KR830010062A - Dl-시스테인의 제조방법 - Google Patents
Dl-시스테인의 제조방법 Download PDFInfo
- Publication number
- KR830010062A KR830010062A KR1019820002428A KR820002428A KR830010062A KR 830010062 A KR830010062 A KR 830010062A KR 1019820002428 A KR1019820002428 A KR 1019820002428A KR 820002428 A KR820002428 A KR 820002428A KR 830010062 A KR830010062 A KR 830010062A
- Authority
- KR
- South Korea
- Prior art keywords
- producing
- trithiocarbonate
- cysteine
- cysteine according
- acid
- Prior art date
Links
- XUJNEKJLAYXESH-UHFFFAOYSA-N Cysteine Chemical compound SCC(N)C(O)=O XUJNEKJLAYXESH-UHFFFAOYSA-N 0.000 title claims 16
- 229940078469 dl- cysteine Drugs 0.000 title claims 8
- 238000000034 method Methods 0.000 title claims 5
- HIZCIEIDIFGZSS-UHFFFAOYSA-L trithiocarbonate Chemical compound [S-]C([S-])=S HIZCIEIDIFGZSS-UHFFFAOYSA-L 0.000 claims 7
- 239000012989 trithiocarbonate Substances 0.000 claims 7
- 239000002253 acid Substances 0.000 claims 3
- 238000004519 manufacturing process Methods 0.000 claims 3
- -1 amino carboxyethyl Chemical group 0.000 claims 2
- 238000000354 decomposition reaction Methods 0.000 claims 2
- 150000002148 esters Chemical class 0.000 claims 2
- ORQLXCMGAMWKMJ-REOHCLBHSA-N (2r)-2-amino-3-bromopropanoic acid Chemical compound BrC[C@H](N)C(O)=O ORQLXCMGAMWKMJ-REOHCLBHSA-N 0.000 claims 1
- ASBJGPTTYPEMLP-UHFFFAOYSA-N 3-chloroalanine Chemical group ClCC(N)C(O)=O ASBJGPTTYPEMLP-UHFFFAOYSA-N 0.000 claims 1
- 102100028292 Aladin Human genes 0.000 claims 1
- 101710065039 Aladin Proteins 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims 1
- 150000001342 alkaline earth metals Chemical class 0.000 claims 1
- 150000003863 ammonium salts Chemical class 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 150000007522 mineralic acids Chemical class 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
- C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
- C07C323/57—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups
- C07C323/58—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups with amino groups bound to the carbon skeleton
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (7)
- β-할로게노알라닌과 트리티오 탄산염과를 반응시켜서 생성한 트리티오탄산의 모노(아미노 카르복시에틸)에스테르를 산분해함을 특징으로 하는 DL-시스테인의 제조방법.
- 제1항에 있어서, β-할로게노알라닌이 β-클로로알라닌 또는 β-브로모알라닌인 DL-시스테인의 제조방법.
- 제1항에 있어서, 트리티오탄산염이 트리티오탄산의 알카리금속, 알카리토류 금속 또는 암모늄염인 DL-시스테인의 제조방법.
- 제1항에 있어서, β-할로게노알라딘의 1몰에 대하여 트리티오탄산염을 1∼10몰비 사용하는 DL-시스테인의 제조방법.
- 제1항에 있어서, β-할로게노 알라딘과 트리티오 탄산염과의 반응 온도가 -20∼100℃인 DL-시스테인의 제조방법.
- 제1항에 있어서, 트리티오탄산의 모노(아미노 카르복시에틸) 에스테트의 산분해에 사용하는 산이 무기산인 DL-시스테인의 제조방법.
- 제1항에서, 산분해 온도가 0∼80℃인 DL-시스테인의 제조방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP81-82453 | 1981-06-01 | ||
JP82453 | 1981-06-01 | ||
JP56082453A JPS57200356A (en) | 1981-06-01 | 1981-06-01 | Preparation of dl-cysteine |
Publications (2)
Publication Number | Publication Date |
---|---|
KR830010062A true KR830010062A (ko) | 1983-12-24 |
KR860001891B1 KR860001891B1 (ko) | 1986-10-24 |
Family
ID=13774933
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR8202428A KR860001891B1 (ko) | 1981-06-01 | 1982-05-31 | Dl-시스테인의 제조방법 |
Country Status (10)
Country | Link |
---|---|
US (1) | US4453008A (ko) |
EP (1) | EP0079966B1 (ko) |
JP (1) | JPS57200356A (ko) |
KR (1) | KR860001891B1 (ko) |
AU (1) | AU550974B2 (ko) |
CA (1) | CA1183870A (ko) |
DE (1) | DE3263099D1 (ko) |
IT (1) | IT1157942B (ko) |
MX (1) | MX156241A (ko) |
WO (1) | WO1982004251A1 (ko) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0623182B2 (ja) * | 1986-06-19 | 1994-03-30 | 三井東圧化学株式会社 | L−システイン塩酸塩1水和物を分離する方法 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2710304A (en) * | 1955-06-07 | Production of cystein and isocystein | ||
FR1491204A (fr) * | 1962-08-10 | 1967-08-11 | Santen Pharmaceutical Co Ltd | Procédés pour la préparation des alpha-et beta mercaptopropionylglycocolle et de leurs dérivés |
GB1261345A (en) * | 1968-03-07 | 1972-01-26 | Ici Ltd | Sulphur-containing benzyl derivatives and pesticidal compositions containing them |
CA1009252A (en) * | 1972-10-03 | 1977-04-26 | Santen Pharmaceutical Co. | N-(mercaptoacyl) aminoacids |
FR2455606A1 (fr) * | 1979-05-04 | 1980-11-28 | Elf Aquitaine | Nouveau procede de preparation d'organoetains |
JPS55164669A (en) * | 1979-06-08 | 1980-12-22 | Showa Denko Kk | Preparation of cysteine |
-
1981
- 1981-06-01 JP JP56082453A patent/JPS57200356A/ja active Granted
-
1982
- 1982-05-26 US US06/459,533 patent/US4453008A/en not_active Expired - Fee Related
- 1982-05-26 EP EP82901614A patent/EP0079966B1/en not_active Expired
- 1982-05-26 AU AU85201/82A patent/AU550974B2/en not_active Ceased
- 1982-05-26 DE DE8282901614T patent/DE3263099D1/de not_active Expired
- 1982-05-26 WO PCT/JP1982/000198 patent/WO1982004251A1/ja active IP Right Grant
- 1982-05-27 MX MX192889A patent/MX156241A/es unknown
- 1982-05-31 CA CA000404143A patent/CA1183870A/en not_active Expired
- 1982-05-31 KR KR8202428A patent/KR860001891B1/ko active
- 1982-05-31 IT IT21602/82A patent/IT1157942B/it active
Also Published As
Publication number | Publication date |
---|---|
US4453008A (en) | 1984-06-05 |
AU8520182A (en) | 1982-12-07 |
IT1157942B (it) | 1987-02-18 |
KR860001891B1 (ko) | 1986-10-24 |
JPS6124385B2 (ko) | 1986-06-10 |
WO1982004251A1 (en) | 1982-12-09 |
DE3263099D1 (en) | 1985-05-23 |
IT8221602A0 (it) | 1982-05-31 |
JPS57200356A (en) | 1982-12-08 |
EP0079966A4 (en) | 1983-09-30 |
EP0079966A1 (en) | 1983-06-01 |
MX156241A (es) | 1988-07-27 |
AU550974B2 (en) | 1986-04-10 |
EP0079966B1 (en) | 1985-04-17 |
CA1183870A (en) | 1985-03-12 |
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