KR910019957A - 아민-말단을 갖는 화합물의 제조방법 - Google Patents

아민-말단을 갖는 화합물의 제조방법 Download PDF

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Publication number
KR910019957A
KR910019957A KR1019910007643A KR910007643A KR910019957A KR 910019957 A KR910019957 A KR 910019957A KR 1019910007643 A KR1019910007643 A KR 1019910007643A KR 910007643 A KR910007643 A KR 910007643A KR 910019957 A KR910019957 A KR 910019957A
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South Korea
Prior art keywords
organic
compound
acid
acetoacetate
group
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KR1019910007643A
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English (en)
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마포티 롭슨
샌더스 조셉
Original Assignee
죠셉 챨스 질
모베이 코포레이션
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Publication of KR910019957A publication Critical patent/KR910019957A/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/32—Polymers modified by chemical after-treatment
    • C08G65/329—Polymers modified by chemical after-treatment with organic compounds
    • C08G65/333—Polymers modified by chemical after-treatment with organic compounds containing nitrogen
    • C08G65/33303—Polymers modified by chemical after-treatment with organic compounds containing nitrogen containing amino group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/67—Unsaturated compounds having active hydrogen
    • C08G18/6795—Unsaturated polyethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/67—Unsaturated compounds having active hydrogen
    • C08G18/68—Unsaturated polyesters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/32—Polymers modified by chemical after-treatment
    • C08G65/321—Polymers modified by chemical after-treatment with inorganic compounds
    • C08G65/325—Polymers modified by chemical after-treatment with inorganic compounds containing nitrogen
    • C08G65/3255—Ammonia
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/32—Polymers modified by chemical after-treatment
    • C08G65/329—Polymers modified by chemical after-treatment with organic compounds
    • C08G65/331—Polymers modified by chemical after-treatment with organic compounds containing oxygen
    • C08G65/332—Polymers modified by chemical after-treatment with organic compounds containing oxygen containing carboxyl groups, or halides, or esters thereof
    • C08G65/3322—Polymers modified by chemical after-treatment with organic compounds containing oxygen containing carboxyl groups, or halides, or esters thereof acyclic

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Peptides Or Proteins (AREA)

Abstract

내용 없음

Description

아민-말단을 갖는 화합물의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (8)

  1. 용매 및 (i)보론 트리플루오라이드 에테레이트와 (ⅱ)0.1내지 0.8의pKa값을 갖는 유기산( 단, 일차 아미노그룹을 함유한 화합물이 방향족 상태로 결합한 아미노 그룹을 함유하지 않는다면, 상기 유기산의pKa값은 0.1내지 0.7미만이다)으로 구성된 그룹으로부터 선택된 산성 촉매 존재하에, 다중작용성 아세토아세트산 에스테르를 암모니아 또는 하나 이상의 일차 아미노그룹을 함유하는 유기 화합물과 반응시킴을 특징으로 하여, 아민-말단을 갖는 화합물을 제조하는 방법.
  2. 제1항에 있어서, 상기 유기산이 할로겐화된 유기 카복실산인 방법.
  3. 제2항에 있어서, 상기 유기산이 할로겐화된 아세트산인 방법
  4. 제3항에 있어서, 상기 유기산이 트리플루오로아세트산인 방법
  5. 제1항에 있어서, 1몰의 아세토아세테이트가 각각의 하이드록실 그룹에 사용되도록하는 비율로, C1내지 C5알킬 아세토아세테이트 2내지 6개의 하이드록시 그룹을 함유하며 192내지 8000의 분자량을 갖는 유기 화합물과 반응시켜 다중작용성 아세토아세트산 에스테르를 제조하는 방법.
  6. 제5항에 있어서, 1몰의 아세토아세테이트가 각각의 하이드록실 그룹에 사용되도록하는 비율로, C1내지 C5알킬 아세토아세테이트 2내지 6개의 하이드록시 그룹을 함유하며 192내지 8000의 분자량을 갖는 유기 화합물과 반응시켜, 다중작용성 아세토아세트산 에스테르를 제조하는 방법.
  7. 제1항에 있어서, 유기 화합물이 방향족 디아민인 방법.
  8. 제7항에 있어서, 방향족 디아민이 톨루엔디아민, 알킬-치환된 톨루엔디아민, 메틸렌비스(페닐아민), 알킬-치환된 메닐렌비스(페닐아민), 1,5-나프탈렌디아민 및 페닐렌 디아민으로 구성된 그룹으로부터 선택되는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019910007643A 1990-05-15 1991-05-13 아민-말단을 갖는 화합물의 제조방법 KR910019957A (ko)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US524,268 1983-08-18
US52426890A 1990-05-15 1990-05-15
US07/562,293 US5066824A (en) 1990-05-15 1990-08-03 Novel process for the preparation of amine-terminated compounds
US562293 1990-08-03

