KR20240051754A - Natural bath treatments based on juice exytraction cake of ginger and its preparation method - Google Patents

Natural bath treatments based on juice exytraction cake of ginger and its preparation method Download PDF

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KR20240051754A
KR20240051754A KR1020220131847A KR20220131847A KR20240051754A KR 20240051754 A KR20240051754 A KR 20240051754A KR 1020220131847 A KR1020220131847 A KR 1020220131847A KR 20220131847 A KR20220131847 A KR 20220131847A KR 20240051754 A KR20240051754 A KR 20240051754A
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ginger
cake
bath
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powder
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손호용
이성옥
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이성옥
국립안동대학교 산학협력단
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216Solid or semisolid forms
    • A61K8/022Powders; Compacted Powders
    • A61K8/0225Granulated powders
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q15/00Anti-perspirants or body deodorants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/522Antioxidants; Radical scavengers

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  • Microbiology (AREA)
  • Mycology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

본 발명은 생강 착즙 후 케이크인 생강박을 주성분으로 하는 입욕제 조성물에 관한 것으로서, 보다 구체적으로는, 생강을 착즙 후 발생하는 케이크를 60~70℃에서 6-10시간 건조하고 이를 50~300메쉬로 분쇄하여 건조 생강박을 조제하고, 상기 건조 생강박 90~95중량%에 한약재 또는 허브류를 5~10중량%로 첨가하여 제조된 입욕제 조성물에 관한 것이다. 본 발명의 생강 착즙 후 케이크를 주성분으로 하는 입욕제는 특유의 생강 향미의 제공과 함께 강력한 항균, 항산화 및 소취 활성을 나타내어 소비자 기호도가 높으며, 현재까지 별도 용도없이 폐기되고 있는 생강 착즙 후 케이크를 이용하므로 환경 보호, 자원 재활용 및 아로마 테라피 산업의 경제성 확보에 기여할 것으로 판단된다. The present invention relates to a bath salt composition containing ginger gourd, which is a cake after squeezing ginger, as the main ingredient. More specifically, the cake generated after squeezing ginger is dried at 60-70°C for 6-10 hours and cut into 50-300 mesh. It relates to a bath additive composition prepared by pulverizing dried ginger gourd and adding 5 to 10 weight % of herbal medicine or herbs to 90 to 95 weight % of the dried ginger gourd. The bath agent of the present invention, which is mainly composed of cake after ginger extraction, provides a unique ginger flavor and exhibits strong antibacterial, antioxidant and deodorizing activities, so it has a high consumer preference. It uses cake after ginger extraction, which has been discarded without any other purpose to date. It is believed that it will contribute to environmental protection, resource recycling, and securing the economic feasibility of the aromatherapy industry.

Description

생강박을 주성분으로 하는 천연 입욕제 조성물 및 그 제조방법{NATURAL BATH TREATMENTS BASED ON JUICE EXYTRACTION CAKE OF GINGER AND ITS PREPARATION METHOD}Natural bath additive composition containing ginger gourd as the main ingredient and method for manufacturing the same {NATURAL BATH TREATMENTS BASED ON JUICE EXYTRACTION CAKE OF GINGER AND ITS PREPARATION METHOD}

본 발명은 생강 착즙 후 케이크인 생강박을 주성분으로 하는 입욕제 조성물에 관한 것으로서, 보다 구체적으로는, 생강을 착즙 후 발생하는 케이크를 60~70℃에서 6-10시간 건조하고 이를 50~300메쉬로 분쇄하여 건조 생강박을 조제하고, 상기 건조 생강박 90~95중량%에 한약재 또는 허브류를 5~10중량%로 첨가하여 제조된 입욕제 조성물에 관한 것이다. The present invention relates to a bath salt composition containing ginger gourd, which is a cake after squeezing ginger, as the main ingredient. More specifically, the cake generated after squeezing ginger is dried at 60-70°C for 6-10 hours and cut into 50-300 mesh. It relates to a bath additive composition prepared by pulverizing dried ginger gourd and adding 5 to 10 weight % of herbal medicine or herbs to 90 to 95 weight % of the dried ginger gourd.

