KR890701657A - 강성 폴리방향족 전구체 물질로부터 제조된 폴리이소시아네이트 예비중합체 및 이로부터 제조된 폴리우레탄 - Google Patents

강성 폴리방향족 전구체 물질로부터 제조된 폴리이소시아네이트 예비중합체 및 이로부터 제조된 폴리우레탄

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Publication number
KR890701657A
KR890701657A KR1019890700456A KR890700456A KR890701657A KR 890701657 A KR890701657 A KR 890701657A KR 1019890700456 A KR1019890700456 A KR 1019890700456A KR 890700456 A KR890700456 A KR 890700456A KR 890701657 A KR890701657 A KR 890701657A
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group
active hydrogen
polyaromatic
polyisocyanate
bond
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KR1019890700456A
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English (en)
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피. 토마스 옴만
이. 버트 3세 얼
디. 페플리 리챠드
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리챠드 지. 워터맨
더 다우 케미칼 캄파니
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Publication of KR890701657A publication Critical patent/KR890701657A/ko

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/81—Unsaturated isocyanates or isothiocyanates
    • C08G18/8141—Unsaturated isocyanates or isothiocyanates masked
    • C08G18/815—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen
    • C08G18/8191—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen with acetylenic compounds having active hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/487—Polyethers containing cyclic groups
    • C08G18/4879—Polyethers containing cyclic groups containing aromatic groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/80—Masked polyisocyanates
    • C08G18/8003—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen
    • C08G18/8006—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32
    • C08G18/8009—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203
    • C08G18/8012—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203 with diols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/80—Masked polyisocyanates
    • C08G18/8003—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen
    • C08G18/8006—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32
    • C08G18/8038—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3225
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/80—Masked polyisocyanates
    • C08G18/8003—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen
    • C08G18/8054—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/38
    • C08G18/8058—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/38 with compounds of C08G18/3819
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/81—Unsaturated isocyanates or isothiocyanates
    • C08G18/8141—Unsaturated isocyanates or isothiocyanates masked
    • C08G18/815—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyurethanes Or Polyureas (AREA)

Abstract

내용 없음

Description

강성 폴리방향족 전구체 물질로부터 제조된 폴리이소시아네이트 예비중합체 및 이로부터 제조된 폴리우레탄
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (13)

