes.

2. 1)항에 의한 살균된 고추를 10메쉬체로 걸러서 물기를 없앤후 건조온도 60∼80℃에서 20분∼40분 건조하였다.2. The sterilized red pepper according to 1) was filtered through 10 mesh sieve to remove water and dried for 20-40 minutes at the drying temperature of 60-80 ℃.

위 시험결과에 의해 수분함량 15%이하(보사부 규격)로 낮추기 위해 건조온도 60℃이상 건조시간 20분이상 건조하여야 함을 알 수 있다.From the above test result, it can be seen that the drying temperature should be more than 20 ℃ and drying time more than 20 minutes in order to lower the moisture content to 15% or less (compartment part standard).

[실시예 4]Example 4

1. 분쇄하지 않은 코리안더를 100∼400ppm의 NaOCI 용액에 1∼4분까지 침지시키면서 대장균소장시험을 하였다.1. Coliform small intestine was immersed in 100 to 400 ppm NaOCI solution for 1 to 4 minutes.

2. 1)항에 의해 코리안더 원두를 10∼28메쉬채로 걸러서 물기를 없앤후 건조온도 60∼80℃에서 20분∼40분 건조하였다.2. According to 1), the coriander beans were filtered with 10-28 mesh and then drained, and dried for 20 to 40 minutes at a drying temperature of 60 to 80 ° C.

Claims (3)

향신료(후추, 계피, 고추, 코리안더)에 있어서 분쇄하지 않은 후추를 350∼400ppm의 NaOCI 용액에서 3∼5분간, 분쇄하지 않은 계피를 400∼500ppm의 NaOCI용액에서 3∼4분간, 분쇄하지 않은 고추를 500∼600ppm의 NaOCI 용액에서 3∼5분간 및 분쇄하지 않은 코리안더를 200~400ppm의 NaOCI 용액에서3~5분간 각각 침지시킴을 특징으로 하는 향신료의 살균방법.Uncooked pepper in spices (pepper, cinnamon, red pepper, coriander) for 3-5 minutes in 350-400 ppm NaOCI solution, uncrushed cinnamon in 400-500 ppm NaOCI solution for 3-4 minutes The sterilization method of the spice, characterized in that immersed in 500 ~ 600ppm NaOCI solution for 3 to 5 minutes and unpulverized coriander in 200 ~ 400ppm NaOCI solution for 3 to 5 minutes. 제 1 항에 있어서, 살균된 향신료원두를 10∼50메쉬의 체망에 걸러 탈수시킴을 특징으로 하는 향신료의 살균방법.The method for sterilizing spices according to claim 1, wherein the sterilized spice beans are dehydrated in a mesh of 10 to 50 mesh. 제 2 항에 있어서, 탈수된 향신료원두를 60∼80℃에서 30분∼1시간정도 건조하여 수분함량이 15%이하가 되도록 처리함을 특징으로 하는 향신료의 살균방법.3. The method of sterilizing spices according to claim 2, wherein the dehydrated spice beans are dried at 60 to 80 DEG C for about 30 minutes to 1 hour, so that the moisture content is 15% or less.
KR1019900018970A 1990-11-22 1990-11-22 Sterilization method of spice KR960003886B1 (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CZ301416B6 (en) * 2007-11-23 2010-02-24 Výzkumný ústav potravinárský Praha, v.v.i. Heat sterilization method of spices with subsequent recovery of aromatic substances

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CZ301416B6 (en) * 2007-11-23 2010-02-24 Výzkumný ústav potravinárský Praha, v.v.i. Heat sterilization method of spices with subsequent recovery of aromatic substances

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