현대인들은 환경오염, 짜고 매운 인스턴트 식품에 의한 소화장애, 사회 구조적인 압박 및 자연 노화 등으로 발생하는 스트레스를 목욕을 통해 완화하고 있다. 우리나라는 특히 약수 온천의 개념을 가지고 있어 미네랄, 유황 등이 풍부한 온천수 목욕을 힐링여행의 대표로 인식하고 있다.Modern people are relieving stress caused by environmental pollution, digestive problems caused by salty and spicy instant foods, social structural pressure, and natural aging through bathing. Korea especially has the concept of medicinal hot springs, and bathing in hot spring water rich in minerals and sulfur is recognized as a representative healing trip.

입욕제는 목욕 중에 첨가하는 제품으로, 애엽, 건강, 녹차 등과 같은 약초 등을 탕속에 넣어 목욕하거나, 또는 이러한 약초,허브류의 추출물을 건조하여 분말로 제조한 것을 탕속에 첨가하는 방식으로 사용하고 있다. 이러한 입욕제는 피부 세정 및 탄력증진, 유해균의 사멸, 피부 보습 유지, 혈액순환 촉진 등의 직접적 건강 기여은 물론 은은한 향으로 인한 긴장완화, 정신건강에도 도움이 된다. 따라서, 최근에는 다양한 식물 허브류가 포함된 입욕제 시장이 빠르게 성장하고 있다. Bath additives are products that are added during bathing, and are used by putting medicinal herbs such as leaf, health, green tea, etc. in a bath, or by drying the extracts of these herbs and herbs and making them into powder and adding them to the bath. These bath salts not only contribute directly to health by cleansing the skin and improving elasticity, killing harmful bacteria, maintaining skin moisture, and promoting blood circulation, but also help relieve tension and mental health due to the subtle scent. Therefore, recently, the bath salt market containing various plants and herbs has been growing rapidly.

국내의 경우, 족욕제는 입욕제에 비해 아직 산업화가 활성화되지 못한 분야이나, 한방에서는 신체의 건강이 발과 많은 관련이 있다고 알려져 있어 수험생, 임산부, 노약자 등을 대상으로 족욕제에 대한 관심이 증가하고 있는 실정이다. 족욕은 42℃ 정도의 뜨거운 물에 10∼20분간 발을 담그는 온욕의 일종으로 입욕과 차이가 있으나, 국내에서는 입욕제와 족욕제의 큰 차이가 없이 사용되고 있는 실정이다. 그러나, 족욕은 입욕에 비해 간편하면서도, 발부터 몸을 따뜻하게 해주고 혈액순환과 자율신경계를 조절하여 빠르게 피로회복 및 스트레스 완화에 기여하는 장점을 가진다.In Korea, foot baths are a field that has not yet been industrialized compared to bath salts, but in oriental medicine, it is known that physical health is closely related to feet, so interest in foot baths is increasing among test takers, pregnant women, the elderly, etc. There is a situation. A foot bath is a type of warm bath in which the feet are soaked in hot water of about 42℃ for 10 to 20 minutes. It is different from a bathing bath, but in Korea, there is no significant difference between bath salts and foot baths. However, foot baths are simpler than bathing and have the advantage of warming the body starting from the feet and regulating blood circulation and the autonomic nervous system, contributing to rapid recovery from fatigue and stress relief.

