KR900018345A - 개선된, 분지된 아미도-아민 분산제 첨가제 - Google Patents
개선된, 분지된 아미도-아민 분산제 첨가제 Download PDFInfo
- Publication number
- KR900018345A KR900018345A KR1019900007836A KR900007836A KR900018345A KR 900018345 A KR900018345 A KR 900018345A KR 1019900007836 A KR1019900007836 A KR 1019900007836A KR 900007836 A KR900007836 A KR 900007836A KR 900018345 A KR900018345 A KR 900018345A
- Authority
- KR
- South Korea
- Prior art keywords
- nitrogen
- dispersant additive
- adduct
- group
- containing compound
- Prior art date
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- 239000002270 dispersing agent Substances 0.000 title claims 32
- 239000000654 additive Substances 0.000 title claims 30
- 230000000996 additive effect Effects 0.000 claims 28
- -1 nitrogen-containing compound Chemical class 0.000 claims 22
- 238000000034 method Methods 0.000 claims 21
- 150000001875 compounds Chemical class 0.000 claims 15
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims 15
- 239000000376 reactant Substances 0.000 claims 15
- 239000002253 acid Substances 0.000 claims 14
- 229920000098 polyolefin Polymers 0.000 claims 14
- 239000000463 material Substances 0.000 claims 12
- 125000001183 hydrocarbyl group Chemical group 0.000 claims 11
- 239000011541 reaction mixture Substances 0.000 claims 10
- 229920000768 polyamine Polymers 0.000 claims 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 8
- 125000000524 functional group Chemical group 0.000 claims 8
- 125000004433 nitrogen atom Chemical group N* 0.000 claims 8
- 239000007788 liquid Substances 0.000 claims 7
- 239000000047 product Substances 0.000 claims 7
- 239000000203 mixture Substances 0.000 claims 6
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims 5
- 125000004432 carbon atom Chemical group C* 0.000 claims 5
- 125000002924 primary amino group Chemical class [H]N([H])* 0.000 claims 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 4
- SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical compound CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 claims 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 4
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims 4
- 229920002367 Polyisobutene Polymers 0.000 claims 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 4
- 150000004820 halides Chemical class 0.000 claims 4
- 150000002430 hydrocarbons Chemical group 0.000 claims 4
- 229910052739 hydrogen Inorganic materials 0.000 claims 4
- 239000001257 hydrogen Substances 0.000 claims 4
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 claims 4
- 229910052757 nitrogen Inorganic materials 0.000 claims 4
- 229910052760 oxygen Inorganic materials 0.000 claims 4
- 239000001301 oxygen Substances 0.000 claims 4
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 claims 4
- 229910052717 sulfur Inorganic materials 0.000 claims 4
- 239000011593 sulfur Substances 0.000 claims 4
- 125000002947 alkylene group Chemical group 0.000 claims 3
- 150000001991 dicarboxylic acids Chemical group 0.000 claims 3
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 2
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims 2
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims 2
- OFHCOWSQAMBJIW-AVJTYSNKSA-N alfacalcidol Chemical compound C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C\C=C1\C[C@@H](O)C[C@H](O)C1=C OFHCOWSQAMBJIW-AVJTYSNKSA-N 0.000 claims 2
- 125000003368 amide group Chemical group 0.000 claims 2
- 229910021529 ammonia Inorganic materials 0.000 claims 2
- 229910052796 boron Inorganic materials 0.000 claims 2
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims 2
