KR950704564A - FLOCK FOR ELECTROSTATIC PILE PLANTING - Google Patents

FLOCK FOR ELECTROSTATIC PILE PLANTING Download PDF

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KR950704564A
KR950704564A KR1019950701572A KR19950701572A KR950704564A KR 950704564 A KR950704564 A KR 950704564A KR 1019950701572 A KR1019950701572 A KR 1019950701572A KR 19950701572 A KR19950701572 A KR 19950701572A KR 950704564 A KR950704564 A KR 950704564A
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floc
fibers
electrostatic
polymer layer
conductive polymer
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KR1019950701572A
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Korean (ko)
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이꾸오 미조구찌
마모루 이또오
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스즈끼 데이지
아킬레스 가부시기 가이샤
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D1/00—Processes for applying liquids or other fluent materials
    • B05D1/02—Processes for applying liquids or other fluent materials performed by spraying
    • B05D1/12—Applying particulate materials
    • B05D1/14—Flocking
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/35—Heterocyclic compounds
    • D06M13/352—Heterocyclic compounds having five-membered heterocyclic rings
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/356—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of other unsaturated compounds containing nitrogen, sulfur, silicon or phosphorus atoms
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/356—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of other unsaturated compounds containing nitrogen, sulfur, silicon or phosphorus atoms
    • D06M15/3562—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of other unsaturated compounds containing nitrogen, sulfur, silicon or phosphorus atoms containing nitrogen
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/356—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of other unsaturated compounds containing nitrogen, sulfur, silicon or phosphorus atoms
    • D06M15/3566—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of other unsaturated compounds containing nitrogen, sulfur, silicon or phosphorus atoms containing sulfur
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06Q—DECORATING TEXTILES
    • D06Q1/00—Decorating textiles
    • D06Q1/04—Decorating textiles by metallising
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
    • H01B1/06—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances
    • H01B1/12—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances organic substances
    • H01B1/124—Intrinsically conductive polymers
    • H01B1/127—Intrinsically conductive polymers comprising five-membered aromatic rings in the main chain, e.g. polypyrroles, polythiophenes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
    • H01B1/06—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances
    • H01B1/12—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances organic substances
    • H01B1/124—Intrinsically conductive polymers
    • H01B1/128—Intrinsically conductive polymers comprising six-membered aromatic rings in the main chain, e.g. polyanilines, polyphenylenes

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Laminated Bodies (AREA)
  • Artificial Filaments (AREA)
  • Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)

Abstract

짧은 섬유의 전체 표면(선후 양단면을 포함)이 도전성 폴리머층(바람직한 두께 : 평균하여 0.01~0.1㎛)에 의하여 실질적으로 완전히 (비피복 부분의 비율은 3%이하)피복되어 있는 정전식모용 플록, 그 제법 및 이것을 사용한 정전식모품을 제공하였다. 바람직한 폴리머층은 피롤, N-메틸피롤, 아닐린, 티오펜을 모노머로 하는 폴리머 또는 코폴리머를 생성된 것이다. 본 플록은 대전성 및 분리성이 주위의 수분의 영향을 받지 않고 정전식모 과정에서 만족한 비행력을 안정하여 얻을 수 있기 때문에, 어느 식모방식에서도 건조한 환경에 있어서의 정전식모로 반복 이용할 수 있어, 종래의 아프터 컨디셔닝 등이 불필요하게된다. 수득한 식모제품은 식모의 밀집도가 균일하여 섬유의 휘감김 등도 없다.An electrostatic wool flock whose entire surface (including both ends of the front and rear ends) of the short fibers is substantially completely covered (the proportion of the uncovered portion is 3% or less) by the conductive polymer layer (preferable thickness: 0.01 to 0.1 탆 on average). The manufacturing method and the electrostatic mother article using the same were provided. Preferred polymer layers are those resulting from polymers or copolymers comprising pyrrole, N-methylpyrrole, aniline, thiophene as monomers. This floc can be repeatedly used as a capacitive bridging device in a dry environment in any type of bridging because stable charging can be achieved in the electrostatic bristle process without being charged and separated from the influence of surrounding moisture. Conventional after-conditioning becomes unnecessary. The obtained woolen product has a uniform density of the wool, and there is no entanglement of fibers or the like.