국내 입욕제 및 족욕제에 대한 연구로는 족욕이 수험생의 스트레스 및 피로에 미치는 효과 -아로마 오일과 발효추출물의 비교연구(오희선 외, 2010. 한국산학기술학회논문지 11: 402-408) 및 아토탕의 항아토피 및 피부재생 효과(김건우, 2017. 대전대학교 박사논문) 등이 있으나 상대적으로 학술적 연구는 미미한 실정이다. 반면, 국내 입욕제 및 족욕제에 대한 특허로는 다양한 입욕제, 족욕제가 보고된 바 있으며, 대한민국 등록특허 제10-1506277호에 [생약재가 함유된 족욕용 소금 조성물], 제10-2359844호에 [천연 입욕제의 제조 방법 및 천연 입욕제] 및 제10-0586268호에 [건강증진 약초족욕제의 제조방법]에는 천궁, 당귀, 어성초, 녹차, 건강, 진피, 계피, 상백피, 애엽 등 식용 및 약용으로 사용하는 한약재를 주성분으로 한 한방족욕제를 제조하는 방법이 알려져 있으며, 제10-1386724호에 [입욕제 조성물 및 그 제조방법], 제10-0540841호에 [제분된 쑥 분말을 이용한 전신입욕제의 제조방법], 제10-2347701호에 [아로마 향의 장시간 유지가 가능한 입욕제] 등이 개시되어 있다. 또한, 대한민국 공개특허 제10-2013-0014694호에는 [부직포 티백을 이용한 1회용 족욕제 제조방법], 제10-2022-0068595호에는 [식물 분말로 구성된 기능성 입욕제 조성물], 제10-2004-0081248호에는 [울금추출물이 함유된 기능성 한방입욕제의 제조방법]이 공개되어 있다. 그러나, 현재까지 항산화, 항균, 소취 활성이 우수한 생강박, 특히, 20μm의 마이크로 생강박을 이용한 입욕제 및 족욕제는 보고된 바 없다. Research on domestic bath and foot baths includes the effect of foot baths on stress and fatigue of test takers - a comparative study of aroma oils and fermented extracts (Oh Hee-seon et al., 2010. Journal of the Korean Society of Industrial-Academic Technology 11: 402-408) and Ato Tang's There are anti-atopy and skin regeneration effects (Kim Geon-woo, 2017. Daejeon University doctoral thesis), but academic research is relatively minimal. On the other hand, various bath and foot baths have been reported as patents for domestic bath and foot baths, and in Korea Patent No. 10-1506277 [Foot bath salt composition containing herbal medicine] and No. 10-2359844 [Natural salt composition] Manufacturing method of bath salts and natural bath salts] and No. 10-0586268 [Manufacturing method of health-promoting herbal foot baths] contains ingredients used for edible and medicinal purposes such as Cheongung, angelica root, Houttuynia cordata, green tea, health, dermis, cinnamon, Mori alba bark, and leaves. Methods for manufacturing oriental foot baths containing herbal medicine as the main ingredient are known, and are described in No. 10-1386724 [Bathing agent composition and method for manufacturing the same], and No. 10-0540841 [Method for manufacturing a full body bathing agent using milled mugwort powder]. , No. 10-2347701 discloses [Bath additives capable of maintaining aroma for a long time], etc. In addition, Republic of Korea Patent Publication No. 10-2013-0014694 [Method for manufacturing disposable foot bath using non-woven tea bags], No. 10-2022-0068595 [Functional bath bath composition composed of plant powder], No. 10-2004-0081248 In the issue, [Method for manufacturing a functional herbal bathing agent containing turmeric extract] is disclosed. However, to date, there have been no reports of bath or foot baths using ginger gourd, especially 20μm micro ginger gourd, which has excellent antioxidant, antibacterial, and deodorizing activities.