- 229920001577 copolymer Polymers 0.000 claims 2
- 125000004185 ester group Chemical group 0.000 claims 2
- 229930195733 hydrocarbon Natural products 0.000 claims 2
- 125000000743 hydrocarbylene group Chemical group 0.000 claims 2
- 239000010687 lubricating oil Substances 0.000 claims 2
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims 2
- 150000005673 monoalkenes Chemical class 0.000 claims 2
- 150000002825 nitriles Chemical class 0.000 claims 2
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims 2
- 150000002989 phenols Chemical class 0.000 claims 2
- NHARPDSAXCBDDR-UHFFFAOYSA-N propyl 2-methylprop-2-enoate Chemical compound CCCOC(=O)C(C)=C NHARPDSAXCBDDR-UHFFFAOYSA-N 0.000 claims 2
- PNXMTCDJUBJHQJ-UHFFFAOYSA-N propyl prop-2-enoate Chemical compound CCCOC(=O)C=C PNXMTCDJUBJHQJ-UHFFFAOYSA-N 0.000 claims 2
- FALRKNHUBBKYCC-UHFFFAOYSA-N 2-(chloromethyl)pyridine-3-carbonitrile Chemical compound ClCC1=NC=CC=C1C#N FALRKNHUBBKYCC-UHFFFAOYSA-N 0.000 claims 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims 1
- 229930091371 Fructose Natural products 0.000 claims 1
- 239000005715 Fructose Substances 0.000 claims 1
- ZDPOKDGDXOHRPQ-UHFFFAOYSA-N N=P1C=CC=C1 Chemical compound N=P1C=CC=C1 ZDPOKDGDXOHRPQ-UHFFFAOYSA-N 0.000 claims 1
- 150000001299 aldehydes Chemical class 0.000 claims 1
- 125000003277 amino group Chemical group 0.000 claims 1
- 150000008064 anhydrides Chemical class 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 125000004093 cyano group Chemical group *C#N 0.000 claims 1
- SUPCQIBBMFXVTL-UHFFFAOYSA-N ethyl 2-methylprop-2-enoate Chemical compound CCOC(=O)C(C)=C SUPCQIBBMFXVTL-UHFFFAOYSA-N 0.000 claims 1
- 239000000295 fuel oil Substances 0.000 claims 1
- 239000000314 lubricant Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 125000000896 monocarboxylic acid group Chemical group 0.000 claims 1
- 150000002763 monocarboxylic acids Chemical group 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 210000000056 organ Anatomy 0.000 claims 1
- 229920001281 polyalkylene Polymers 0.000 claims 1
- RINCXYDBBGOEEQ-UHFFFAOYSA-N succinic anhydride Chemical group O=C1CCC(=O)O1 RINCXYDBBGOEEQ-UHFFFAOYSA-N 0.000 claims 1
- 229940014800 succinic anhydride Drugs 0.000 claims 1
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- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
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Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (42)
- 하기 (a), (b) 및 (c) 단계에 의해 제조된 개선된 윤활유 질소 함유 분산제 첨가제; (a) 제1액체 반응혼합물중에서 적어도 두개의 반응성 질소 잔기를 갖는 제1질소 함유 화합물과 구조내에 -NH- 그룹과 반응하는 제1작용 그룹 및 -NH- 그룹과 반응하는 적어도 하나의 추가의 작용그룹을 갖는 다작용성 반응물을, 상기 다작용성 반응물의 상기 제1작용그룹 적어도 일부가 상기 반응성 질소 잔기와 선택적으로 반응하기에 충분한 양으로 및 그러한 조건하에 접촉하에 접촉시켜 제1부가물을 제조하는 단계; (b) 상기 제1부가물과 적어도 두개의 -NH- 그룹을 갖는 제2질함유 화합물을, 상기 제1부가물의 상기 추가의 작용그룹이 제2질소함유 화합물의 상기 -NH-그룹과 반응하기에 충분한 양으로 및 그러한 조건하에 접촉시켜 구조내에 평균적으로 (ⅰ) 상기 제1질소함유 화합물로부터 유도된 질소 함유 잔기당 상기 제2질소함유 화합물로부터 유도된 적어도 두개의 질소함유 잔기 및 (ⅱ) 분자당 적어도 두개의 미반응 1급 또는 2급 아민 그룹을 가짐을 특징으로 하는 제2부가물을 제조하는 단계; 및 (c) (ⅰ) 모노 또는 디카복실산, 또는 에스테르 그룹으로 치환된 장쇄 탄화수소; (ⅱ) 할로겐화 장쇄 탄화수소, (ⅲ) 알데히드와 장쇄 하이드로카빌 치환된 페놀의 혼합물; 및 (ⅳ) 모노 또는 디카복실산, 무수물 또는 에스테르 그룹으로 치환된 장쇄 탄화수소와 아미노 치환되고, 임의로 하이드로카빌 치환된 페놀의 반응에 의해 형성된 반응 생성물과 알테하이드로의 혼합물로 이루어진 그룹으로 부터 선택된 적어도 하나의 일원을 제2액체 반응 혼합물중에서 상기 제2부가물과 접촉시키는 단계
- 제1항에 있어서, 상기 장쇄 하이드로카빌 반응물이 수평균 분자량 약 300 내지 10,000을 갖는 C2내지 C10모노 올레핀이 올레핀 중합체를 C4내지 C10모노불포화 디카복실산 물질 및 C3내지 C10모노불포화 모노 카복실산 물질중 적어도 하나와 반응시켜 제조한 장쇄 하이드로카빌 치환된 모노-또는 디카복실산 생성물질(상기 산 생성 물질은 이를 제조하는데 사용된, 반응 혼합물중에 존재하는 상기 올레핀 중합체 분자당 평균 적어도 약 0.5개의 디카복실산 생성 잔기를 갖는다)적어도 하나를 포함하는 분산제 첨가제.
