KR860001063B1 - A method of incombustible composition for spray coating - Google Patents

A method of incombustible composition for spray coating Download PDF

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KR860001063B1
KR860001063B1 KR1019840002304A KR840002304A KR860001063B1 KR 860001063 B1 KR860001063 B1 KR 860001063B1 KR 1019840002304 A KR1019840002304 A KR 1019840002304A KR 840002304 A KR840002304 A KR 840002304A KR 860001063 B1 KR860001063 B1 KR 860001063B1
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mixed
pulverized
mesh
powder
heated
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KR1019840002304A
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Korean (ko)
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KR850007459A (en
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김재운
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김재운
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18Fireproof paints including high temperature resistant paints

Abstract

An incombustible compn. is prepf. of calcium chloride and foaming refractories. Calcium chloride 150g is diluted in water 1800cc. Silicone resins 200cc, sodium silicate 40cc, and polyvinyl acetate resins emulsion 2500cc are mixed and pulverized to 200 450 mesh with 700 - 1000 rpm. Castable refractory 100g, ammonium phosphate 300cc, and silica gel 30g are mixed and pulverized and heated at 800 - 1000≰C. Asbestos powder 30g, slaked lime 1800g, diatomaceous earth 200g and stone powder 600g are mixed in water and heated at 800 - 1200≰C for 3 - 6 hrs, which is pulverized to 200 - 450 mesh. The incombustible compn. is prepd. by heating the mixt. at 100 - 200≰C for 0.5 - 1 hr and precipitating at 30 80≰C for 1 - 2hrs.

Description

분사 도포식 불연제의 제조방법Manufacturing method of spray coating type flame retardant

제1도는 본 발명품을 구조물에 도포하는 실시예도.1 is an embodiment of applying the invention to the structure.

제2도는 본 발명품을 구조물에 도포한 후의 예시단면도.Figure 2 is an exemplary cross-sectional view after applying the present invention to the structure.

본 발명은 염화칼슘, 물, 규소수지, 규산소다, 에말죤 초산비닐수지 케스타블내화재 제일, 인산암모니움, 시리카겔, 석면사 분말, 백석회, 규조토 돌가루 등을 희석 및 혼합하여 내장 시설물 표면에도 포내 화내, 열성을 갖추게 한 분사도포식 불연제의 제조방법에 관한 것이다.The present invention is diluted and mixed with calcium chloride, water, silicon resin, sodium silicate, emalonic vinyl acetate resin castable refractory first, ammonium phosphate, silica gel, asbestos sand powder, white lime, diatomaceous earth stone powder, etc. The present invention relates to a method for producing a spray-coated nonflammable agent that has been provided with fire resistance and heat resistance in a fabric.

종래에 건축 내장에 사용되고 있는 불연제로는 그 견고성이나 섬세함이 높이 평가된 석고 보드가 있었으나, 시공하는 과정에서는 기존내장시설물을 첨거한 후 제시공을 해야만 했기에 여기에 따른 경제적인 부담이 커서 적합하지 않아 일반화되지를 못하였으며, 흔히 사용되는 합성수지류의 미장재와 벽지류는 우선 내부시설을 장식하기에는 시공이 간편하나, 부주의로 화재가 발생하였을 때는 합성수지류가 연소되는 과정에 발생하는 아황산 까스의 배출로 인해 인명의 피해를 발생시키는 결점이 있었다.In the past, there were gypsum boards that were highly evaluated for their robustness and delicacy. However, in the process of construction, they had to be added after adding existing interior facilities. Plaster and wallpaper of commonly used synthetic resins are not easy to generalize, but they are easy to install in order to decorate internal facilities.However, in case of inadvertent fire, the dissipation of sulfurous acid cuts generated in the process of burning synthetic resins There was a defect that caused damage to life.

본 발명은 상기와 같은 종래의 문제점을 해결하기 위해 건축물의 내부구조를 개조할 때에 천거 또는 훼손하지 않고, 내장재를 불연처리하여 화재가 발생하여도 유독까스의 발생을 방지할 수 있는 불연제를 제조하여 간편 신속히 분사도포 작업 공정을 단축하여 경제적으로도 유익하도록 한 것으로 그 제조공정별로 상세히 설명하면 다음과 같다.The present invention provides a non-flammable agent that can prevent the generation of toxic cutlet even if a fire occurs by flame retardant treatment without damaging or damaging when modifying the internal structure of the building to solve the conventional problems as described above. In order to shorten the spray coating work process quickly and economically beneficial as described in detail by the manufacturing process as follows.

