KR950701966A - 용접 실링 냉각 압축기용 폴리올 에스테르 윤활제(polyol ester lubricants for hermetically sealed refrigerating compressors) - Google Patents

용접 실링 냉각 압축기용 폴리올 에스테르 윤활제(polyol ester lubricants for hermetically sealed refrigerating compressors)

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Publication number
KR950701966A
KR950701966A KR1019940704427A KR19940704427A KR950701966A KR 950701966 A KR950701966 A KR 950701966A KR 1019940704427 A KR1019940704427 A KR 1019940704427A KR 19940704427 A KR19940704427 A KR 19940704427A KR 950701966 A KR950701966 A KR 950701966A
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South Korea
Prior art keywords
acyl groups
mixture
group
carbon atoms
ester
Prior art date
Application number
KR1019940704427A
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English (en)
Other versions
KR100254624B1 (ko
Inventor
이. 쉬너 니콜라스
알. 질러 유겐
Original Assignee
웨인 씨. 제쉬크
헨켈 코포레이션(Hendel Corporation)
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from PCT/US1992/004438 external-priority patent/WO1993024585A1/en
Application filed by 웨인 씨. 제쉬크, 헨켈 코포레이션(Hendel Corporation) filed Critical 웨인 씨. 제쉬크
Priority claimed from PCT/US1993/004887 external-priority patent/WO1993024597A1/en
Publication of KR950701966A publication Critical patent/KR950701966A/ko
Application granted granted Critical
Publication of KR100254624B1 publication Critical patent/KR100254624B1/ko

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    • C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
    • C10M105/08—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing oxygen
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    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
    • C09K5/02—Materials undergoing a change of physical state when used
    • C09K5/04—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa
    • C09K5/041—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for compression-type refrigeration systems
    • C09K5/044—Materials undergoing a change of physical state when used the change of state being from liquid to vapour or vice versa for compression-type refrigeration systems comprising halogenated compounds
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Abstract

본 발명은 장애된 폴리올, 가장 바람직하게는 펜타에리트리톨과, 아디프산과 같은 이소-노난산 및 아디프산과 같은 이 염기산과 함게 최소한 몇개의 이소-펜탄산을 포함하는 카르복실산 혼합물과의 에스테르 혼합물에 의해 제공되는, 염소가 없는 히드로플루오로카아본 냉매 작용 유체를 사용하는, 용접 실링된 가정용 에어컨디셔너 및 냉각의 압축기용 고품질 윤활제에 관한 것이다.

Description

용접 실링 냉각 압축기용 폴리올 에스테르 윤활제( POLYOL ESTER LUBRICANTS FOR HERMETICALLY SEALED REFRIGERATING COMPRESSORS)
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (20)