- 제1항에 있어서, 상기 다작용성 반응물이 하기 일반식(ⅰ) 내지 (ⅱ)의 화합물중 적어도 하나를 포함하는 분산제 첨가제;상기식들에서, W1및 W2는 같거나 다르며, 산소 또는 황이고, X및 Y는 같거나 다르며, 할라이드, -OR4, -SR4, -N(R4)(R5), -Z1C(O)OR4, -C(O)R4, -(R3)C=C(R1)(R2), -Z1니트릴, -Z1-시아노, -Z1-티오시아노, -Z1-이소티오 시아노 및 Z1-이소시아노(여기에서 R1, R2, R3, R4및 R5는 같거나 다르며, 수소 또는 치환되거나 비치환된 하이드로카빌이며, Z1은 C1내지 C20의 이가 하이드로카빌렌이다)로 이루어진 그룹중에서 선택된 일원을 포함하고, T는 치환되거나 비치환된 탄화수소 잔기이며, a는 0또는 1이고, b는 0또는 1이며, c는 적어도 1인 정수이고, a가 1이고 T가 >C=C<그룹을 함유하는 경우, X및 Y는 함께 -0- 또는 -S-를 포함하고, X, Y 및 T중 적어도 두개는 -NH- 그룹과 반응하는 그룹이고, 단 a가 0인 경우 c는 1이고, a가 1인 경우 b는 1이고, d1 및 d2는 각각 1 내지 10의 정수이고, Y"은 할라이드, -OR4, -SR4, -N(R4)(R5), -Z1C(O)OR4, 및 (-R3)C=C(R1)(R2), 로 이루어진 그룹중에서 선택된 반응성 작용성 그룹을 포함한다.
- 제1항에 있어서, 상기 다작용성 반응물이 하이 일반식의 알파, 베타-불포화 화합물 적어도 하나를 포함하는 분산제 첨가제.상기식에서 , X는 황 또는 산소이고, Y는 -OR4, SR4또는 -NR4(R5)이고, R1, R2, R3, R4및 R5는 같거나 다르며, 수소 또는 치환되거나 비치환된 하이드로카빌이다.
- 제1항에 있어서, 상기 제2질소함유 화합물이 분자당 탄소원자 2내지 60개와 질소원자 2내지 12개를 함유하는 폴리아민을 적어도 하나 포함하는 분산제 첨가제.
- 제5항에 있어서, 상기 폴리아민이 폴리알킬렌폴리아민을 포함하고 각각의 상기 알킬렌 그룹이 탄소원자 2내지 6개를 함유하고 상기 폴리알킬렌폴리아민이 분자당 질소원 6내지 약 9개를 함유하는 분산제 첨가제.
