KR910006622B1 - Process for extracting from shrimps - Google Patents
Process for extracting from shrimps Download PDFInfo
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- KR910006622B1 KR910006622B1 KR1019890019782A KR890019782A KR910006622B1 KR 910006622 B1 KR910006622 B1 KR 910006622B1 KR 1019890019782 A KR1019890019782 A KR 1019890019782A KR 890019782 A KR890019782 A KR 890019782A KR 910006622 B1 KR910006622 B1 KR 910006622B1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
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Abstract
Description
본 발명은 새우엑기스 제조시에 효소반응후에 남는 잔사를 건조하여 효소반응 상등액에 첨가함으로서 수율이 높고 풍미가 우수한 새우엑기스 제조방법에 관한 것이다.The present invention relates to a method for producing shrimp extracts having high yield and excellent flavor by drying the residues remaining after the enzyme reaction during the preparation of shrimp extracts and adding them to the supernatant of the enzyme reaction.
새우엑기스의 산업적 제조방법은 열수추출, 효소반응 또는 이 두가지 방법을 모두 이용하고 있으나, 어느 방법이든간에 공정중 여과하는 과정에서 잔사가 생성되며 이 잔사는 주성분이 키틴질인 새우의 각질부분이며, 또한 표 1과 같이 새우의 맛성분과 기타 영양분이 잔존하지만 대부분 사료로 처리되어지고 있다.The industrial production of shrimp extract uses hot water extraction, enzymatic reaction, or both methods, but either method produces a residue in the process of filtration, and this residue is a keratinous part of shrimp whose main component is chitin. As shown in Table 1, shrimp's flavor components and other nutrients remain, but most are processed into feed.
따라서 통상의 새우엑기스 제조방법으로는 잔사를 재이용하지 못하고 있는바, 수율이 매우 낮고, 새우의 독특한 맛과 영양이 유실되고 있다.Therefore, the conventional shrimp extract manufacturing method does not reuse the residue, the yield is very low, the unique taste and nutrition of the shrimp is lost.
이런 단점을 해소하기 위해 부분적으로 덱스트린, 전분등의 부용제를 첨가하여 최종 제품의 수율은 다소 증진시키지만 수율의 원만한 증진을 기대치 못하고 있으며 고유의 맛과 향미가 매우 떨어지게 된다.In order to alleviate this drawback, a partial addition of dextrin, starch, etc., may be used to improve the yield of the final product, but it is not expected to increase the yield smoothly and the inherent taste and flavor will be very poor.
본 발명에서는 상기와 같은 점을 개선하기 위하여 대부분 사료로 처리되고 있는 새우엑기스 제조시의 부산물인 잔사를 재이용하여 새우엑기스의 생산성과 풍미를 높이기 위하여 이런 잔사를 동결건조나 열풍건조 또는 진공건조등의 방법을 이용하여 건조한 뒤 이를 새우엑기스 제조시에 첨가하여 폐기물이 전혀 생성되지 않고 생새우 원료를 모두 이용함으로서 수율면에 있어서 기존의 효소 분해 공법에 의한 수율보다 약 43% 증가하였으며, 잔사의 건조에 따른 새우의 맛과 향미가 보강되어 단백질 36.4% 아미노테질소 8.1%가 증가하는등 품질이 우수한 새우 엑기스를 제공하는데 그 목적이 있다.In the present invention, in order to improve the above points, the residue is reused as a by-product of the preparation of shrimp extracts, which are mostly processed as feed, to increase the productivity and flavor of the shrimp extracts, such as freeze drying, hot air drying or vacuum drying. After drying by using the method, it was added at the time of producing the shrimp extract, so that no waste was produced and all raw shrimp raw materials were used, and the yield was increased by about 43% compared to the yield by the conventional enzymatic digestion method. Its purpose is to provide shrimp extracts of high quality, with the added flavor and flavor of shrimp being increased by 36.4% aminotenitrogen by 8.1%.
[표 1]TABLE 1
이하 본 발명의 제조방법을 구체적으로 설명하면 다음과 같다.Hereinafter, the manufacturing method of the present invention will be described in detail.