  1. 40℃에서 약 22.5내지 약 44센티스토크의 점도를 갖는 액체이고 폴리올 에스테를 분자의 혼합물로 구성되는, 윤활제 또는 윤활제 원료로 사용하기에 적합한 물질의 조성물로서, 폴리올 에스테르 분자의 혼합물에서, 알콜부분의 최소한 약 92%가 TMP, DTMP, PE및 DPE부터 유도된 알코올 부분으로 구성된 군으로 부터 선택 되고, 아실기의 최소한 약 92%가 각각 C4내지 C127의 모든 직쇄 및 분지 1염기 및 2염기 카르복실산의 아실기로 구성된 군으로 부터 선택되며, 알코올 부분 및 아실기는 (a)혼합물 중에서, 최소한 총 3% 이상의 아실기가 i-C5산의 아실기이고; (b)8개 이상의 탄소 원자를 함유하고 분지되지 않은 혼합물 중의 아실기 % 대 6개 이하의 탄소 원자를 함유하고 분지된 혼합물 중의 아실기 %의 비가 1.56이하이고 : (c)분지되었거나 또는 그렇지 않은, 초소한 9개의 탄소 원자를 함유하는 혼합물 중의 아실기의 %가 약 81%이하이고; (d)에스테르 혼합물 중의 아실기의 약 2%이하가 각가 2개 이상의 카르복실기를 함유하고 ((d-1)혼합물내 산 분자의 최소한 약 20%가 트리메틸헥산산 중 하나이며; 에스테르 혼합물내 알콜 부분의 최소한 약 90%가 PE이며, 에스테르 혼합물내 아실기의 약 7.5% 이하가 이염기성 이거나; 또는 (d-2)에스테르 혼합물내 아실기의 약 2. 0내지 13%가 이염기성이고, 산 혼합물내 일염기성 아실기의 총 최소한 약 82%이상이 5또는 6개의 탄소원자를 갖는 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  2. 제1항에 있어서, 40℃에서 약 25.0내지 38.5센티스토크의 점도를 갖고 폴리올 에스테르 분자의 혼합물로 구성되며, 상기 알코올 부분 및 아실기는 (a)혼합물에서 아실기의 총 최소한 총 약 7%가 i-C5산이고; (b)8개 이상의 탄소 원자를 함유하고 분지되지 않은 혼합물중의 아실기의 %대 6개 이하의 탄소 원자를 함유하고 분지된 혼합물 중의 아실기 %의 비가 1.56이하이고; (c)분지되거나 또는 그렇지 않은, 9개 이상의 탄소 원자를 함유하는 혼합물 중의 아실기의 %가 약 67%이하이고; (d-1)혼합물내 산 분자의 최소한 약 29%가 트리메틸헥산 중 하나이며; 산 혼합물내 아실기의 6.0%이하가 이염기성이나; (d-2)에스테르 혼합물내 아실기의 약 2.8 내지 약 10%가 이 염기성이며, 에스테르 혼합물내 일염기성 아실기의 최소한 85%가 5개 또는 6개의 탄소 원자를 갖는 것으로 제한되도록 선택되는 것을 특징으로 하는 조성물.
  3. 제2항에 있어서, 40℃에서 약 27.4내지 약 37.6센터스토크의 점도를 갖고 폴리올 에스트르 분자의 혼합물로 구성되는 조성물로서, TMP, DTMP, PE, 및 DPE로 부터 유도된 알코올 부분으로 구성된 군으로 부터 알코올 부분의 최소한 약 95%가 선택되고, 아실기의 최소한 약 95%가 각각 4내지 12개의 탄소 원자를 갖는 모든 직쇄 및 측쇄 1염기성 및 2염기성 카르복실산의 아실기로 구성된 군으로 부터 선택되며, 상기 알코올 부분 및 아실기는, (a)혼합물 중에서 최소한 총 10%의 아실기가, i-C5산의 아실기이고; (b)8개 이상의 탄소원자를 함유하고 분지되지 않은 혼합물 중의 아실기의 %대 6개 이하의 탄소 원자를 함유하고 분지된 혼합물중의 아실기의 %의 비가 약 1.21이하이고; (c)분지되거나 그렇지 않은, 최소한 9개의 탄소 원자를 함유하는 에스테르 혼합물 중의 아실기의 %가 약 67%이하이고; (d)에스테르 혼합물중의 아실기 1%이하가 각각 2개 이상의
    카르복실기를 함유하고, (d-1)혼합물네 산 분자의 최소한 약 35%가 트리메틸헥산산중 하나이며; 에스테르 혼합물내 아실기의 약 3%이하가 이염기성이거나; (d-2)에스테르 혼합물내 아실기의 최소한 3.6%가 이염기성이며, 산 혼합물내 일염기성 아실기의 최소한 93%가 각각 5개의 탄소원자를 갖는 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  4. 제3항에 있어서, 40℃에서 약 28.5내지 약 36.6센티스토크의 점도를 갖고, 폴리올 에스테르 분자의 혼합물로 구성되는 조성물로서, 상기 알코올 부분 및 아실기가, (a)혼합물중의 치소한 약 14%의 아실기가 i-C5산이고; (b)8개 이상의 탄소원자를 함유하고 분지되지 않은 혼합물 중의 아실기의 %대 6개 이하의 탄소 원자를