- 제2항에 있어서, 상기 하이드로카빌 치환된 모노불포화 산 생성 물질이 숙신산 무수물 잔기로 치환된, 수평균 분자량 약 700내지 5000의 폴리이소부틸렌을 함유하는 하이드로카빌 치환된 C4내지 C10모노 불포화 디카복실산 생성물을 포함하고; 상기 제1질소함유 화합물이 암모니아를 포함하고 상기 제2질소함유 화합물이 폴리알킬렌폴리아민 (여기에서, 각각의 상기 알킬렌 그룹은 탄소원자 2내지 6개를 함유하고, 상기 폴리알킬렌폴리아민은 분자당 질소원자 5내지 9개를 함유한다)을 포함하고; 상기 알파, 베타-불포화 화합물이 메틸 아크릴레이트, 에틸 아클릴레이트, 프로필 아크릴레이트, 부틸 아크릴레이트, 메틸 메타크릴레이트, 에틸 메타크릴레이트, 프로필 메타크릴레이트 및 부틸 메타크릴레이트로 구성된 그룹중에서 선택된 일원을 적어도 하나 포함하는 분산제 첨가제.
- 제1항에 상기 제2질소함유 화합물이 폴리에틸렌폴리아민 또는 폴리프로필렌폴리아민을 포함하는 분산제 첨가제.
- 제5항에 있어서, 각각의 분산제 첨가제가 붕산화 분산제 붕산화 분산제 첨가중의 붕소함량을 약 0.05 내지 2.0중량%로 제공하도록 붕산화된 분산제 첨가제.
- 제1항에 있어서, 상기 올레핀 중합체가 폴리이소부틸렌을 포함하는 분산제 첨가제.
- 제2항에 있어서, 상기 분산제 첨가제중의 올레핀 중합체 분자당 산생성 잔기의 비율이 약 0.9 내지 1.3인 분산제 첨가제.
- 제11항에 있어서, 상기 올레핀 중합체의 상기 수평균 분자량이 약 1,300내지 3,000인 분산제 첨가제.
- 제2항에 있어서, 상기 모노불포화 산 물질이 말레산 무수물을 포함하는 분산제 첨가제.
- 제2항에 있어서, 상기 제2부가물의 일급 질소 당량당 상기 산 생성 물질 약 1내지 5몰이 상기 (c) 단계의 액체 반응 혼합물에 존재하는 분산제 첨가제.
- 제5항에 있어서, 상기 제2질소함유 화합물이 분자당 평균적으로 적어도 2개의 일급 질소원자를 함유하는 폴리아민을 포함하고, 상기 다작용성 반응물이 적어도 하나의 알파, 베타-불포화 화합물을 포함하고; 상기 제1질소함유 화합물과 상기 알파, 베타-불포화 화합물을 상기 제1질소함유 화합물중의 상기 반응성 잘소 잔기 당량당 상기 알파, 베타-불포화 화합물 약 1. 1 내지 3몰의 양으로 접촉시키는 분산제 첨가제.
- 제15항에 있어서, 상기 제1부가물이 평균 3내지 18의 분지도를 특징으로 하는 분산제 첨가제.
- 제16항에 있어서, 상기 제2질소함유 반응물이 분자당 평균적으로 적어도 2개의 일급 질소원자를 함유하는 폴리아민을 포함하고; 상기 제2부가물이 분자당 평균적으로 2내지 4개의 미반응 일급 아민과 0내지 8개의 미반응 2급 아민을 그룹을 함유하는 분산제 첨가제.
- 제17항에 있어서, 상기 아미도-아민이 상기 아미도-아민 분자당 평균적으로 1내지 3개의 아미도 그룹을 함유하는 분산제 첨가제.