본 발명은 꽃새우(pink shrimp)와 중하새우(shiba shrimp)를 용기에 넣고 물을 넣은 다음 오토클레이브(autoclave)에서 118-120℃의 온도로 0.5-2.0시간 쿠킹(cooking)한다.In the present invention, pink shrimp and shrimp shrimp are placed in a container, and water is cooked in a autoclave at a temperature of 118-120 ° C. for 0.5-2.0 hours.
쿠킹이 끝난 후 이를 효소반응조에 넣고 상업용 단백분해 효소인 프로틴 에이와이 텐(protin AY 10)을 원료새우의 생물량에 대해 0.1-1.0% 첨가한 뒤 50-55℃온도에서 0.5-3.0시간 효소반응 시킴으로서 37.3%의 단백분해율(a-N/T-N)을 얻을 수 있었다.After cooking, put it in the enzyme reaction tank and add the protein of protein protin AY 10 (protin AY 10) 0.1-1.0% of biomass of raw shrimp and enzymatic reaction at 50-55 ℃ for 0.5-3.0 hours. Proteolysis (aN / TN) of 37.3% was obtained.
효소반응이 끝난 후 100℃ 열탕에서 10분간 넣고 효소를 불활성시킨 다음 분당 8.000회의 회전속도로 원심분리하여 새우반응액에 대해 상등액 83%, 잔사 17%의 비율로 분리하였다.After the enzymatic reaction, the mixture was placed in a 100 ° C. hot water for 10 minutes, and the enzyme was inactivated, followed by centrifugation at a rotational speed of 8.000 times per minute to separate the supernatant 83% and the residue 17%.
이렇게 하여 얻은 잔사를 영하 20℃의 냉동고에서 예비 동결시킨 다음 동결건조기를 이용하여 40℃에서 20시간 동결건조하거나, 캐비넷 건조기를 이용하여 60℃에서 10시간 열풍건조하거나, 진공건조기를 이용하여 70℃에서 5시간 진공건조시킨다.The residue thus obtained is preliminarily frozen in a freezer at minus 20 ° C. and then lyophilized at 40 ° C. for 20 hours using a freeze dryer, hot air dried at 60 ° C. for 10 hours using a cabinet dryer, or 70 ° C. using a vacuum dryer. Vacuum dry at 5 hours.
이와 같이 건조된 잔사를 유발에서 곱게 갈아 분쇄한 후 50메쉬(mesh) 표준체를 이용하여 체질함으로서 잔사를 모두 회수하였다. 이렇게 회수된 잔사를 효소반응 상등액에 혼합하여 진공 농축함으로서 갈색의 새우엑기스가 제조된다.Thus, the dried residue was ground finely ground in a mortar and then sieved using a 50 mesh (mesh) standard to recover all the residue. The residue thus recovered is mixed with the enzyme reaction supernatant and concentrated in vacuo to give a brown shrimp extract.
이와 같이 제조된 시료를 비교적 그 맛에 익숙한 시식요원 30명을 대상으로 관능검사를 하여 새우의 맛과 향미가 제일 좋다고 느끼는 선호도를 조사한 결과 표 2와 같았다.As a result of examining the sensory taste and flavor of the shrimp, the sample prepared as described above was examined in 30 taste agents who are relatively familiar with the taste.
표 2 관능검사를 통한 선호도Table 2 Preference through Sensory Testing
상기 표 2와 같이 잔사의 건조방법중에서 열풍건조나 진공건조에 비해 동결건조하여 첨가한 새우엑기스 제품에서 고유한 맛과 향미를 느끼는 선호도가 높았다.As shown in Table 2, the preference for feeling the unique taste and flavor in the shrimp extract product added by freeze drying compared to hot air drying or vacuum drying in the drying method of the residue.
이와 같이 새우엑기스 제조시에 부산물로 생성되는 잔사를 건조하여 재이용함으로서 폐기물이 전혀 생성되지 않고 수율이 높으며, 풍미가 우수한 새우엑기스를 제조함으로서 스낵, 스프 베이스, 조미료, 기타 식품첨가물에 이용되는 우수한 새우엑기스를 제공할 수 있다.As a result, the residue produced as a by-product in the manufacture of shrimp extract is dried and reused to produce shrimp extract with high yield and excellent flavor, making excellent shrimp used for snacks, soup bases, seasonings and other food additives. Can provide an extract.