[제1공정][Step 1]

염화칼슘(Calcium Choride Cacl2) 150gCalcium Choride Cacl 2 150g

물(H2O) 1800CCWater (H 2 O) 1800CC

를 잘 희석하여 본 발명의 불연제가 분사도포경화될 때에 균열 및 화재발생시의 착화를 방지하는 작용을 한다.By diluting well, the flame retardant of the present invention acts to prevent ignition during cracking and fire when spray coating and curing.

[제2공정][Step 2]

규소수지(Silicone Resins) 200CCSilicon Resins 200CC

규산소다(Soidum Silicate NaOnSiO2XH2O) 40CCSodium silicate (Soidum Silicate NaO n SiO 2 XH 2 O) 40CC

에말죤 초산비닐수지(Polyvinyl Acetate Resins emulsion) 250CCPolyvinyl Acetate Resins emulsion 250CC

을 혼합하여 회전속도가 700-1000rpm인 분쇄기로 분쇄하여 입도(粒度)가 200-450매쉬인 약제를 제조 접착력을 좋게하고 화재발생시에 불연제층이 열에 의해 발포되어To grind with a grinder with a rotation speed of 700-1000rpm to manufacture a drug with a particle size of 200-450 mesh.Adhesion is improved and the fire retardant layer is foamed by heat in case of fire.

포층을 형성하게 한다.Allow to form a fabric layer.

[제3공정][Step 3]

케스타블 내화재(Castablerefractory) 100gCastable refractory 100g

제1인산 암모니움(NH4H2PO4) 300CCMonomonium phosphate (NH 4 H 2 PO 4 ) 300CC

시리카겔(Silica Gel SiO2XH2O) 30g30 g of silica gel SiO 2 XH 2 O

을 혼하여 200-450 매쉬정도의 입도(粒度)를 가진 분말로 분쇄한 후 이를 800℃-1000℃로 재차가열하면서 혼합 용응시켜 내열성을 높이고, 화재발생시에 유독까스의 발생을 중화억제하는 작용을 한다.The mixture is pulverized into a powder having a particle size of 200-450 mash and then heated again to 800 ℃ -1000 ℃, mixed and melted to increase the heat resistance, and to suppress the occurrence of poisonous cutlet in the event of fire. do.

[제4공정][Step 4]

석면사 분말 30g 규조토(Diatomaceous Earth) 200gAsbestos Sand Powder 30g Diatomaceous Earth 200g

백석회 1800g 돌가루 600gWhite lime 1800g stone powder 600g

를 잘 혼합하여 200-450 매쉬의 입도를 가진 분말로 분쇄한 후 10-20%의 물과 혼합 800℃-1200℃의 온도로 3-6시간 가열 다시 200-450매쉬 정도로 분쇄하여 토석분을 만들어 불길을 차단하여 우수한 단열작용을 한다.Mixed well and pulverized into a powder having a particle size of 200-450 mash, and then mixed with 10-20% of water and heated at a temperature of 800 ° C.-1200 ° C. for 3-6 hours and pulverized again to 200-450 mash to make earth powder. Blocks flames and provides excellent thermal insulation.

[제5공정][Step 5]

제1, 2, 3공정에서 각각의 용량비로 희석, 및 혼합된 발포성내화제를 제조 침전시키고 제4공정에서의 혼합물을 적정배합비로 혼합하여 100℃-200℃로 30분-1시간동안 가열한 후 1시간 내지 2시간동안 30℃-80℃의 온도를 유지하면서 침전시킨다.In the first, second, and third steps, dilution and mixed foamed refractory agent were prepared and precipitated, and the mixture in the fourth step was mixed at an appropriate mixing ratio and heated to 100 ° C.-200 ° C. for 30 minutes to 1 hour. After 1 hour to 2 hours to precipitate while maintaining a temperature of 30 ℃ -80 ℃.

