KR920016561A - Preparation method of colored resin spherical fine particles and colored resin spherical fine particles - Google Patents

Preparation method of colored resin spherical fine particles and colored resin spherical fine particles Download PDF

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KR920016561A
KR920016561A KR1019910016360A KR910016360A KR920016561A KR 920016561 A KR920016561 A KR 920016561A KR 1019910016360 A KR1019910016360 A KR 1019910016360A KR 910016360 A KR910016360 A KR 910016360A KR 920016561 A KR920016561 A KR 920016561A
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inorganic pigment
fine particles
colored resin
spherical fine
group
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KR1019910016360A
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Korean (ko)
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KR950005306B1 (en
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사부로 나까하라
야스히로 야마모또
요오지 아까자와
마사오 바바
요시구니 모리
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다나까 쇼오소
가부시기가이샤 니뽄쇼꾸바이
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/20—Compounding polymers with additives, e.g. colouring
    • C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
    • C08J3/226—Compounding polymers with additives, e.g. colouring using masterbatch techniques using a polymer as a carrier
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/20—Compounding polymers with additives, e.g. colouring
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/44—Carbon
    • C09C1/48—Carbon black
    • C09C1/56—Treatment of carbon black ; Purification
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/10—Treatment with macromolecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
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    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
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    • C01P2006/80—Compositional purity
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/90—Other properties not specified above
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2361/00—Characterised by the use of condensation polymers of aldehydes or ketones; Derivatives of such polymers
    • C08J2361/20—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2461/00—Characterised by the use of condensation polymers of aldehydes or ketones; Derivatives of such polymers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

내용 없음No content

Description

착색수지 구상 미립자의 제조방법 및 착색수지 구상 미립자Preparation method of colored resin spherical fine particles and colored resin spherical fine particles

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

Claims (8)