다음은 실시예를 통하여 본 방법을 설명키로 한다.The following describes the method through an embodiment.
[실시예 1]Example 1
꽃새우 300그램과 중하새우 150그램을 용기에 넣고 물 225그램을 가해 오토클레이브(autoclave)에서 118℃-120℃ 온도로 1시간 쿠킹(cooking)한 다음, 상온에서 50℃로 식혀 효소반응조에 넣고, 상업용 단백분해효소인 프로틴 에이와이 텐(protin AY 10)을 2.25그램 넣는다. 분당 회전속도가 60회인 항온반응조에서 반응온도 50℃로 2시간 효소반응시켰다.Place 300 grams of shrimp and 150 grams of Shrimp shrimp in a container, add 225 grams of water, cook for 1 hour at 118 ℃ -120 ℃ in an autoclave, cool to 50 ℃ at room temperature and place in an enzyme reaction tank. Add 2.25 grams of protin AY 10, a commercial protease. Enzymatic reaction was carried out at a reaction temperature of 50 ° C. for 2 hours in an incubator having a rotational speed of 60 times per minute.
효소반응이 끝난 후, 100℃열탕에서 10분간 넣고 효소를 불활성화 시킨 다음, 분당 8,000회의 회전속도로 원심분리를 하여 상등액 560그램과 잔사 95그램을 얻었다. 이 잔사 95그램을 냉동고에 넣고 영하 20℃의 온도로 예비동결시킨 후에 동결건조기에 넣고 40℃에서 20시간 온도로 예비동결시킨 후에 동결건조기에 넣고 40℃에서 20시간 동결건조한 뒤에, 이것을 분쇄기로 분쇄하고 50메쉬(mesh) 표준체로 체질을 하여 고운 가루상태의 잔사 36그램을 얻었다. 이 가루상태의 새우잔사 36그램을 효소반응 상등액 560그램과 혼합하여 진공 농축함으로서 풍미가 우수한 새우엑기스(수분함량 50%) 200그램을 얻었다. 표준시료로서 효소반응 상등액 560그램만을 그대로 진공농축하여 만든 새우엑기스(수분함량 50%) 140그램과 비교하여 볼 때, 제품수율이 42.8% 상승하였다.After the enzyme reaction was completed, the mixture was placed in a 100 ° C. hot water for 10 minutes to inactivate the enzyme, and then centrifuged at 8,000 revolutions per minute to obtain 560 g of supernatant and 95 g of residue. 95 grams of the residue was put in a freezer, pre-frozen at a temperature of minus 20 ° C., then placed in a freeze dryer, pre-frozen at 40 ° C. for 20 hours, then placed in a lyophilizer, lyophilized at 40 ° C. for 20 hours, and then crushed by a grinder. The resultant was sieved using a 50 mesh standard to obtain 36 grams of fine powdery residue. 36 grams of this powdered shrimp residue was mixed with 560 grams of the enzyme reaction supernatant and concentrated in vacuo to obtain 200 grams of shrimp extract (50% water content) with excellent flavor. Compared to 140 grams of shrimp extract (50% moisture content), which was made by vacuum concentration of only 560 grams of the enzyme reaction supernatant as a standard sample, the product yield increased by 42.8%.
[실시예 2]Example 2
꽃새우 300그램과 중하새우 150그램을 용기에 넣고 물 225그램을 가해 오토클레이브(autoclave)에서 118℃-120℃ 온도로 1시간 쿠킹(cooking)한 다음, 상온에서 50℃로 식혀 효소반응조에 넣고, 상업용 단백분해효소인 프로틴 에이와이 텐(protin AY 10)을 2.25그램 넣는다. 분당 회전속도가 60회인 항온반응조에서 반응온도 50℃로 2시간 효소반응시켰다.Place 300 grams of shrimp and 150 grams of Shrimp shrimp in a container, add 225 grams of water, cook for 1 hour at 118 ℃ -120 ℃ in an autoclave, cool to 50 ℃ at room temperature and place in an enzyme reaction tank. Add 2.25 grams of protin AY 10, a commercial protease. Enzymatic reaction was carried out at a reaction temperature of 50 ° C. for 2 hours in an incubator having a rotational speed of 60 times per minute.
