KR870001488B1 - Method for producing vitamine containing products - Google Patents

Method for producing vitamine containing products Download PDF

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Publication number
KR870001488B1
KR870001488B1 KR1019850002362A KR850002362A KR870001488B1 KR 870001488 B1 KR870001488 B1 KR 870001488B1 KR 1019850002362 A KR1019850002362 A KR 1019850002362A KR 850002362 A KR850002362 A KR 850002362A KR 870001488 B1 KR870001488 B1 KR 870001488B1
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South Korea
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liver
suspension
liver oil
oil
vitamin
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KR1019850002362A
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Korean (ko)
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KR860007890A (en
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모리미츠 미야기
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백인천
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L17/00Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof

Abstract

Inodorous cod-liver oil havings high content of vitamines is prepd. from sea animal's liver. Thus, the liver obtd. from sharks is crushed with a mixer. The suspension is freezed at -25 C, stored for 10days, and thawed naturally. The viscous solids floated on the surface of aq. matter and the moisture and impurities of lower layer are removed at room temp. The obtd. oily matter is treated with mirabilite and filtered in vacuo to give a purified cod-liver oil contg. 26500IU/100g of vit A and 41.6mg/ 100g of vit E.

Description

고도로 탈취한 고단위 비타민유의 제조법Preparation of Highly Deodorized High-Unit Vitamin Oil

본 발명은 상어, 대구, 고래등의 해양동물의 간장에서, 열을 가하지 않고 간유를 채취하는 방법에 관한 것으로, 어취 및 불쾌취가 없고, 맛이 양호하고, 고단위 비타민을 함유하는 간유를 제공하는데 있다.The present invention relates to a method for extracting liver oil from the liver of marine animals such as sharks, cod, whales, etc. without applying heat, and to provide liver oils without odor and unpleasant taste, good taste, and containing high unit vitamins. have.

종래, 해향동물의 간장으로부터 간유를 채취하는 방법은 다수 제안되어 왔다. 그중. 가열처리법, 진공증류와 분별 증류의 조합이나 알카리소화법이 현재 실시되고 있다. 그 어느 방법도 기온을 필요로 하고 적어도 50℃이상으로 가열하여야 한다.Conventionally, a number of methods for collecting liver oil from the liver of marine animals have been proposed. among them. A heat treatment method, a combination of vacuum distillation and fractional distillation, and an alkaline digestion method are currently carried out. Neither method requires a temperature and must be heated to at least 50 ° C.

그러나, 비타민유는 열에 약하며, 지극히 불안정하기 때문에, 50°-60℃정도의 가온으로도 대부분의 비타민유는 파괴돈다. 그 뿐만 아니라, 간유의 어취 및 불괘취의 제거, 맛의 향상이 극히 곤란하고, 만족할 수 있는 처리법은 알려져 있지 않아, 이런 점을 해결할 수 있는 방법이 요망되고 있었다.However, since vitamin oil is weak to heat and extremely unstable, most vitamin oils are destroyed even when heated to about 50 ° -60 ° C. Not only that, but it is extremely difficult to remove the odor, unpleasant odor and taste of the liver oil, and a satisfactory treatment method is not known, and a method for solving this problem has been desired.

본 발명자는 열을 가하지 않고 간유를 채취하는 방법에 관하여 예의 연구를 거듭한 결과, 해양동물의 간장을 분쇄하여 현탁액으로 하고, 그 현탁액을 냉동시키고 잠시동안 정치후, 자연 해동시켜, 생성된 액상물의 표면층에 있는 점성의 고형물등을 제거하고, 다음에 저부층에 있는 수분이나 불순물등을 분리하고얻어진 유상물에 일반법의 탈수처리를 행하여 고도로 탈취한 불쾌취가 없고, 맛좋은 고단위의 비타민을 함유하는 간유를 얻을 수 있는 사실을 발견하여 본 발명을 완성하였다.As a result of intensive research on a method of collecting cod liver oil without applying heat, the present inventors have pulverized soy sauce of marine animals to make a suspension, freezing the suspension and allowing it to stand for a while, and then thaw it naturally. Viscous solids in the surface layer are removed, water and impurities in the bottom layer are separated, and the obtained oils are subjected to dehydration by a general method, and there is no highly deodorizing odor and contains a delicious high unit vitamin. The present invention has been completed by finding the fact that liver oil can be obtained.

