KR910006227A - 크로토노베타인히드로클로리드의 제조방법 - Google Patents
크로토노베타인히드로클로리드의 제조방법 Download PDFInfo
- Publication number
- KR910006227A KR910006227A KR1019900013847A KR900013847A KR910006227A KR 910006227 A KR910006227 A KR 910006227A KR 1019900013847 A KR1019900013847 A KR 1019900013847A KR 900013847 A KR900013847 A KR 900013847A KR 910006227 A KR910006227 A KR 910006227A
- Authority
- KR
- South Korea
- Prior art keywords
- hydrochloride
- crotonobine
- preparing
- acetic anhydride
- reaction
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/30—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and unsaturated
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
- C07C227/16—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions not involving the amino or carboxyl groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Steroid Compounds (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (5)
- 90 내지 130℃에서 산성촉매의 존재하에 라세미체로서 또는 거울상 이성질체의 형으로서의 카르니틴히드로 클로리드를 아세트산 무수물 1.5 내지 15몰과 반응시키는 것을 특징으로 하는 크로토노베타인히드로콜로리드의 제조방법.
- 제1항에 있어서, 1.8내지 2몰의 아세트산 무수물을 사용하는 것을 특징으로 하는 방법.
- 제1항 또는 제2하에 있어서, 사용된 카르니틴히드로클로리드에 대해 0.5내지 2중량%의 p-톨루엔술폰산을 산성 촉매로서 사용하는 것을 특징으로 하는 방법.
- 제1항 내지 제3항중 어느 하나에 있어서, 110 내지 125℃에서 반응시키는 것을 특징으로 하는 방법.
- 제1항 내지 제4하중 어느 하나에 있어서, 반응이 종결된 후 반응혼합물로 저급 지방족 알코올을 첨가한 다음 냉각시킴으로써 크로토노베타인히드로클로리드를 침전 및 단리하는 것을 특징으로 하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH3253/89 | 1989-09-07 | ||
CH325389 | 1989-09-07 |
Publications (1)
Publication Number | Publication Date |
---|---|
KR910006227A true KR910006227A (ko) | 1991-04-27 |
Family
ID=4251970
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019900013847A KR910006227A (ko) | 1989-09-07 | 1990-08-31 | 크로토노베타인히드로클로리드의 제조방법 |
Country Status (15)
Country | Link |
---|---|
EP (1) | EP0416583B1 (ko) |
JP (1) | JPH03106853A (ko) |
KR (1) | KR910006227A (ko) |
AT (1) | ATE83768T1 (ko) |
CA (1) | CA2023744A1 (ko) |
CZ (1) | CZ278017B6 (ko) |
DD (1) | DD295340A5 (ko) |
DE (1) | DE59000657D1 (ko) |
DK (1) | DK0416583T3 (ko) |
ES (1) | ES2036386T3 (ko) |
FI (1) | FI904363A0 (ko) |
HU (1) | HU205065B (ko) |
IE (1) | IE64605B1 (ko) |
IL (1) | IL95571A (ko) |
NO (1) | NO173731C (ko) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4713348B2 (ja) * | 2006-01-13 | 2011-06-29 | 日本電産サンキョー株式会社 | 永久磁石型同期モータ |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1190280B (it) * | 1986-04-24 | 1988-02-16 | Sigma Tau Ind Farmaceuti | Procedimento per la preparazione di gamma-butirrobetaina |
-
1990
- 1990-08-22 CA CA002023744A patent/CA2023744A1/en not_active Abandoned
- 1990-08-27 IE IE311190A patent/IE64605B1/en not_active IP Right Cessation
- 1990-08-31 KR KR1019900013847A patent/KR910006227A/ko not_active Application Discontinuation
- 1990-08-31 JP JP2232312A patent/JPH03106853A/ja active Pending
- 1990-09-03 IL IL9557190A patent/IL95571A/en not_active IP Right Cessation
- 1990-09-04 FI FI904363A patent/FI904363A0/fi not_active IP Right Cessation
- 1990-09-05 ES ES199090117091T patent/ES2036386T3/es not_active Expired - Lifetime
- 1990-09-05 AT AT90117091T patent/ATE83768T1/de not_active IP Right Cessation
- 1990-09-05 DE DE9090117091T patent/DE59000657D1/de not_active Expired - Fee Related
- 1990-09-05 DK DK90117091.0T patent/DK0416583T3/da not_active Application Discontinuation
- 1990-09-05 EP EP90117091A patent/EP0416583B1/de not_active Expired - Lifetime
- 1990-09-06 NO NO903888A patent/NO173731C/no unknown
- 1990-09-06 HU HU905808A patent/HU205065B/hu not_active IP Right Cessation
- 1990-09-07 DD DD90343872A patent/DD295340A5/de not_active IP Right Cessation
- 1990-09-07 CZ CS904362A patent/CZ278017B6/cs unknown
Also Published As
Publication number | Publication date |
---|---|
CZ278017B6 (en) | 1993-07-14 |
NO903888L (no) | 1991-03-08 |
DK0416583T3 (da) | 1993-02-01 |
NO173731B (no) | 1993-10-18 |
JPH03106853A (ja) | 1991-05-07 |
IL95571A0 (en) | 1991-06-30 |
NO903888D0 (no) | 1990-09-06 |
DD295340A5 (de) | 1991-10-31 |
IE64605B1 (en) | 1995-08-23 |
IL95571A (en) | 1995-05-26 |
EP0416583A1 (de) | 1991-03-13 |
CA2023744A1 (en) | 1991-03-08 |
HU905808D0 (en) | 1991-03-28 |
EP0416583B1 (de) | 1992-12-23 |
HUT54971A (en) | 1991-04-29 |
DE59000657D1 (de) | 1993-02-04 |
FI904363A0 (fi) | 1990-09-04 |
HU205065B (en) | 1992-03-30 |
CZ436290A3 (en) | 1993-01-13 |
ES2036386T3 (es) | 1993-05-16 |
NO173731C (no) | 1994-01-26 |
IE903111A1 (en) | 1991-03-13 |
ATE83768T1 (de) | 1993-01-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
A201 | Request for examination | ||
E902 | Notification of reason for refusal | ||
E601 | Decision to refuse application |