효소반응이 끝난 후, 100℃ 열탕에서 10분간 넣고 효소를 불활성화 시킨 다음, 분당 8,000회의 회전속도로 원심분리를 하여 상등액 560그램과 잔사 95그램을 얻었다.After the enzyme reaction was completed, the mixture was placed in a 100 ° C. hot water for 10 minutes to inactivate the enzyme, and then centrifuged at 8,000 revolutions per minute to obtain 560 g of supernatant and 95 g of residue.
이 잔사 95그램을 캐비넷 건조기에 넣고 60℃에서 10시간 열풍 건조한 뒤에 이것을 분쇄기로 분쇄하고 50메쉬(mesh) 표준체로 체질을 하여 고운 가루상태의 잔사 36그램을 얻었다.95 grams of the residue was put in a cabinet drier and hot-air dried at 60 ° C. for 10 hours, and then pulverized with a pulverizer and sieved with a 50 mesh standard to obtain 36 grams of fine powdery residue.
이 가루상태의 새우잔사 36그램을 효소반응 상등액 560그램과 혼합하여 진공농축함으로서 풍미가 우수한 새우엑기스(수분함량 50%) 200그램을 얻었다. 표준시료로서 효소반응 상등액 560그램만을 그대로 진공 농축하여 만든 새우엑기스(수분함량 50%) 140그램과 비교하여 볼 때 제품수율이 42.8% 상승하였다.36 grams of this powdered shrimp residue was mixed with 560 grams of the enzyme reaction supernatant to obtain 200 grams of shrimp extract (50% water content) with excellent flavor. As a standard sample, the product yield increased by 42.8% compared with 140 grams of shrimp extract (50% moisture content) made by vacuum concentration of only 560 grams of the enzyme reaction supernatant.
[실시예 3]Example 3
꽃새우 300그램과 중하새우 150그램을 용기에 넣고 물 225그램을 가해 오토클레이브(autoclave)에서 118℃-120℃ 온도로 1시간 쿠킹(cooking)한 다음, 상온에서 50℃로 식혀 효소반응조에 넣고, 상업용 단백분해효소인 프로틴 에이와이 텐(protin AY 10)을 2.25그램 넣는다. 분당 회전속도가 60회인 항온반응조에서 반응온도 50℃로 2시간 효소반응시켰다.Place 300 grams of shrimp and 150 grams of Shrimp shrimp in a container, add 225 grams of water, cook for 1 hour at 118 ℃ -120 ℃ in an autoclave, cool to 50 ℃ at room temperature and place in an enzyme reaction tank. Add 2.25 grams of protin AY 10, a commercial protease. Enzymatic reaction was carried out at a reaction temperature of 50 ° C. for 2 hours in an incubator having a rotational speed of 60 times per minute.
효소반응이 끝난 후, 100℃ 열탕에서 10분간 넣고 효소를 불활성화 시킨 다음, 분당 8,000회의 회전속도로 원심분리를 하여 상등액 560그램과 잔사 95그램을 얻었다. 이 잔사 95그램을 진공건조기에 넣고 70℃에서 5시간 진공건조한 뒤에 이것을 분쇄기로 분쇄하고 50메쉬(mesh) 표준체로 체질을 하여 고운 가루상태의 잔사 36그램을 얻었다. 이 가루상태의 새우잔사 36그램을 효소반응 상등액 560그램과 혼합하여 진공농축함으로서 풍미가 우수한 새우엑기스(수분함량 50%) 200그램을 얻었다. 표준시료로서 효소반응 상등액 560그램만을 그대로 진공농축하여 만든 새우엑기스(수분함량 50%) 140그램과 비교하여 볼 때 제품수율이 42.8% 상승하였다.After the enzyme reaction was completed, the mixture was placed in a 100 ° C. hot water for 10 minutes to inactivate the enzyme, and then centrifuged at 8,000 revolutions per minute to obtain 560 g of supernatant and 95 g of residue. 95 grams of this residue was put in a vacuum dryer, vacuum dried at 70 DEG C for 5 hours, and then pulverized with a pulverizer and sieved with a 50 mesh standard to obtain 36 grams of fine powdery residue. 36 grams of this powdered shrimp residue was mixed with 560 grams of the enzyme reaction supernatant to obtain 200 grams of shrimp extract (50% water content) with excellent flavor. As a standard sample, the product yield increased by 42.8% compared to 140 grams of shrimp extract (50% moisture content) made by vacuum concentration of only 560 grams of the enzyme reaction supernatant.