Publications (1)

Publication Number Publication Date
KR910019957A true KR910019957A (ko) 1991-12-19

Family

ID=27061442

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019910007643A KR910019957A (ko) 1990-05-15 1991-05-13 아민-말단을 갖는 화합물의 제조방법

Country Status (9)

Country Link
US (1) US5066824A (ko)
EP (1) EP0457129B1 (ko)
JP (1) JPH04226951A (ko)
KR (1) KR910019957A (ko)
AT (1) ATE117329T1 (ko)
BR (1) BR9101963A (ko)
CA (1) CA2039941A1 (ko)
DE (1) DE69106773T2 (ko)
ES (1) ES2069114T3 (ko)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5231217A (en) * 1991-03-20 1993-07-27 Miles Inc. Process for the preparation of amine-terminated compounds
US5180857A (en) * 1992-03-10 1993-01-19 E. I. Du Pont De Nemours And Company Reduction of molecular weight of poly(tetramethylene ether) glycol
US5368806A (en) * 1992-11-05 1994-11-29 Miles Inc. Production of moldings by the reaction injection molding process
AU675252B2 (en) * 1992-12-18 1997-01-30 Tremco, Inc. Fast-curing, high strength, two-part sealants using acetoacetate-amine cure chemistry
US5321118A (en) * 1993-09-30 1994-06-14 Eastman Chemical Company 1-acetoacetamido-2,3-propane diol monomer and polyesters prerpared therefrom
US5464920A (en) * 1994-07-05 1995-11-07 Bayer Corporation Cast elastomers prepared from aminocrotonates
US5516872A (en) * 1994-07-05 1996-05-14 Bayer Corporation Preparation of cast elastomers using aminocrotonate-terminated polyether chain extenders
US5714563A (en) * 1996-01-16 1998-02-03 Depompei; Michael Frederick One-part, low viscosity, moisture curable composition
US20050131136A1 (en) 2003-12-16 2005-06-16 Rosthauser James W. Soft polyurethaneurea spray elastomers with improved abrasion resistance
US20070098997A1 (en) 2005-11-02 2007-05-03 Bayer Materialscience Llc Composite articles and a process for their production
US20070105970A1 (en) * 2005-11-10 2007-05-10 Kenneth Warnshuis Energy absorbing flexible foam
PL2387490T3 (pl) 2009-01-14 2016-01-29 Bayer Materialscience Llc Kompozyt termoutwardzalny o długich włóknach z małym efektem skórki pomarańczowej, sposób otrzymywania i zastosowanie tego kompozytu
US20100216903A1 (en) 2009-02-20 2010-08-26 Bayer Materialscience Llc Foam-forming system with reduced vapor pressure
WO2020025422A1 (de) * 2018-07-30 2020-02-06 Sika Technology Ag Polyurethanzusammensetzung mit langer verarbeitungszeit und hoher festigkeit
CN114080411A (zh) * 2019-07-10 2022-02-22 科思创有限公司 聚醚及其在制备柔性聚氨酯泡沫中的用途

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1158496B (de) * 1961-01-20 1963-12-05 Bayer Ag Verfahren zur Herstellung von N, N', N'-trisubstituierten p-Phenylendiaminen
DE1935485A1 (de) * 1969-07-12 1971-01-21 Bayer Ag Verfahren zur Herstellung von Polyamiden mit Urethan- und/oder Harnstoffgruppierungen
DE1935484A1 (de) * 1969-07-12 1971-01-14 Bayer Ag Verfahren zur Herstellung von Polyamiden
JPS5331857B1 (ko) * 1971-02-20 1978-09-05
DE2658401A1 (de) * 1976-12-23 1978-07-06 Merck Patent Gmbh Cyclopentan-1-amine, verfahren zu ihrer herstellung und diese verbindungen enthaltende mittel

Also Published As

Publication number Publication date
EP0457129A3 (en) 1991-12-18
EP0457129A2 (en) 1991-11-21
CA2039941A1 (en) 1991-11-16
JPH04226951A (ja) 1992-08-17
ES2069114T3 (es) 1995-05-01
BR9101963A (pt) 1991-12-24
US5066824A (en) 1991-11-19
DE69106773D1 (de) 1995-03-02
DE69106773T2 (de) 1995-05-18
EP0457129B1 (en) 1995-01-18
ATE117329T1 (de) 1995-02-15

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