- (a) (ⅰ) 제1반응은 혼합물중에서 적어도 두개의 반응성 질소 잔기를 갖는 제1질소함유 화합물과 구조내에 -NH-그룹과 반응하는 제1작용그룹 및 -NH- 그룹과 반응하는 적어도 하나의 추가의 작용그룹을 갖는 다작용성 반응물을, 상기 다작용성 반응물의 상기 제1작용그룹이 상기 반응성 질소 잔기와 선택적으로 반응하기에 충분한 양으로 및 그러한 조건하에 접촉시켜 제1부가물을 제조하고; (ⅱ) 제2액체 반응 혼합물중에서 상기 제1부가물과 적어도 두개의 -NH- 그룹을 갖는 제2질소함유 화합물을, 상기 제1부가물의 상기 추가의 작용그룹이 상기 제2질소함유 화합물의 상기 -NH- 그룹과 반응하기에 충분한 양으로 및 그러한 조건하에 접촉시킴을 포함하는 방법에의해 구조내에 분자당 평균적으로 적어도 두개의 미반응 일급 또는 2급 아민 그룹을 가짐을 특징으로 하고, 구조내에 평균적으로 상기 제1질소함유 화합물로부터 유도된 질소함유 잔기당 상기 제2질소함유 화합물로부터 유도된 적어도 두개의 질소함유 잔기를 가짐을 또한 특징으로 하는 질소를 함유한 분지된 제2부가물을 제공하고; (b) 수평균 분자량 약 300내지 10,000을 갖는 C2내지 C10모노올레핀의 올레핀 중합체를 C4내지 C10모노불포화 디카복실산 물질 및 C3내지 C10모노불포화 모노카복실산 물질중 적어도 하나와 반응시켜 제조한 장쇄 하이드로카빌 치환된 모노-또는 디카복실산 생성물질(상기 산생성물질은 이를 제조하는데 사용된, 반응 혼합물중네 존재하는 이를 제조하는데 사용된, 반응 혼합물중에서 존재하는 상기 올레핀 중합체 분자당 평균 적어도 약 0.5개의 디카복실산생성 잔기를 갖는다)을 제공하고; (c) 상기 산 생성물질과 상기 분지된 질소함유 제2부가물을 상기 분지된 질소함유 부가물상의 일급 아민 그룹의 적어도 일부가 상기 산 생성물질중의 산 생성 그룹 적어도 일부와 반응하기에 충분한 양으로 및 그러한 조건하에 접촉시켜 분산제 첨가제를 제조함을 포함하는 오일 첨가제로 유용한 분산제 첨가제의 제조방법.
- 제19항에 있어서, 상기 올레핀 중합체가 수평균 분자량 약 700내지 5,000을 갖는 폴리이소부틸렌을 포함하고; 상기 모노불포화 산 물질이 말레산 무수물을 포함하고; 상기 산 생성물질이 이를 제조하는 데 사용된 반응 혼합물중에 존재하는 상기 올레핀 중합체 분자당 숙신산 무수물 생성 장기를 평균적으로 적어도 약 0.8개 갖는 방법.
- 제19항에 있어서, 상기 다작용성 반응물이 하기 일반식(ⅰ) 내지 (ⅳ)의 화합물중 적어도 하나를 포함하는 방법.상기식들에서, W1및 W2는 같거난 다르며, 산소 또는 황이고, X 및 Y는 같거나 다르며, 할라이드, -OR4, -SR4, -N(R4)(R5), -Z1C(O)OR4-C(O)R4, -(R3)C=C(R1)(R2), -Z1니트릴, -Z1-시아노, -Z1-티오시아노, -Z1-이소티오시아노 및 Z1-이소시아노(여기에서 R1, R2, R3, R4및 R5는 같거나 다르며, 수소 또는 치환되거나 비치환된 하이드로카빌이고, Z1은 C1내지 C20의 이가 하이드로카빌렌이다)로 이루어진 그룹중에서 선택된 일원을 포함하고, T는 치환되거나 비치환된 탄화수소 잔기이고, a는 0또는 1이며, b는 0또는 1이고, c는 적어도 1인 정수이고, a가 1이고, T가 ＞C=C＜ 그룹을 함유하는 경우, X 및 Y는 함께 -0- 또는 -S-를 포함하고, X, Y 및 T중 적어도 둘은 -NH- 그룹과 반응하는 그룹이고, 단 a가 0인 경우 c는 1이고, a가 1인 경우 b는 1이고, d1및 d2는 각각 1내지 10의 정수이고, Y"은 할라이드, -OR4, -SR4, -N(R4)(R5), -Z1C(O)OR4, 및 -(R3)C=C(R1)(R2), 로 이루어진 그룹중에서 선택된 반응성 작용성 그룹을 포함한다.