[실시예 4]Example 4
꽃새우 300그램과 중하새우 150그램을 용기에 넣고 물 225그램을 가해 그대로 효소반응조에 넣고 상업용 단백분해효소인 프로틴 에이와이 텐(protin AY 10)을 2.25그램 넣는다.300 grams of shrimp and 150 grams of Shrimp shrimp are placed in a container, 225 grams of water is added to the enzyme reactor, and 2.25 grams of protein AY 10, a commercial protease.
분당 회전속도가 60회인 항온반응조에서 반응온도 50℃로 2시간 효소반응시켰다. 효소반응이 끝난 후, 100℃ 열탕에서 10분간 넣고 효소를 불활성화 시킨 다음, 분당 8,000회의 회전속도로 원심분리를 하여 상등액 560그램과 잔사 95그램을 얻었다. 이 잔사 95그램을 냉동고에 넣고 영하 20℃의 온도로 예비동결시킨 후에 동결건조기에 넣고 40℃에서 20시간 동결건조시켰다.Enzymatic reaction was carried out at a reaction temperature of 50 ° C. for 2 hours in an incubator having a rotational speed of 60 times per minute. After the enzyme reaction was completed, the mixture was placed in a 100 ° C. hot water for 10 minutes to inactivate the enzyme, and then centrifuged at 8,000 revolutions per minute to obtain 560 g of supernatant and 95 g of residue. 95 grams of this residue was placed in a freezer, pre-frozen at a temperature of minus 20 ° C., then placed in a freeze dryer, and freeze-dried at 40 ° C. for 20 hours.
이것을 분쇄기로 분쇄하고 50메쉬(mesh) 표준체로 체질을 하여 고운 가루상태의 잔사 36그램을 얻었다. 이 가루상태의 새우잔사 36그램을 효소반응 상등액 560그램과 혼합하여 진공농축함으로서 풍미가 우수한 새우엑기스(수분함량 50%) 200그램을 얻었다. 표준시료로서 효소반응 상등액 560그램만을 그대로 진공 농축하여 만든 새우엑기스(수분함량 50%) 140그램과 비교하여 볼 때 제품수율이 42.8% 상승하였다.This was pulverized with a grinder and sieved to a 50 mesh standard to obtain 36 grams of fine powdery residue. 36 grams of this powdered shrimp residue was mixed with 560 grams of the enzyme reaction supernatant to obtain 200 grams of shrimp extract (50% water content) with excellent flavor. As a standard sample, the product yield increased by 42.8% compared with 140 grams of shrimp extract (50% moisture content) made by vacuum concentration of only 560 grams of the enzyme reaction supernatant.
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KR1019890019782A KR910006622B1 (en) | 1989-12-28 | 1989-12-28 | Process for extracting from shrimps |
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KR1019890019782A KR910006622B1 (en) | 1989-12-28 | 1989-12-28 | Process for extracting from shrimps |
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WO2012108593A1 (en) * | 2011-02-11 | 2012-08-16 | 대덕에프알디(주) | Method for producing krill oil, and krill oil produced by the method |
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WO2012108593A1 (en) * | 2011-02-11 | 2012-08-16 | 대덕에프알디(주) | Method for producing krill oil, and krill oil produced by the method |
CN103501623A (en) * | 2011-02-11 | 2014-01-08 | 大德Frd有限公司 | Method for producing krill oil, and krill oil produced by the method |
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