Description

정전식모용 플록(FLOCK FOR ELECTROSTATIC PILE PLANTING)FLOCK FOR ELECTROSTATIC PILE PLANTING

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

제1도는 규산나트륨을 사용한 전착처리가 폴리에스테르 섬유에 대하여 실시된 종래의 정전식모용 플록에 대하여 전자현미경을 사용하여 확대된 플록선단부를 촬영한 현미경사진을 뜻한다. 더욱이, 사진의 오른쪽 아래부분에 있어서의 백선의 길이는 50㎛을 뜻하고,1 shows a micrograph of an enlarged floc tip portion using an electron microscope for a conventional electrostatic wool flock in which electrodeposition treatment using sodium silicate has been performed on polyester fibers. Moreover, the length of the white line in the lower right part of the photograph means 50 µm,

제2도는 폴리에스테르섬유(섬도 : 1.5데니어)의 단면을 포함하는 모든 표면이 피롤폴리머층에 의하여 완전히 피복되어 있다. 본 발명에 의한 정전식모용 플록에 대하여, 전자현미경을 사용하여 확대된 플록선단부를 촬영한 현미경사진을 뜻한다. 더욱이, 사진의 오른쪽 아래부분에 있어서의 백선의 길이는 20㎛를 뜻하고,2 shows that all surfaces including the cross section of polyester fiber (fineness: 1.5 denier) are completely covered by a pyrrole polymer layer. For the capacitive floc according to the present invention, it refers to a micrograph photographing the enlarged floc tip portion using an electron microscope. Moreover, the length of the white line in the lower right part of the photograph means 20 µm,

제3도는 제2도의 폴리에스테르 섬유의 원착사(pre-coloredfilament)(그 표면에 피롤폴리머층에 형성되어 있지 않다.)에 대하여 전자현미경을 사용하여 확대된 선단부를 촬영한 현미경 사진을 뜻한다. 더욱이, 사진의 오른쪽 아래부분에 있어서의 백선의 길이는 20㎛를 뜻한다.FIG. 3 is a micrograph of the tip portion enlarged using an electron microscope for the pre-coloredfilament (not formed on the surface of the pyrrole polymer layer) of the polyester fiber of FIG. 2. Moreover, the length of a white line in the lower right part of a photograph means 20 micrometers.

Claims (18)