- 제20항에 있어서, 상기 다작용성 반응물이 하기 일반식 알파, 베타-불포화 화합물 적어도 하나를 포함하는 방법.상기식에서, X는 황 또는 산소이고, Y는 -OR4, -SR4또는 -NR4(R5)이고, R1, R2, R3, R4및 R5는 같거나 다르며, 수소 또는 치환되거나 비치환된 하이드로카빌이다.
- 제22항에 있어서, 상기 제2질소함유 화합물이 분자당 탄소원자 2내지 60개와 질소원자 2내지 12개를 함유하는 폴리아민을 적어도 하나 포함하는 방법.
- 제23항에 있어서, 상기 폴리아민이 폴리알킬렌폴리아민을 포함하고, 각각의 상기 알킬렌 그룹이 탄소원자 2내지 6개를 함유하고, 사기 폴리알킬렌폭리아민이 분자당 질소원자 5내지 약9 개를 함유하는 방법.
- 제24항에 있어서, 상기 제1질소함유 화합물이 암모니아를 포함하고, 상기 알파, 베타-불포화 화합물이 메틸 아크릴레이트, 에틸 아크릴레이트, 프로필 아크릴레이트, 부틸 아크릴레이트, 메틸 메타크릴레이트, 에틸메탈크릴레이트, 프로필 메타크릴레이트 및 부틸 메타클릴레이트로 구성된 그룹중에서 선택된 일원을 적어도 하나 포함하는 방법.
- 제25항에 있어서, 상기 제2질소함유 화합물이 폴리에틸렌폴리아민 또는 폴리프로필렌폴리아민을 포함하는 방법.
- 제26항에 있어서, 상기 올레핀 중합체가 폴리이소부틸렌을 포함하는 방법.
- 제27항에 있어서, 각각의 분산제 첨가제가 붕산화 분산제 첨가제중의 붕소 함량을 약 0.05내지 2.0중량%로 제공하도록 붕산화된 방법.
- 제27항에 있어서, 상기 분산제 첨가제중의 올레핀 중합체 분자당 산 생성 잔기의 비율이 약 0.8내지 1.3인 방법.
- 제29항에 있어서, 상기 올레핀 중합체의 상기 수 평균 분자량이 약 1,300 내지 3,000이고 상기 제2액체 반응 혼합물이 상기 다작용성 반응물을 거의 함유하지 않는 방법.
- 제19항에 있어서, 상기 제1부가물과 상기 폴리아민을 접촉시키기 전에 상기 제1액체 반응 혼합물에 대해 미반응 다작용성 반응물의 제거 처리를 수행하는 방법.
- 제19항에 있어서, 상기 제2부가물의 일급 질소 당량당 상기 산 생성 물질 약 1내지 5몰이 상기 (c) 단계의 액체 반응 혼합물에 존재하는 방법.
- 제20항에 있어서, 상기 제2질소함유 화합물이 분자당 평균적으로 적어도 2개의 일급 질소원자를 함유하는 폴리아민을 포함하고; 상기 다작용성 반응물이 적어도 하나의 알파, 베타-불포화 화합물을 포함하고; 상기 제1질소함유 화합물과 상기 알파, 베타-불포화 화합물을 상기 제1질소함유 화합물중의 상기 반응성 질소 잔기 당량당 상기 알파, 베타-불포화 화합물 약 1.1 내지 3몰의 양으로 접촉시키는 방법.
- 제33항에 있어서, 상기 제1부가물이 평균 3내지 18의 분지도를 특징으로 하는 방법.
- 제34항에 있어서, 상기 제2질소함유 반응물이 분자당 평균적으로 적어도 2개의 일급 질소원자를 함유하는 폴리아민을 포함하고; 상기 제2부가물이 분자당 평균적으로 2내지 4개의 미반응 일급 아민과 0내지 8개의 미반응 2급 아민그룹을 함유하는 방법.
