KR950000824A - 마이크로캡슐형 접착제의 제조방법 - Google Patents

마이크로캡슐형 접착제의 제조방법 Download PDF

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Publication number
KR950000824A
KR950000824A KR1019930010985A KR930010985A KR950000824A KR 950000824 A KR950000824 A KR 950000824A KR 1019930010985 A KR1019930010985 A KR 1019930010985A KR 930010985 A KR930010985 A KR 930010985A KR 950000824 A KR950000824 A KR 950000824A
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KR
South Korea
Prior art keywords
concentration
solvent
monomer
adhesive
organic solvent
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Application number
KR1019930010985A
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English (en)
Other versions
KR970000309B1 (ko
Inventor
박인환
민경석
박상철
Original Assignee
강박광
재단법인 한국화학연구소
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by 강박광, 재단법인 한국화학연구소 filed Critical 강박광
Priority to KR1019930010985A priority Critical patent/KR970000309B1/ko
Priority to US08/564,219 priority patent/US5827924A/en
Priority to PCT/KR1994/000073 priority patent/WO1994029603A1/en
Publication of KR950000824A publication Critical patent/KR950000824A/ko
Application granted granted Critical
Publication of KR970000309B1 publication Critical patent/KR970000309B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J9/00—Adhesives characterised by their physical nature or the effects produced, e.g. glue sticks
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02—Non-macromolecular additives
    • C09J11/06—Non-macromolecular additives organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/08—Macromolecular additives
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Manufacturing Of Micro-Capsules (AREA)

Abstract

본 발명은 볼트/너트나 나사에 사용되는 마이크로캡슐형 접착제의 제조방법에 관한 것으로 더욱 상세하게는 접착성분의 단량체, 개시제 및 유기용매등이 들어 있는 마이크로캡슐들을 용매활성화형 수지를 포함하는 또다른 접착성분의 단량체/올리고머, 코팅중진제, 커플링제, 비점착 부여제 및 유기용매 등의 바인더 용액과 함께 섞어서, 필요한 부위에 코팅, 건조하여 사용하는 것으로, 그 접착방식이 접착성분의 단량체/올리고머등에 의한 화학반응은 물론 캡슐내부의 유기용매와 용매활성화 수지간의 용매활성화 반응을 동시에 적용하는 방법이다.

Description

마이크로캡슐형 접착제의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제 1 도는 본 발명의 실시예 2에 얻은 마이크로캡슐화 되어 있는 혐기성 접착제가 바인더와 함께 볼트(bolt)에 코팅되어 있는 것을 나타낸 것이고, 제 2 도는 본 발명의 실시예 2에서 얻은 마이크로캡슐형 접착제와 시판되는 일본 THREE BOND사 동급 제품을 아연 도급한 볼트(직경 3/8in, 길이 1·1/4in)/너트에 적용, 25℃에서 체결(체결)하고, 24시간후의 접착강도(파괴-풀림 토오크)를 비교한 것이다.

Claims (1)

  1. 접착성분의 단량체, 산화제/환원제 조합의 유기개시제, 유기용매 등이 함유되어 있는 마이크로캡슐들을 만들고, 이들을 접착제로 이용하기 위하여 혼합될 바인더용액을 용매활성화형 수지, 또다른 접착성분의 단량체/올리고머, 코팅증진제, 커플링제, 비점착성 부여제 및 유기용매들을 구성하여 제조함에 있어서, 용매활성화 수지로는 클로로프렌 고무를 바인더 혼합용제에 대하여 0.5중량%-8중량% 농도로 사용하며, 폴리에스테르 아크릴레이트를 15중량%-25중량% 농도, 우레탄 아크릴레이트들을 10+중량%-25중량% 농도로 함께 사용하고, 코팅증진제로는 카르복시기 변성된 비닐클로라이드-비닐아세테이트 공중합체를 바인더용액에 대하여 5중량%-13중량% 농도로 사용하는 것을 특징으로 하는 마이크로캡슐형 접착제의 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019930010985A 1993-06-16 1993-06-16 마이크로 캡슐형 접착제의 제조방법 KR970000309B1 (ko)

Priority Applications (3)

Application Number Priority Date Filing Date Title
KR1019930010985A KR970000309B1 (ko) 1993-06-16 1993-06-16 마이크로 캡슐형 접착제의 제조방법
US08/564,219 US5827924A (en) 1993-06-16 1994-06-16 Polymer sealant microencapsulated by polyurethane reaction and its binder solution
PCT/KR1994/000073 WO1994029603A1 (en) 1993-06-16 1994-06-16 Polymer sealant microencapsulated by polyurethane reaction and its binder solution

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019930010985A KR970000309B1 (ko) 1993-06-16 1993-06-16 마이크로 캡슐형 접착제의 제조방법

Publications (2)

Publication Number Publication Date
KR950000824A true KR950000824A (ko) 1995-01-03
KR970000309B1 KR970000309B1 (ko) 1997-01-08

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ID=19357498

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019930010985A KR970000309B1 (ko) 1993-06-16 1993-06-16 마이크로 캡슐형 접착제의 제조방법

Country Status (1)

Country Link
KR (1) KR970000309B1 (ko)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101415433B1 (ko) * 2006-07-07 2014-07-04 섀플러 테크놀로지스 아게 운트 코. 카게 벨트 구동기용 인장 장치

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101415433B1 (ko) * 2006-07-07 2014-07-04 섀플러 테크놀로지스 아게 운트 코. 카게 벨트 구동기용 인장 장치

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Publication number Publication date
KR970000309B1 (ko) 1997-01-08

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