KR930012739A - Manufacturing method of diazo-type photosensitive member raw material - Google Patents

Manufacturing method of diazo-type photosensitive member raw material Download PDF

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Publication number
KR930012739A
KR930012739A KR1019910022029A KR910022029A KR930012739A KR 930012739 A KR930012739 A KR 930012739A KR 1019910022029 A KR1019910022029 A KR 1019910022029A KR 910022029 A KR910022029 A KR 910022029A KR 930012739 A KR930012739 A KR 930012739A
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KR
South Korea
Prior art keywords
formula
compound
reacted
reacting
ammonia
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KR1019910022029A
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Korean (ko)
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KR940002713B1 (en
Inventor
민병탁
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하기주
주식회사 코오롱
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Priority to KR1019910022029A priority Critical patent/KR940002713B1/en
Publication of KR930012739A publication Critical patent/KR930012739A/en
Application granted granted Critical
Publication of KR940002713B1 publication Critical patent/KR940002713B1/en

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/14—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D295/145—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals with the ring nitrogen atoms and the carbon atoms with three bonds to hetero atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

본 발명은 다음 일반식(Ⅳ)의 화합물과 다음 일반식(Ⅲ)의 화합물을 반응시켜서 다음 일반식(Ⅱ)의 화합물을 제조한 다음 이 일반식(Ⅱ)의 화합물을 암모니아와 반응시켜서 다음 일반식(Ⅰ)의 화합물을 제조하는 방법에 관한 것이며,The present invention is prepared by reacting a compound of formula (IV) with a compound of formula (III) to prepare a compound of formula (II), and then reacting the compound of formula (II) with ammonia To a method for preparing the compound of formula (I),

식중, R1및 R2는 같거나 다르며, 각각 탄소수 1-4의 잭쇄 또는 측쇄의 알킬 그룹이며, R3는 수소 또는 메틸기이며, Z는 산소 또는 탄소원자이며, X는 할로겐 원자이다.Wherein R 1 and R 2 are the same or different and are each a C 1-4 jack or branched alkyl group, R 3 is hydrogen or a methyl group, Z is oxygen or a carbon atom, and X is a halogen atom.

본 발명의 방법으로 일반식(Ⅰ)의 화합물을 높은 수율과 순도 및 낮은 코스트의 원료를 사용하여 제조할 수 있다.The compounds of general formula (I) can be prepared by the process of the invention using raw materials of high yield, purity and low cost.

Description

디아조타입 감광체 원료의 제조방법Manufacturing method of diazo-type photosensitive member raw material

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음As this is a public information case, the full text was not included.

Claims (5)

다음 일반식(Ⅳ)의 화합물과 다음 일반식(Ⅲ)의 화합물을 반응시켜서 다음 일반식(Ⅱ)의 화합물을 금속 또는 금속산화물존재하에 암모니아와 반응시켜서 다음 일반식(Ⅰ)의 화합물을 제조하는 방법.The following compound of formula (IV) is reacted with a compound of formula (III) to react a compound of formula (II) with ammonia in the presence of a metal or metal oxide to prepare a compound of formula (I) Way. 식중, R1및 R2는 같거나 다르며, 각각 탄소수 1-4의 잭쇄 또는 측쇄의 알킬 그룹이며, R3는 수소 또는 메틸기이며, Z는 산소 또는 탄소원자이며, X는 할로겐 원자이다.Wherein R 1 and R 2 are the same or different and are each a C 1-4 jack or branched alkyl group, R 3 is hydrogen or a methyl group, Z is oxygen or a carbon atom, and X is a halogen atom. 제1항에서 일반식(Ⅳ)의 화합물과 일반식(Ⅲ)의 화합물을 반응시킬 때 반응압력을 10-50kg/cm의 압력에서 반응시키는 방법.The method of claim 1 wherein the reaction pressure is reacted at a pressure of 10-50 kg / cm when the compound of formula (IV) and the compound of formula (III) are reacted. 제1항에서 일반식(Ⅳ)의 화합물과 일반식(Ⅲ)의 화합물을 반응시킬 때 반응온도를 150-200도의 온도에서 반응시키는 방법.The method of claim 1 wherein the reaction temperature is reacted at a temperature of 150-200 degrees when the compound of formula (IV) is reacted with a compound of formula (III). 제1항에서 일반식(Ⅱ)의 화합물과 암모니아를 반응시킬때 반응압력을 10-100kg/cm의 압력에서 반응시키는 방법.A method of reacting the reaction pressure at a pressure of 10-100 kg / cm when reacting the compound of Formula (II) with ammonia in claim 1. 제1항에서 일반식(Ⅱ)의 화합물과 암모니아를 반응시킬때 반응온도를 150-250도의 온도에서 반응시키는 방법.The method of claim 1 wherein the reaction temperature is reacted at a temperature of 150-250 degrees when the compound of formula (II) is reacted with ammonia. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019910022029A 1991-12-03 1991-12-03 Process for the preparation of photosensitive diazo-type compounds KR940002713B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019910022029A KR940002713B1 (en) 1991-12-03 1991-12-03 Process for the preparation of photosensitive diazo-type compounds

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1019910022029A KR940002713B1 (en) 1991-12-03 1991-12-03 Process for the preparation of photosensitive diazo-type compounds

Publications (2)

Publication Number Publication Date
KR930012739A true KR930012739A (en) 1993-07-21
KR940002713B1 KR940002713B1 (en) 1994-03-31

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Application Number Title Priority Date Filing Date
KR1019910022029A KR940002713B1 (en) 1991-12-03 1991-12-03 Process for the preparation of photosensitive diazo-type compounds

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210108993A (en) * 2018-12-27 2021-09-03 다이킨 고교 가부시키가이샤 Process for the preparation of cyclobutene

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210108993A (en) * 2018-12-27 2021-09-03 다이킨 고교 가부시키가이샤 Process for the preparation of cyclobutene

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Publication number Publication date
KR940002713B1 (en) 1994-03-31

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