한편, 생강(Zingiber officinale)은 생강과(Zingiberaceae)의 아열대, 열대산 다년생 초본식물의 하나로서, 지하부 근경은 특이한 맛과 향을 가지고 있어, 국내에서는 마늘, 고추와 함께 3대 향신료로 이용되고 있다. 생강은 그대로 식품으로 이용되기도 하며, 김치, 젓갈, 과자류 등의 다양한 식품산업에 양념으로도 이용되고 있다. 또한, 건조한 생강(건강 또는 건조분말), 올레오레진(생강 함유지), 생강 정유 등의 제품 형태로 가공되어 식의약 소재 및 화장품 소재로 이용되기도 한다(김선희 2013. 한양대학교 박사논문). 실제 생강은 본초강목에 백사(백가지 질병)를 방지한다고 기술될 만큼 다양한 생리활성이 알려져 있으며, 한방에서는 건위약 및 소화불량, 구토, 진통에 효과가 우수하다고 알려져 있다. 생강의 생약명은 [건강]이며, 일반인은 [새앙]으로도 많이 부른다. 고려시대에는 왕의 하사품으로 사용될 만큼 진기하였으며, 인도의 고대의학서적 [아유르데바]에는 "신이 내린 치료제"로 소개되어 있다. Meanwhile, ginger ( Zingiber officinale ) is one of the subtropical and tropical perennial herbaceous plants of the Zingiberaceae family. The underground rhizome has a unique taste and aroma, and is used as one of the three major spices in Korea along with garlic and red pepper. Ginger is used as a food as is, and is also used as a seasoning in various food industries such as kimchi, salted fish, and confectionery. In addition, it is processed into products such as dried ginger (health or dried powder), oleoresin (ginger-containing fat), and ginger essential oil, and is used as a food and pharmaceutical material and cosmetic material (Kim Seon-hee, 2013. Doctoral thesis, Hanyang University). In fact, ginger is known for its diverse physiological activities, so much so that it is described in the herbal medicine class as preventing white snakes (hundred diseases), and in oriental medicine, it is known to be effective in treating stomach upset, indigestion, vomiting, and pain relief. The herbal medicine name for ginger is [Health], but the general public also calls it [Saeang]. It was so rare that it was used as a king's gift during the Goryeo Dynasty, and is introduced as a "cure given by God" in India's ancient medical book [Ayurdeva].

생강의 주요 생산국은 인도이며, 전 세계 생산량의 50% 이상을 차지한다. 국내에서는 경북 안동, 영주지역과 충남 서산, 당진지역, 전북 완주지역에서 주로 생산되고 있다. 생강의 품종은 재래종, 개량종으로, 또한 조생종, 중생종, 만생종으로 분류하며, 크기에 따라 소생강, 중생강, 대생강 등으로 구분한다. 농촌진흥청 식품분석 DB(2006)에 따르면, 생강은 단백질 1.5%. 지방 0.2%. 탄수화물 13.9%, 회분 1.1%, 수분 83.3%를 가지고 있으며, 다양한 비타민과 미네랄, 필수 아미노산을 포함하고 있다. 특히, 생강은 100g당 344mg의 칼륨을 가지고 있어, 염분 배출에도 도움이 된다. 생강의 유효성분으로는 다양한 hydrocarbon, ketone 류의 증류성분과 zingiberene 등의 향기성분, borneol, gingiberol 등의 기름성분, 매운맛의 6-ginegerol, 6-shagaol 등이 알려져 있다. 이들 성분은 항산화 활성(이은주 외, 2011, 한국식품과학회지, 43: 469-474), 항균작용(이명희 외, 2012. J. Fd Hyg. Safety 27: 109-116), 항 위염, 항위궤양 작용(김신정 외, 2012, J Korean Soc Food Sci Nutr, 41: 1528-1533), 항암 작용(이예솔, 2013. 울산대학교 박사논문), 항진해 작용, 해독 진정작용(한효선 2016, 건국대학교 박사논문), pancreatic lipase 저해작용(Bae JS 등, 2011. Korean J. Food Preserv. 18: 390-396), 혈중 콜레스테롤 저하 작용(오수정, 2015. 이화여자대학교 석사논문), 간보호 작용(Koo SW 외, 2012, J Vet Clin 29: 441-446), 뇌세포 보호 작용(정길생 외, 2010, 생약학회지 41: 190-195) 등 다양한 생리활성이 알려져, 현재 생강은 식품 부재료이면서 건강 기능성 식품소재로 각광받고 있다.The main producer of ginger is India, accounting for more than 50% of global production. In Korea, it is mainly produced in Andong and Yeongju areas of Gyeongbuk, Seosan and Dangjin areas of South Chungcheong Province, and Wanju area of Jeollabuk-do. Ginger varieties are classified into native, improved, and early-ripening, medium-growing, and late-ripening varieties, and are classified into small, medium, and large ginger depending on their size. According to the Rural Development Administration Food Analysis DB (2006), ginger has 1.5% protein. Fat 0.2%. It has 13.9% carbohydrates, 1.1% ash, and 83.3% moisture, and contains various vitamins, minerals, and essential amino acids. In particular, ginger has 344mg of potassium per 100g, which also helps excrete salt. The active ingredients of ginger are known to include distilled components such as various hydrocarbons and ketones, aroma components such as zingiberene, oil components such as borneol and gingiberol, and spicy 6-ginegerol and 6-shagaol. These ingredients have antioxidant activity (Lee Eun-ju et al., 2011, Journal of the Korean Society of Food Science, 43: 469-474), antibacterial activity (Lee Myung-hee et al., 2012. J. Fd Hyg. Safety 27: 109-116), anti-gastritis, and anti-gastric ulcer activity. (Kim Shin-jeong et al., 2012, J Korean Soc Food Sci Nutr, 41: 1528-1533), anti-cancer activity (Lee Ye-sol, 2013. Doctoral thesis, Ulsan University), anti-tussive action, detoxification and sedative action (Han Hyosun, 2016, Doctoral thesis, Konkuk University) ), pancreatic lipase inhibitory action (Bae JS et al., 2011. Korean J. Food Preserv. 18: 390-396), blood cholesterol lowering action (Oh Soo-jeong, 2015. Ewha Womans University master's thesis), liver protection (Koo SW et al., Ginger is known to have various physiological activities such as 2012, J Vet Clin 29: 441-446) and brain cell protection (Jeong Gil-saeng et al., 2010, Journal of Herbal Medicine 41: 190-195). Ginger is currently in the spotlight as a food supplement and a health functional food ingredient. there is.