  1. 화학양론적 과량의 폴리이소시아네이트와 내부 강성 폴리방향족 그룹을 함유하는 폴리방향족 활성 수소-함유 화합물과의 반응 생성물을 포함하는, 유리 이소시아네이트 그룹을 함유하는 액체 예비중합체 조성물.
  2. 제1항에 있어서, 폴리방향족 활성 수소-함유 화합물이 일반식(Ⅰ)로 표시되는 예비중합체 조성물.
    상기식에서 D는 각각 독립적으로 -A- 결합에 대해 오르토 위치인 경우, -A- 결합 및 방향족 환과 사이클릭 구조를 형성할 수 있는 불활성 치환체 그룹이고; b는 1 내지 10의 수이며; Z는 각각 독립적으로 활성 수소-함유 그룹이고; R은 각각 독립적으로 폴리이소시아네이트와 이소시아네이트-반응성 폴리페닐렌 화합물과의 반응에 대해 불활성인 2가 라디칼이며, A는 공유결합, 치환족 디라디칼, -CH2CH2- 또는 강성 결합그룹이거나, -A-결합에 대해 오르토 위치인 그룹 D 및 방향족 환과 함께 사이클릭 구조를 형성한다.
  3. 제2항에 있어서, 예비중합체 조성물을 제조하기 위해 폴리이소시아네이트 100중량부당 폴리방향족 활성 수소-함유 화합물 1 내지 50중량부를 사용하는 예비중합체 조성물.
  4. 제3항에 있어서, 폴리이소시아네이트가 방향족 폴리이소시아네이트 또는 지방족 폴리이소시아네이트인 예비중합체 조성물.
  5. 제4항에 있어서, D가 각각 수소, 저급 알킬 또는 할로겐이고, b가 1 내지 2의 수이며, Z가 각각 하이드록실, 1급 아민 또는 2급 아민 그룹이고, R이 각각 옥시알킬렌 또는 폴리옥시알킬렌 디라디칼인 예비중합체 조성물.
  6. 제5항에 있어서, 그룹 D는 폴리방향족 활성 수소-함유 화합물이 대칭이 되도록 선택되고, R은 각각 1 내지 4개의 옥시에틸렌 또는 옥시프로필렌 반복 단위를 함유하는 옥시알킬렌 또는 폴리옥시알킬렌 그룹인 예비중합체 조성물.
  7. 제6항에 있어서, 폴리이소시아네이트가 (1) 2,4- 및/또는 2,6-톨루엔 디이소시아네이트; 또는 (2) 2,4'- 및/또는 4,4'-디페닐메탄디이소시아네이트, 또는 이의 유도체를 포함하는 예비중합체 조성물.
  8. 화학양론적 과량의 폴리이소시아네이트와 내부강성 폴리방향족 그룹을 함유하는 폴리방향족 활성 수소-함유 화합물과의 반응 생성물을 포함하는 유리 이소시아네이트 그룹을 함유하는 액체 예비중합체 조성물과 활성 수소-함유 조성물과의 반응에 의해 제조된 폴리우레탄 및/또는 폴리우레아 중합체.
  9. 제8항에 있어서, 폴리방향족 활성 수소-함유 화합물이 일반식(Ⅰ)로 표시되는 폴리우레탄 및/또는 폴리우레아 중합체.
    상기식에서, D는 독립적으로 -A-결합에 대해 오르토 위치인 경우, -A-결합 및 방향족 환과 사이클릭 구조를 형성할 수 있는 불활성 치환제 그룹이고; b는 1 내지 10의 수이며; Z는 각각 독립적으로 활성 수소-함유 그룹이고; R은 각각 독립적으로 폴리이소시아네이트와 이소시아네이트-반응성 폴리페닐렌 화합물과의 반응에 대해 불활성인 2가 라디칼이며; A는 공유결합, 치환족 디라디칼, -CH2CH2- 또는 강성 결합그룹이거나, 방향족 환 및 -A-결합에 대해 오르토 위치인 그룹 D와 사이클릭 구조를 형성한다.
  10. 제9항에 있어서, 활성 수소-함유 조성물이 (1)하이드록실 또는 1급 또는 2급 아민-차단된 폴리에테르 및 방향족 폴리이소시아네이트; 또는 (2) 비교적 고당량의 활성 수소-함유 화합물 및 발포제를 포함하는 폴리우레탄 및/또는 폴리우레아 중합체.
  11. 제8항 내지 제10항중의 어느 한 항에 있어서, 연질 발포체 또는 경질 발포체인 폴리우레탄 및/또는 폴리우레아 중합체.
  12. 화학양론적 과량의 폴리이소시아네이트와 내부 강성 폴리방향족 그룹을 함유하는 폴리방향족 활성 수소-함유 화합물과의 반응을 포함하여, 유리 이소시아네이트 그룹을 함유하는 액체 예비중합제 조성물을 제조하는 방법.
  13. 화학양론적 과량의 폴리이소시아네이트와 내부 강성 폴리방향족 그룹을 함유하는 폴리방향족 활성 수소-함유 화합물과의 반응 생성물을 포함하는 유리 이소시아네이트 그룹을 함유하는 액체 예비중합체 조성물과 활성 수소-함유 조성물과의 반응을 포함하여, 폴리우레탄 및/또는 폴리우레아 중합체를 제조하는 방법.
    ※ 참고사항: 최초출원 내용에 의하여 공개하는 것임.
KR1019890700456A 1987-07-14 1988-07-07 강성 폴리방향족 전구체 물질로부터 제조된 폴리이소시아네이트 예비중합체 및 이로부터 제조된 폴리우레탄 KR890701657A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US7304687A 1987-07-14 1987-07-14
US073,046 1987-07-14
PCT/US1988/002291 WO1989000588A1 (en) 1987-07-14 1988-07-07 Polyisocyanate prepolymers prepared from rigid polyaromatic precursor materials, and polyurethanes prepared therefrom

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KR890701657A true KR890701657A (ko) 1989-12-21

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EP (2) EP0365599A4 (ko)
JP (1) JPH02502384A (ko)
KR (1) KR890701657A (ko)
AU (1) AU606737B2 (ko)
BR (1) BR8807617A (ko)
WO (1) WO1989000588A1 (ko)

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AU2139088A (en) 1989-02-13
BR8807617A (pt) 1990-06-12
EP0365599A4 (en) 1990-09-12
EP0299462A2 (en) 1989-01-18
EP0299462A3 (en) 1989-01-25
EP0365599A1 (en) 1990-05-02
AU606737B2 (en) 1991-02-14
JPH02502384A (ja) 1990-08-02

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