아미노수지와 무기 안료를 혼합하여 유화시키고, 유화상태에서 중축합 반응을 행하며, 아미노수지 경화물과 무기 안료 합계량에 대해 안료비율이 1-30중량%이가 되도록 아미노수지 경화물과 무기 안료를 일체화시키는 것을 포함하는 것을 특징으로 하는 착색수지 구상미립자의 제조방법.The emulsified mixture of the amino resin and the inorganic pigment is emulsified, the polycondensation reaction is carried out in the emulsified state, and the cured amino resin and the inorganic pigment are integrated so that the pigment ratio is 1-30% by weight based on the total amount of the cured amino resin and the inorganic pigment. The manufacturing method of colored resin spherical fine particles containing the thing. 제1항에 있어서, 아미노수지가 벤조구아나민, 시클로헥산카르보구아나민 및 시클로헥센카르보구아나민으로 된 군에서 선택된 1종 이상의 구아나민이 40-100중량%을 차지하는 아미노 화합물과 포름 알데히드의 초기 반응생성물이고, 무기 안료가 카본 블랙이고 그 관능기와 반응성 및/또는 친화성을 갖는 관능기를 갖는 화합물로 처리되어 있는 것을 특징으로 하는착색수지 구상 미립자의 제조방법.The amino compound and formaldehyde of claim 1, wherein the amino resin is 40-100% by weight of at least one guanamine selected from the group consisting of benzoguanamine, cyclohexanecarboguamine and cyclohexenecarboguamine. A process for producing colored resin spherical fine particles, which is an initial reaction product and is treated with a compound having an inorganic pigment having carbon black and a functional group reactive and / or affinity with the functional group. 제2항에 있어서, 카본 블랙의 관능기와 반응성 및/또는 친화성을 갖는 관능기를 갖는 화합물이 하기 일반식(1), 즉The compound according to claim 2, wherein the compound having a functional group having a reactivity and / or affinity for a functional group of carbon black is represented by the following general formula (1), (다만, R은 수소원자이거나, 또는 치환기가 있어도 좋은 탄소수 1-20의 알킬기 및 불포화 지방족 잔기로 군에서 선택된적어도 1종의 기이고, n은 1-30의 정수임)으로 나타낸 폴리에틸렌 글리콜 글리시틸 에테르 화합물 및 그 유도체로된 군에서 선택된 적어도 하나인 것을 특징으로 하는 착색수지 구상 미립자의 제조방법.Polyethylene glycol glycidyl represented by (wherein R is a hydrogen atom or optionally substituted alkyl group and unsaturated aliphatic residue having 1 to 20 carbon atoms and at least one group selected from the group, n is an integer of 1-30) It is at least one selected from the group consisting of ether compounds and derivatives thereof. 제1항 내지 제3항중 어느 한항에 있어서, 유화제를 아미노 수지에 대해 1-30중량%의 범위에서 사용하는 것을 특징으로 하는 착색수지 구상 미립자의 제조방법.The method for producing colored resin spherical fine particles according to any one of claims 1 to 3, wherein an emulsifier is used in an amount of 1-30% by weight based on the amino resin. 아미노수지 경화물과 무기 안료가 일체화되고, 아미노수지 경화물과 무기안료 합계량에 대한 무기안료의 비율이 1-30중량%이며, 아미노수지 경화물은 벤조구아나민, 시클로헥산카르보구아나민 및 시클로헥센카르보구아나민으로 된 군에서 선택된 1종 이상의 구아나민이 40-100중량%를 차지하는 아미노 화합물과 포름알데히드의 반응 생성물이골, 무기 안료는 카본블랙이고 그 관능기와 반응성 및/또는 친화성을 갖는 화합물로 처리되어 있는 것을 특징으로 하는 착색수지 구상 미립자.The cured amino resin and the inorganic pigment are integrated, and the ratio of the inorganic pigment to the total cured amino resin and the inorganic pigment is 1-30% by weight, and the cured amino resin is benzoguanamine, cyclohexanecarboguamine and cyclo At least one guanamine selected from the group consisting of hexenecarboguamine is a reaction product of an amino compound with formaldehyde, which accounts for 40-100% by weight, and the inorganic pigment is carbon black and its functional and reactive and / or affinity Colored resin spherical microparticles | fine-particles which are processed by the compound which has. 제5항에 있어서, 무기 안료의 비율이 아미노수지 경화물과 무기 안료의 합계량에 대해 5-20중량%인 것을 특징으로 하는착색수지 구상 미립자.6. The colored resin spherical fine particles according to claim 5, wherein the proportion of the inorganic pigment is 5-20% by weight based on the total amount of the cured amino resin and the inorganic pigment. 제5항에 있어서, 0.1-50㎛범위의 평균 입자직경을 갖는 것을 특징으로 하는 착색수지 구상 미립자.6. The colored resin spherical fine particles according to claim 5, having an average particle diameter in the range of 0.1-50 mu m. 제5항 내지 제7항중 어느 한항에 있어서, 1.0-1.1 범위의 입자직경비(장경/단경)를 갖는 것을 특징으로 하는 착색수지 구상 미립자..8. The colored resin spherical fine particles according to any one of claims 5 to 7, having a particle diameter ratio (long diameter / short diameter) in the range of 1.0-1.1. ※ 참고사항 : 최초출원 내용에 의하여 공개되는 것임.※ Note: This is to be disclosed by the original application.
KR1019910016360A 1990-04-02 1991-09-19 Method for producing spherical fine particles of colored resin KR950005306B1 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP8481790 1990-04-02
JP3-30207 1991-02-25
JP3030207A JPH04211450A (en) 1990-04-02 1991-02-25 Fine spherical particle of colored resin and its production
JP03-030207 1991-02-25

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KR920016561A true KR920016561A (en) 1992-09-25
KR950005306B1 KR950005306B1 (en) 1995-05-23

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100543545B1 (en) 2000-12-28 2006-01-20 니폰 쇼쿠바이 컴파니 리미티드 Process for producing amino resin particles
TWI229094B (en) 2001-09-28 2005-03-11 Nippon Catalytic Chem Ind Amino resin crosslinked particles and producing process thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS585924B2 (en) * 1975-10-24 1983-02-02 株式会社日本触媒 thailand thorns
JPH02115271A (en) * 1988-10-25 1990-04-27 Sumitomo Naugatuck Co Ltd Resin molded

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