생강은 저장성이 매우 낮아 장기간 저장이 어려우며, 국내의 경우 10월 수확기 이후 홍수 출하가 반복되어 매년 가격폭락이 나타나고 있다. 또한, 어렵게 저장한 생강은 3월 이후 발아율이 매우 높게 나타나면서 저장 생강의 50% 이상이 상품성을 상실하게 된다. 따라서, 생강을 이용한 가공제품 개발 연구가 꾸준히 이루어져 왔으며, 생강의 매운 관능성을 개선하고, 기능성을 강화하려는 많은 시도가 있었다. 대표적인 연구로 생강의 효소처리(Schweiggert U 등, 2008, Journal of Food Engineering. 84: 2838), 열처리(김희수 등, 2010, 한국식품저장유통학회지, 17: 784-792), 유산균 발효(Chun, YG 등, 2011. Korean J. Food Sci. Technol., 43, 249-254), 고분자 수용성 물질(예들 들어, maltodextrin)을 이용한 탈수 건조반응(cytorrhysis) 등이 알려져 있다(김민희 외, 2009. 한국식품과학회지 41: 146-150). Ginger has very low storability, making it difficult to store for a long period of time, and in Korea, flood shipments are repeated after the harvest season in October, causing prices to plummet every year. In addition, ginger that was stored with difficulty shows a very high germination rate after March, and more than 50% of the stored ginger loses its marketability. Therefore, research on the development of processed products using ginger has been continuously conducted, and many attempts have been made to improve the spicy sensory properties of ginger and strengthen its functionality. Representative studies include enzyme treatment of ginger (Schweiggert U et al., 2008, Journal of Food Engineering. 84: 2838), heat treatment (Hee-soo Kim et al., 2010, Journal of Korean Food Storage and Distribution, 17: 784-792), and lactic acid fermentation (Chun, YG). et al., 2011. Korean J. Food Sci. Technol., 43, 249-254), dehydration drying reaction (cytorrhysis) using polymer water-soluble substances (e.g. maltodextrin), etc. are known (Minhee Kim et al., 2009. Korean Food Department) Journal of Korean Studies 41: 146-150).