짧은 섬유의 단면을 포함하는 모든 표면이 도전성 폴리머층에 의하여 실질적으로 완전히 피복되어 있음을 특징으로 하는 정전식모용 플록.An electrostatic wool flock, wherein all surfaces, including cross sections of short fibers, are substantially completely covered by a conductive polymer layer. 제1항에 있어서, 플록표면중 도전성 폴리머층에 의하여 피복되어 있지 않은 부분의 전체표면에 대한 비율은 3%이하임을 특징으로 하는 플록.2. The floc of claim 1, wherein a proportion of the floc surface to the entire surface of the portion of the floc surface not covered by the conductive polymer layer is 3% or less. 제1항 또는 2항에 있어서, 짧은 섬유는 염색되어 있음을 특징으로 하는 플록.The floc of claim 1, wherein the short fibers are dyed. 제1항~제3항중의 한 항에 있어서, 도전성 폴리머층의 두께는 평균하여 0.01㎛~0.1㎛범위임을 특징으로 하는 플록.The floc according to claim 1, wherein the thickness of the conductive polymer layer is in the range of 0.01 μm to 0.1 μm on average. 제1항~제4항중의 어느 하나의 항에 있어서, 도전성 포리머층은 피롤, N-메틸필롤, 아닐린, 티오펜 및 티오펜-3-술폰산으로 된 집단으로부터 선택된 1종 또는 2종 이상의 모노머를 중합하여 형성된 폴리머층 또는 코폴리머층임을 특징으로 하는 플록.The conductive polymer layer according to any one of claims 1 to 4, wherein the conductive polymer layer comprises at least one monomer selected from the group consisting of pyrrole, N-methylpyrrole, aniline, thiophene and thiophene-3-sulfonic acid. Flock characterized in that the polymer layer or copolymer layer formed by polymerization. 제5항에 있어서, 도전성 폴리머층은 피롤을 모노머로서 중합하여 얻을 수 있는 폴리머층임을 특징으로 하는 플록.The floc according to claim 5, wherein the conductive polymer layer is a polymer layer obtained by polymerizing pyrrole as a monomer. 제1항~제4항중의 어느 하나의 항에 있어서, 도전성 폴리머층의 두께는 짧은 섬유가 흡수성 섬유일 때는, 평균하여 대체로 0.01㎛~0.03㎛이고, 짧은 섬유가 비흡수성 섬유일때는 평균하여 대체로, 0.02㎛~0.05㎛임을 특징으로 하는 플록.The thickness of the conductive polymer layer is generally 0.01 µm to 0.03 µm when the short fibers are absorbent fibers, and averages when the short fibers are non-absorbent fibers. , Floc, characterized in that 0.02㎛ ~ 0.05㎛. 제1항~제7항중의 하나의 항에 있어서 짧은 섬유는 천연섬유 또는 반합성 섬유 그렇지 않으면 합성섬유로 되었고, 또한 섬유의 가로 세로비는 1:30~1:100범위내의 것임을 특징으로 하는 플록.The floc according to any one of claims 1 to 7, wherein the short fibers are made of natural or semi-synthetic fibers or synthetic fibers, and the aspect ratio of the fibers is in the range of 1:30 to 1: 100. 제1항~제8항중의 어느 하나의 항에 있어서, 플록의 표면 누설 저항치는 105Ω~108Ω㎝ 범위내임을 특징으로 하는 플록.The floc according to any one of claims 1 to 8, wherein the surface leakage resistance of the floc is in the range of 10 5 Pa-10 8 Pa. 제1항 또는 제2항에 있어서, 모노머의 중합반응을 짧은 섬유를 포함한 처리액속에서 화학산화 중합제를 촉매로 하여, 희망에 따라 첨가된 도우팬트 및/또는 표면장력 저하제와 함께 진행시켜서, 생성한 도전성 폴리머 처리액속의 섬유의 표면에 피복함에 따라 이루어지는 것을 특징으로 하는 정전식모용 플록의 제조방법.The process according to claim 1 or 2, wherein the polymerization of the monomers is carried out in a treatment liquid containing short fibers by using a chemical oxidation polymerizer as a catalyst and proceeding together with a desired dopant and / or surface tension reducing agent. A method for producing an electrostatic wool floc, which is formed by coating a surface of a fiber in a conductive polymer treatment liquid. 제1항 또는 제2항에 있어서, 모노머의 중합반응을 짧은 섬유를 포함하는 처리액속에서 화학산화 중합제를 촉매로 하여, 희망에 따라 첨가된 도우팬트 및/또는 표면장력 저하제와 함께 진행시켜서, 생성한 도전성 폴리머를 처리액속의 섬유의 표면에 피복하고, 그런 다음 피복된 긴 섬유를 절단하여 짧은 섬유로 함에 이루어지는 것을 특징으로 하는 정진식모용 플록의 제조방법.The process according to claim 1 or 2, wherein the polymerization of the monomers is carried out with a dopant and / or surface tension reducing agent added as desired using a chemical oxidation polymerizer as a catalyst in a treating liquid containing short fibers. The produced conductive polymer is coated on the surface of the fibers in the treatment liquid, and then the coated long fibers are cut to form short fibers. 제10항 또는 제11하에 있어서, 모노머로서는 피롤, N-메틸피롤, 아닐린, 티오펜 및 티오펜-3-술폰산으로 된 집단으로부터 선택된 1종 또는 2종 이상의 모노머가 사용되었음을 특징으로 하는 정전식모용 플록의 제조방법.12. Electrostatic hair according to claim 10 or 11, wherein one or more monomers selected from the group consisting of pyrrole, N-methylpyrrole, aniline, thiophene and thiophene-3-sulfonic acid are used as monomers. Method of making flocs. 제12항에 있어서, 모노머로서는 피롤이 사용되었음을 특징으로 하는 정전식모용 플록의 제조방법.13. The method of claim 12, wherein pyrrole is used as the monomer. 제10항~제13항중의 어느 하나의 항에 있어서, 사용하는 짧은 섬유 또는 긴 섬유는 염색된 섬유인 것임을 특징으로 하는 정전식모용 플록의 제조방법.The method for producing an electrostatic wool flock according to any one of claims 10 to 13, wherein the short or long fibers to be used are dyed fibers. 제10항~제14항중의 어느 하나의 항에 있어서, 촉매로서 사용하는 화학산화 중합제는 수용성 제2철염임을 특징으로 하는 정전식모용 플록의 제조방법.The method for producing an electrostatic wool floc according to any one of claims 10 to 14, wherein the chemical oxidation polymerizing agent used as a catalyst is a water-soluble ferric salt. 제10항~제15항중의 어느 하나의 항에 있어서, 중합반응이 종료한 다음, 피복한 섬유를 더욱 유연제 또는 평활제와 함께 수세함에 따라 이루어지는 것을 특징으로 하는 정전식모용 플록의 제조방법.The method for producing an electrostatic wool floc according to any one of claims 10 to 15, wherein after the polymerization reaction is completed, the coated fibers are washed with more softening agent or leveling agent. 제10항~제16항중의 어느 하나의 항에 있어서, 그에 기재된 방법에 따라서 제조된 것을 특징으로 하는 정전식모용 플록.The floc for capacitive hair according to any one of claims 10 to 16, which is produced according to the method described therein. 제1항~제9항 및 제17항중의 어느 하나의 항에 있어서, 정전식모용 플록을 원료로 하여 업식 정전식모법, 다운식 정전식모법, 업 다운식 정전식모법 그렇지 않으면 사이드식 정전식모법에 따라서, 또는 유동탱크형 정전식모기를 사용하여, 기재의 식모하여야 할 표면에 정전식모함에 따라 제조되는 것을 특징으로 하는 정전식모품.18. The electrostatic cap method, down electrostatic cap method, up-down capacitive cap method, or the side capacitive cap according to any one of claims 1 to 9 and 17, using as a raw material the floc for the cap. The capacitive article according to the law or by using a flow tank type capacitive mosquito is produced according to the electrostatic cap on the surface to be implanted. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019950701572A 1992-10-23 1993-10-15 FLOCK FOR ELECTROSTATIC PILE PLANTING KR950704564A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP92-309521 1992-10-23
JP30952192 1992-10-23
PCT/JP1993/001481 WO1994010371A1 (en) 1992-10-23 1993-10-15 Floc for electrostatic hair transplantation