이때에 염료를 적당량첨가하면 본 발명의 불연제를 착색할 수 있다.At this time, if the dye is added in an appropriate amount, the flame retardant of the present invention can be colored.

위와 같은 제조공정을 거쳐 제조된 본 발명의 불연제(2)는 구조물을 파괴하지 않고, 목재나 벽지등 구조물(1)의 어디에든지 적정층이 형성되게 자동제어식 분사기(3)로 분사를 하면 불연층(4)이 즉시 견고한 석고 보드와 같은 성질로 바뀌게 되어 굳게되며, 이 때보다 시각적으로 조화를 이루게 하려면 수성패인트(5)로 미적 감각을 살려 책색을 할 수도 있다.The non-flammable agent (2) of the present invention manufactured through the manufacturing process as described above does not destroy the structure, non-combustible when sprayed to the automatic control injector (3) to form an appropriate layer anywhere in the structure (1), such as wood or wallpaper The layer (4) immediately turns into a solid gypsum board-like property and hardens. For a more visual harmony, the water-based paint (5) can be used to color aesthetics.

본 발명의 불연제는 목재, 직물, 종이, 플라스틱 등의 가연성 물질에 분사 또는 도포하여 가연성 건축 내장재를 불연처리할 수 있고, 화재발생시에는 발포되어 절연층을 형성하여 단열 작용을 하여 유독까스를 중화억제하는 효과가 있다.The non-flammable agent of the present invention can disinfect the combustible building interior materials by spraying or applying to a combustible material such as wood, fabric, paper, plastic, etc., and in case of a fire, it foams to form an insulating layer to insulate the poisonous cutlet. It has a suppressing effect.

Claims (1)

염화칼슘 150g,과 물 180CC를 혼합하고 규소수지 200CC, 규산소다 40CC, 에말죤 초산비닐수지 250CC,를 혼합 회전속도가 700-1000rpm인 분쇄기로 분쇄하여 입도(粒度)가 200-450매쉬인 분말로 제조하고 케스타블 내화재 100g, 제1인산 암모니움 300CC, 시리카겔 30g, 을 혼합 분쇄한 후 800℃-1000℃로 재차 가열한 다음 석면사분말 30g, 백석회 1800g, 규조토 200g, 돌가루 600g를 물과 혼합 800℃-1200℃ 온도로 3-6시간 가열하고, 200-450매쉬인 입도로 분쇄한 뒤, 공정별로 희석 혼합된 혼합물을 100℃-200℃로 30분 내지 1시간동안 가열한 후 1시간-2시간 동안 30℃-80℃의 온도로 유지하면서 침전시킨 후 200-450매쉬 이상의 입도를 갖도록 제조함을 특징으로 하는 분사도포식 불연제의 제조방법.150 g of calcium chloride and 180 CC of water are mixed, and silicon powder 200CC, sodium silicate 40CC, emerald vinyl acetate resin 250CC are pulverized with a grinder with a mixing rotation speed of 700-1000rpm to produce a powder having a particle size of 200-450 mesh. 100 g of castable refractory, ammonium monophosphate 300CC, and 30 g of silica gel were mixed and pulverized and then heated again to 800 ° C.-1000 ° C., followed by 30 g of asbestos powder, 1800 g of white lime, 200 g of diatomaceous earth and 600 g of stone powder. Mixed 3-6 hours at 800 ℃ -1200 ℃ temperature, pulverized to a particle size of 200-450 mesh, and diluted by process, the mixed mixture is heated to 100 ℃ -200 ℃ for 30 minutes to 1 hour and then 1 hour Method of producing a spray-coated nonflammable, characterized in that to prepare to have a particle size of 200-450 mesh or more after being precipitated while maintaining at a temperature of 30 ℃ -80 ℃ for -2 hours.
KR1019840002304A 1984-04-26 1984-04-26 A method of incombustible composition for spray coating KR860001063B1 (en)

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KR1019840002304A KR860001063B1 (en) 1984-04-26 1984-04-26 A method of incombustible composition for spray coating

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KR1019840002304A KR860001063B1 (en) 1984-04-26 1984-04-26 A method of incombustible composition for spray coating

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KR850007459A KR850007459A (en) 1985-12-04
KR860001063B1 true KR860001063B1 (en) 1986-08-04

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