생강과 관련된 특허로는 대한민국 등록특허 제10-1224873호에 생강의 맵고 자극적인 맛 및 향을 감소시켜 향미를 향상시키는 "발효 생강의 제조방법", 등록특허 제10-0880127호에 "발효생강 음료수 제조방법", 등록특허 제10-1833345호에 생강과 치자를 엿기름을 이용한 발효법을 이용하여 차를 제조하는 "생강 발효차의 제조방법", 등록특허 제10-2035428호에 "발효생강엑기스 및 그 제조방법", 등록특허 제10-1736809에 "발효 생강차 조성물 제조 방법", 등록특허 제10-1866636호에 "발효생강과 숙성생강을 포함하는 혈행개선용 조성물", 등록특허 제10-1634232호에 "생강발효액 및 그 제조 방법", 등록특허 제10-1254740호에 "발효생강 추출물의 제조방법 및 이를 이용한 생강차", 등록특허 제10-1486293호에 "발효 생강 식품 및 이의 제조방법", 등록특허 제10-1713095호에 "Schizosaccharomyces pombe를 이용한 생강 발효물 및 이의 용도", 등록특허 제10-2118059호에 "발효생강 추출물을 포함하는 대사성 질환 예방 또는 치료용 약학 조성물", 등록특허 제10-1967073호에 "Bacillus subtilis를 이용한 발효생강추출물과 진공건조 홍삼농축액을 유효성분으로 포함하는 면역 증강용 조성물"이 개시되어 있으며, 대한민국 공개특허 제10-2014-0145875호에 "발효된 생강 부산물을 유효성분으로 포함하는 살모넬라균에 대한 내성 증진용 사료 첨가제" 등 생강 발효물에 대한 특허가 대부분인 실정이다. 그러나, 현재까지 생강을 착즙한 후 발생하는 [생강 착즙후 케이크]를 이용한 입욕제 및 족욕제에 연구나 관련 특허는 현재까지 알려진 바 없다. Patents related to ginger include Korean Patent No. 10-1224873 titled “Method for manufacturing fermented ginger,” which improves flavor by reducing the spicy and pungent taste and aroma of ginger, and Korean Patent No. 10-0880127 titled “Fermented Ginger Drink.” "Manufacturing method" in Patent No. 10-1833345, "Manufacturing method of fermented ginger tea", which produces tea using a fermentation method using ginger and gardenia malt, in Patent No. 10-2035428, "Fermented ginger extract and its Manufacturing Method", Patent No. 10-1736809, "Method for Manufacturing Fermented Ginger Tea Composition", Patent No. 10-1866636, "Composition for Improving Blood Circulation Containing Fermented Ginger and Aged Ginger", Patent No. 10-1634232 “Fermented ginger liquid and its manufacturing method”, registered patent No. 10-1254740, “Manufacturing method of fermented ginger extract and ginger tea using the same”, registered patent No. 10-1486293, “Fermented ginger food and its manufacturing method”, registered patent No. 10-1713095, “Fermented ginger using Schizosaccharomyces pombe and its uses”, Registration Patent No. 10-2118059, “Pharmaceutical composition for preventing or treating metabolic diseases containing fermented ginger extract,” Registration Patent No. 10-1967073 "A composition for enhancing immunity containing fermented ginger extract using Bacillus subtilis and vacuum-dried red ginseng concentrate as active ingredients" is disclosed, and in Korean Patent Publication No. 10-2014-0145875, "Fermented ginger by-product is used as an active ingredient." Most of the patents are on fermented ginger products, such as "Feed additives for improving resistance to salmonella, including ". However, to date, there has been no research or related patents known on bath and foot baths using [Ginger Cake after Squeezing Ginger].