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KR950704564A true KR950704564A (en) 1995-11-20

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AU2003227431B2 (en) 2002-06-28 2008-08-14 S.T. Corporation Moisture retentive gloves and process for producing the same
CN1295731C (en) * 2002-11-25 2007-01-17 财团法人工业技术研究院 Method for implanting metal nano wire or nano tube into field emission source assembly
WO2007099889A1 (en) * 2006-02-28 2007-09-07 University Of Yamanashi Method of treating conductive polymer
RU2490738C2 (en) 2007-11-27 2013-08-20 Мария СТРЕММЕ Composite materials containing internally conducting polymer and method and apparatus
GB2475714A (en) * 2009-11-27 2011-06-01 Pangaea Lab Ltd Hair building solids
CN101844872B (en) * 2010-05-07 2012-05-02 上海长悦涂料有限公司 Preparation method of flocking liquid
CN109023989A (en) * 2018-09-06 2018-12-18 山东领潮新材料有限公司 A kind of flaxen fiber electrostatic flocking fabric and preparation method thereof that natural antibacterial is mould proof
CN109763317A (en) * 2019-01-16 2019-05-17 广东顺德贰发毛绒有限公司 A kind of electricity of dust-proof villus treatment process
CN109734905B (en) * 2019-02-13 2022-02-08 东北大学 Preparation method and application of partially crystalline copolymer for enhancing performance of electrocatalyst

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JPS5497647A (en) * 1978-01-19 1979-08-01 Unitika Ltd Electrostatic flocking
US4975317A (en) * 1987-08-03 1990-12-04 Milliken Research Corporation Electrically conductive textile materials and method for making same
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JP2986857B2 (en) * 1989-08-29 1999-12-06 アキレス株式会社 Method for producing conductive fiber substrate
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EP0667413B1 (en) 1998-07-15
DE69319738T2 (en) 1999-01-07
EP0667413A4 (en) 1995-12-27
EP0667413A1 (en) 1995-08-16
CN1111170A (en) 1995-11-08
DE69319738D1 (en) 1998-08-20
WO1994010371A1 (en) 1994-05-11

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