    함유하고 분지된 혼합물중의 아실기의 %의 비가 1 : 00이하이며; (c)분지되거나 분지되지 않은 적어도 9개의 탄소원자를 함유하는 에스테르 혼합물 중의 아실기 %가 약 49%이하이고; (d)에스테르 혼합물 중의 아실기의 약 0.4%이하가 각각 2개 이상의 카르복실기를 함유하고, (d-1)혼합물내 산 분자의 최소한 약 35%가 트리메틸헥산산 중 하나이며; 혼합물내 아실기의 최소한 약 29%가 3, 5, 5-트리메틸헥사노일기이고, 에스테르 혼합물내 알콜부분의 최소한 약 95%가 PE이며, 에스테르 혼합물내 아실기의 1.7%가 이염기성이거나, 또는 ((d-2)에스테르 혼합물내 아실기의 최소한 4.1%가 이염기성이며, 각각 C5내지 C7의 탄소원자를 포함하고, 산 혼합물내 일염기성 아실기의 최소한 약 96%가 각각 5개의 탄소원자를 갖는 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  5. 제4항에 있어서, 40℃에서 약 29.4내지 35.7센티스토크의 점도를 갖고, 폴리올 에스테르 분자의 혼합물로 구성되는 조성물로서, 각각 4내지 12개의 탄소 원자를 갖는 모든 직쇄 및 측쇄 1염기성 및 2염기성 카르복실산의 아실기로 구성된 군으로 부터 아실기의 최소한 약 95%이상이 선택되며, 상기 알코올 부분 및 아실기는, (a)에스테르 흔함물중의 아실기의 최소한 충 51%이 i-C5산이고; (b)8개 이상의 탄소 원자를 함유하고 분지되지 않은 혼합물 중의 아실기 %대 6개 이하의 탄소 원자를 함유하고 분지된 혼합물 중의 아실기 %의 비가 1 : 00이하이며; (c)분지되거나 분지되지 않은 적어도 9개의 탄소 원자를 함유하는 에스테르 혼합물중의 아실기 %가 약 49%이하이고; (d)에스테르 혼합물내 알콜 부분의 최소한 약 95%가 PE이며, (d-1)에스테르 혼합물내 아실기의 최소한 약 41%가 트리메틸헥산산중 하나의 아실기이며 , 혼합물내 아실기의 최소한 약 29%가 3, 5, 5-트리메틸헥사노일기이고, 에스테르 혼합물내 아실기의 1%이하가 이염기성이며거나, 또는; (d-2)에스테르 혼합물내 아실기의 최소한 4.9%가 이염기성인 것으로 제한되도록 선택됨을 특징으로 하는 조성물.
  6. 최소한 약 95중량 %의 제5항에 따르는 조성물, 및 산화 방지성 및 열안정성 개량제, 부식 억제제, 금속 비활성화제, 윤활성 첨가제, 점성도 개선제, 용융점 강하제, 세척제, 분산제, 발포 방지제, 내마멸제 및 극압 저항성 첨가제로 구성된 군으로 부터 선택되는 나머지 중량 %의 하나 이상의 첨가제로 구성되는 배합 윤활제.
  7. 최초한 약 92중량 %의 제3항에 따르는 조성물, 산화 방지성 및 열안정성 개량제, 부식 억제제, 금속 비활성화제, 윤활성 첨가제, 점성도 개선제, 용융점 강하제, 세착제, 분산제, 발포방지제, 내마멸제 및 극압 저항성 첨가제로 구성된 군으로 부터 선택되는 나머지 중량%의 하나 이상의 텀가제로 구성되는 배합윤활제.
  8. 최소한 약 92중량%이상의 제2항에 따르는 조성물, 산화 방지성 및 열안정성 개량제, 부식 억제제, 금속 활성화제, 윤활성 첨가제, 점성도 개선제, 용융점 강하제, 세탁제, 분산제, 발포방지제, 내마멸제 및 극압 저항성 첨가제로 구성된 군으로 부터 선택되는 나머지 중량%의 하나 이상의 첨가제로 구성되는 배합윤활제.
  9. 최소한 약 92중량%의 제1항에 따르는 조성물 및 산화 방지성 및 열안정성 개량제. 금속 탈활성화제, 윤활성 첨가제, 부식 억제제, 점성도 개선제, 웅융점 강하제, 세척제, 분산제, 발포 방지제, 내마멸제 및 극압 저항성 첨가제로 구성된 군으로 부터 선택되는 나머지 중량 %의 하나 이상의 첨가제로 구성되는 배합윤활제.
  10. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄, 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85중량 %의 1차 열전달 유체 및 나머지 중량 %의 제9항에 따르는 윤활제로 구성되는 냉매작용 유체.
  11. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄, 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85중량 %의 1차 열전달 유체, 및 나머지 중량 %의 제8항에 따르는 윤활제로 구성되는 냉매작용 유체.
  12. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄, 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85중량 %의 1차 열전달 유체, 및 나머지 중량 %의 제7항에 따르는 윤활제로 구성되는 냉매작용 유체.