본 발명 방법에서는 열을 가하지 않고 있기 때문에, 비타민유의 파괴는 실질적으로 방지되고, 고단위의 비타민을 함유하는 간유가 얻어진다. 예를들어, 비타민 A에 대해서는 26,500 IU/100g, 비타민 B에 대해서는 41.6ml/100g이라는 고단위의 비타민이 함유된 간유가 본 발명에 의해 얻어진다.Since no heat is applied in the method of the present invention, destruction of the vitamin oil is substantially prevented, and liver oil containing a high unit of vitamin is obtained. For example, a liver oil containing a high unit of vitamins of 26,500 IU / 100 g for vitamin A and 41.6 ml / 100 g for vitamin B is obtained by the present invention.

간유의 효력은 그 내부에 포함되는 비타민의 함유량으로 결정되기 때문에 비타민이 파괴되지 않고, 완전한 탈취를 행할 수 있는 본 발명의 방법의 실용적 가치는 극히 큰 것이다.Since the effect of the liver oil is determined by the content of the vitamin contained therein, the vitamin is not destroyed, and the practical value of the method of the present invention that can completely deodorize is extremely large.

본 발명에서는 상어, 대구, 고래등의 해양동물의 간장을 충분히 분쇄하여 현탁액으로하고, 그 현탁액을 냉동한다. 냉동 처리에 의한 현탁액중의 유분과 수분이나 간장조직중의 육질(고기질), 섬유, 혈관, 표피기타 노폐물과를 분리 박리시킨다. 유분은 일반적으로 -50℃ 이상이 아니면 동결하지 않는다는 것이 알려져 있다. 냉동처리의 냉각온도는 -15℃--50℃(보다 높은)에서 임의로 선택할 수가 있으나, 조작상, 약-25℃--35℃의 범위가 가장 적당하다. 냉동상태의 정치 기간으로서는 3일보다 짧은 일수로는 불순물의 박리가 불출분하고, 한편 20일보다 더 긴기간 방치하면, 저온에서도 산화 혹은 유효성분의 비율저하가 나타나 바람직하지 못하다. 효율상, 그정치기간은 약 5일간-15일간이 가장 적당하다.In the present invention, the livers of marine animals such as sharks, cods, whales and the like are sufficiently ground to form a suspension, and the suspension is frozen. Separation and separation of oil from suspension by freezing treatment, flesh (meat), fiber, blood vessels, epidermis and other waste products in water or soy tissue are carried out. It is known that oils generally do not freeze above -50 ° C. The refrigeration temperature can be arbitrarily selected from -15 ° C--50 ° C (higher), but in operation, the range of about -25 ° C-35 ° C is most suitable. In the stationary period of the frozen state, the peeling of impurities is undissolved in days shorter than 3 days, and if left for a longer period than 20 days, oxidation or a decrease in the ratio of the active ingredient is not preferable even at low temperatures. For efficiency, the political period is about 5-15 days.

현탁액의 냉동 처리후 자연 해동의 완만한 해동에 의해 생성한 액상물의 표면층에 있어서의 점성의 고형물등을 제고하고, 저부층에 있는 수분 및 불순물등을 분리하고, 얻어진 유상물에 일반법의 탈수처리를 하므로서, 어취 및 불쾌취가 없고, 맛이 양호한 고단위 비타민을 함유한 간유가 얻어진다.After freezing of the suspension, viscous solids in the surface layer of the liquid product produced by gentle thawing of natural thawing are removed, water and impurities in the bottom layer are separated, and the obtained oily substance is subjected to the dehydration treatment of the general method. Thus, cod liver oil containing high unit vitamins having good taste without odor and odor is obtained.

본 발명 방법에 의해 얻어진 간유는 함유성분의 파괴없이, 또 성분 발란스의 변화없이 그 안정성을 유지한다. 그 제품은 종랭의 가열 처리법에 의한 제품보다 상당히 장기간에 걸쳐 변질됨이 없이 보존이 가능하다.The liver oil obtained by the method of the present invention maintains its stability without destroying the components and without changing the component balance. The product can be stored without deterioration for a considerably longer time than the product by longitudinal heat treatment.