- 제35항에 있어서, 상기 아미도-아민이 상기 아미도-아민 분자당 평균적으로 1내지 3개의 아미도 그룹을 함유하는 방법.
- 제19항에 있어서, 상기 산 생성 물질과 접촉시켜 상기 분산제 물질을 제조하기 전에, (a) 및 (b) 단계를 1회 이상 반복하여 분지도가 증가된 질소함유 부가물을 제공하는 방법.
- 제1항의 분산제 첨가제 약 0.001내지 0.5중량%를 함유하는 연료유 조성물.
- 제1항의 분산제 첨가제 0.1내지 20중량%를 함유하는 윤활유 조성물.
- 제7항의 분산제 첨가제 약 0.1내지 8중량%를 함유하는 윤활유 조성물.
- 제1항에 있어서, 상기 폴리올레핀이 에틸렌-프로필렌 공중합체를 포함하는 분산제 첨가제.
- 제19항에 있어서, 상기 폴리올레핀이 에틸렌-프로필렌 공중합체를 포함하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US35890389A | 1989-05-30 | 1989-05-30 | |
| US358903 | 1989-05-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR900018345A true KR900018345A (ko) | 1990-12-21 |
Family
ID=23411513
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019900007836A KR900018345A (ko) | 1989-05-30 | 1990-05-30 | 개선된, 분지된 아미도-아민 분산제 첨가제 |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0400864A3 (ko) |
| JP (1) | JPH0362891A (ko) |
| KR (1) | KR900018345A (ko) |
| BR (1) | BR9002569A (ko) |
| CA (1) | CA2016022A1 (ko) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0587250B1 (en) * | 1992-09-11 | 1997-05-14 | Shell Internationale Researchmaatschappij B.V. | Gasoline compositions |
| JP2002306365A (ja) * | 2001-04-16 | 2002-10-22 | Worldtop Co Ltd | おしぼり巻き上げ装置 |
| EP1858634A1 (en) * | 2005-02-03 | 2007-11-28 | The Lubrizol Corporation | Dispersants from condensed polyamines |
| JP4757053B2 (ja) * | 2006-02-17 | 2011-08-24 | 株式会社パイロットコーポレーション | クリップを有するノック式筆記具 |
| CN117567912B (zh) * | 2023-11-22 | 2024-05-28 | 江西科技师范大学 | 一种可回收聚丙烯酸酯乳液涂层及其制备方法和应用 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1068133A (en) * | 1965-02-04 | 1967-05-10 | Lubrizol Corp | Nitrogen-containing derivatives of substituted succinic acids |
| US3445441A (en) * | 1965-03-25 | 1969-05-20 | Petrolite Corp | Amino-amido polymers |
| US3718663A (en) * | 1967-11-24 | 1973-02-27 | Standard Oil Co | Preparation of oil-soluble boron derivatives of an alkylene polyamine-urea or thiourea-succinic anhydride addition product |
| ZA771959B (en) * | 1976-04-01 | 1978-03-29 | Orogil | Compositions based on alkenylsuccinimides |
| US4855116A (en) * | 1985-04-03 | 1989-08-08 | Bergwerksverband Gmbh | Activated coke method of removing nitrogen oxides from exhaust gases |
| US4857217A (en) * | 1987-11-30 | 1989-08-15 | Exxon Chemical Patents Inc. | Dispersant additives derived from amido-amines |
-
1990
- 1990-05-03 CA CA002016022A patent/CA2016022A1/en not_active Abandoned
- 1990-05-22 EP EP19900305560 patent/EP0400864A3/en not_active Withdrawn
- 1990-05-29 JP JP2137310A patent/JPH0362891A/ja active Pending
- 1990-05-30 KR KR1019900007836A patent/KR900018345A/ko not_active Application Discontinuation
- 1990-05-30 BR BR909002569A patent/BR9002569A/pt not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| EP0400864A3 (en) | 1991-08-14 |
| JPH0362891A (ja) | 1991-03-18 |
| BR9002569A (pt) | 1991-08-20 |
| EP0400864A2 (en) | 1990-12-05 |
| CA2016022A1 (en) | 1990-11-30 |
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