  13. 85중량 %이상의 1, 1, 1, 2-테트라플루오로에탄 및 나머지 중량 %의 제6항에 따르는 윤활제로 구성되는 냉매 작용 유체.
  14. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄, 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85중량%의 1차 열전달 유체, 및 나머지 중량 %의 제5항에 따르는 윤활제로 구성되는 냉매 작용 유체.
  15. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85 중량%이상의 1차 열전달 유체, 및 나머지 중량%의 제4항에 따르는 윤활제로 구성되는 냉매 작용 유체.
  16. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85 중량%이상의 1차 열전달 유체, 및 나머지 중량%의 제3항에 따르는 윤활제로 구성되는 냉매 작용 유체.
  17. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85 중량%이상의 1차 열전달 유체, 및 나머지 중량%의 제2항에 따르는 윤활제로 구성되는 냉매 작용 유체.
  18. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85 중량%이상의 1차 열전달 유체, 및 나머지 중량%의 제1항에 따르는 윤활제로 구성되는 냉매 작용 유체.
  19. 최소한 85중량 %의 1, 1, 2, 2-테트라플루오로에탄 및 나머지 중량 %의 제6항에 따르는 윤활제로 구성된 열전달 유체의 순환식 압축, 액화, 팽창 및 증발로 이루어지는 냉동기 조작 방법.
  20. 펜타플루오로에탄, 1, 1-디플루오로에탄, 1, 1, 1-트리플루오로에탄 테트라플루오로에탄 및 이들의 혼합물로 구성되는 군으로 부터 선택된 최소한 85 중량%이상의 1차 열전달 유체, 및 나머지 중량%의 제1항에 따르는 윤활제로 구성된 열전달 유체의 순환식 압축, 액화, 팽창 및 증발로 이루어지는 냉각기 조작 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019940704427A 1992-06-03 1993-05-27 용접 실링 냉각 압축기용 폴리올 에스테르 윤활제 KR100254624B1 (ko)

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USPCT/US92/04438 1992-06-03
WOPCT/US92/04438 1992-06-03
PCT/US1992/004438 WO1993024585A1 (en) 1992-06-03 1992-06-03 Polyol ester lubricants for refrigerant heat transfer fluids
US2762893A 1993-03-10 1993-03-10
US08/027,628 1993-03-10
US8/027628 1993-03-10
PCT/US1993/004887 WO1993024597A1 (en) 1992-06-03 1993-05-27 Polyol ester lubricants for hermetically sealed refrigerating compressors

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KR950701966A true KR950701966A (ko) 1995-05-17
KR100254624B1 KR100254624B1 (ko) 2000-05-01

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KR950005694B1 (ko) * 1989-07-05 1995-05-29 가부시끼가이샤 교오세끼 세이힝기주쓰 겡뀨쇼 냉각윤활제
JP2801703B2 (ja) * 1989-09-01 1998-09-21 花王株式会社 冷凍機油
US5021179A (en) * 1990-07-12 1991-06-04 Henkel Corporation Lubrication for refrigerant heat transfer fluids

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DE69327904D1 (de) 2000-03-30
HK1025595A1 (en) 2000-11-17

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