본 발명 방법에 의한 간유는 의약으로서 또는 건강식품으로서 유아로 부터 성인가지도 섭취할수가 있다. 이간유는 해드크림, 헤어크림, 루즈등의 화장품 재료로서도 사용된다. 이외에 무좀, 위장, 페기타 내장제 기관의 질환에 대한 의료의 대중요법 및 체내의 신진대사기능의 앙양과 체력의 증강에 현저하게 유효한 체험예가 많이 알려져 있고, 자연 건강식품으로서 널리 어용될 수 있다.Liver oil by the method of the present invention can be consumed by an adult even from an infant as a medicine or a health food. This liver oil is also used as cosmetic ingredients such as head cream, hair cream, and rouge. In addition, there are many known experiences that are remarkably effective in the treatment of diseases of athlete's foot, gastrointestinal, and other organs of peggy other organs, and the improvement of metabolic function in the body and the enhancement of physical strength, and can be widely used as natural health foods.

따라서, 번 발명은 산업상에 공헌하는바 극히 크다.Therefore, the invention of the invention contributes to the industry and is extremely large.

이하 실시예에 의해 본 발명을 설명한다.The invention is illustrated by the following examples.

[실시예]EXAMPLE

심해 상어의 간장을 분쇄기(보니표의 믹서, 기어드모터직결식)으로 분쇄하여 현탁액으로 하고, -25℃--30℃의 분위기에서 그 현탁액을 냉동시키고, 10일간 정지후 자연 해동시킨다. 실온하에서 생성한 액상물의 표면층에 부유하는 점성의 고형물등을 제거하고 저부층에 있는 수분 및 불순물을 분리시키고, 얻어진 유상물에 망초를 가하여, 진공여과시켜 투명한 정제 간유를 얻을 수 있었다.Soy sauce of deep-sea sharks is pulverized with a grinder (Bony's mixer, geared motor direct type) to make a suspension, and the suspension is frozen in an atmosphere of -25 ° C--30 ° C, and then thawed for 10 days. Viscous solids and the like suspended in the surface layer of the liquid product formed at room temperature were removed, water and impurities in the bottom layer were separated, and the obtained oily substance was added to the oily substance to obtain a transparent purified liver oil by vacuum filtration.

얻어진 정제간유는 어취나 불쾌취가 없고, 맛은 양호하고, 그 비타민유등의 영양분석 결과는 아래의 표와 같다.The obtained refined liver oil has no odor or unpleasant odor, tastes good, and the results of nutritional analysis of the vitamin oil are shown in the table below.

또 비교예로서, 종래의 가열처리법(150℃이상으로 가온)에 의해 얻어진 정제 간유의 영양분석 결과도 대비하여 아래 표에 표시한다.In addition, as a comparative example, the nutritional analysis results of the refined liver oil obtained by the conventional heat treatment method (heated at 150 ° C. or higher) are also shown in the table below.

[표][table]

Figure kpo00001
Figure kpo00001

Claims (1)

해양동물의 간장을 분쇄하여 현탁액으로하고, 그 현액을 냉동시키고, 정치후 자연 해동시키고, 생성된 액상물의 표면층에서 고형물등을 제거하고, 다음에 저부층에 있는 수분 및 불순물등을 분리하여 얻어진 유상물을 탈수처리하는 것을 특징으로 하는 고도로 탈취한 고단위 비타민유의 제조법.Soy sauce of marine animals is pulverized to form a suspension, the suspension is frozen, thawed naturally, suspended solids are removed from the surface layer of the resulting liquid, and water and impurities obtained from the bottom layer are separated. A method for producing a highly deodorized high unit vitamin oil, characterized by dehydrating water.
KR1019850002362A 1985-04-09 1985-04-09 Method for producing vitamine containing products KR870001488B1 (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2474292C1 (en) * 2011-09-21 2013-02-10 Олег Иванович Квасенков Method for production of preserves "cod liver with cabbages"
RU2505231C1 (en) * 2013-01-24 2014-01-27 Олег Иванович Квасенков Method for production of preserves "cod liver with cabbages"

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2474292C1 (en) * 2011-09-21 2013-02-10 Олег Иванович Квасенков Method for production of preserves "cod liver with cabbages"
RU2505231C1 (en) * 2013-01-24 2014-01-27 Олег Иванович Квасенков Method for production of preserves "cod liver with cabbages"

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