KRKR 10-0586268 10-0586268 BB KRKR 10-0540841 10-0540841 BB KRKR 10-2022-0068595 10-2022-0068595 AA KRKR 10-2004-0081248 10-2004-0081248 AA

본 발명은 상기와 같은 종래 기술의 문제점을 해결하기 위하여 안출된 것으로서, 본 발명에서 해결하고자 하는 과제는 생강 착즙 후 케이크를 주성분으로 하는 입욕제를 제공하고자 하는 것이다. 보다 구체적으로는 생강을 착즙 후 발생하는 케이크를 60~70℃에서 6~10시간 건조하고 이를 50~300메쉬로 분쇄하여 건조 생강박을 조제하고, 이에 약용식물 및 허브류를 첨가하여 제조하는 입욕제를 제공하고자 하는 것이다.The present invention was created to solve the problems of the prior art as described above, and the problem to be solved by the present invention is to provide a bath agent containing cake as the main ingredient after extracting ginger. More specifically, the cake generated after squeezing ginger is dried at 60-70℃ for 6-10 hours, crushed to 50-300 mesh to prepare dried ginger gourd, and medicinal plants and herbs are added to make a bath additive. This is what we want to provide.

상기와 같은 과제를 해결하기 위하여, 본 발명은 생강박 분말 90~95중량% 및 한약재 분말 또는 허브류 분말 5~10중량%를 포함하는 입욕제 조성물을 제공한다.In order to solve the above problems, the present invention provides a bath composition comprising 90 to 95% by weight of ginger gourd powder and 5 to 10% by weight of herbal medicine powder or herb powder.

상기 생강박 분말은 생강을 착즙한 후 발생하는 생강박을 마이크로 분쇄하여 제조되는 것이 바람직하다.The ginger gourd powder is preferably manufactured by micro-grinding the ginger gourd produced after squeezing ginger.

상기 한약재 분말은 천궁, 당귀, 어성초, 녹차잎, 건강, 진피, 계피, 상백피, 애엽 및 야관문으로 이루어지는 군으로부터 1종 이상 선택되고, 상기 허브류 분말은 페퍼민트, 로즈마리, 바질, 애플민트, 타임, 딜, 차이브, 타라곤, 오레가노, 마조람, 펜넬, 터버릭 및 넛메그로부터 1종 이상 선택되는 것이 바람직하다.The herbal medicine powder is one or more selected from the group consisting of Cheongung, Angelica, Houttuynia cordata, green tea leaves, health, dermis, cinnamon, Morus bark, leaf and night gate, and the herbal powder is peppermint, rosemary, basil, apple mint, thyme, and dill. , chives, tarragon, oregano, marjoram, fennel, turmeric and nutmeg are preferably selected from one or more types.

상기 입욕제 조성물은 항세균, 항진균, 항산화 및 소취 활성을 갖는 것이 바람직하다.The bath additive composition preferably has antibacterial, antifungal, antioxidant and deodorizing activities.

상기 입욕제는 족욕제인 것이 바람직하다.It is preferable that the bath agent is a foot bath agent.

본 발명의 생강 착즙 후 케이크를 주성분으로 하는 입욕제는 특유의 생강 향미의 제공과 함께 강력한 항균, 항산화 및 소취 활성을 나타내어 소비자 기호도가 높으며, 현재까지 별도 용도없이 폐기되고 있는 생강 착즙 후 케이크를 이용하므로 환경 보호, 자원 재활용 및 아로마 테라피 산업의 경제성 확보에 기여할 것으로 판단된다. The bath agent of the present invention, which is mainly composed of cake after ginger extraction, provides a unique ginger flavor and exhibits strong antibacterial, antioxidant and deodorizing activities, so it has a high consumer preference. It uses cake after ginger extraction, which has been discarded without any other purpose to date. It is believed that it will contribute to environmental protection, resource recycling, and securing the economic feasibility of the aromatherapy industry.

도 1은 실험에 사용된 (1) 생강 착즙 후 케이크(수분 66%), (2) 이를 60℃에서 건조한 건조 케이크, (3) 건조 케이크를 ~50메쉬로 분쇄한 분말 및 (4) 1차 분쇄한 생강박 분말을 ~300메쉬(평균 입도 20μm)로 분쇄한 분말의 사진도이다.
도 2는 1차 분쇄한 생강박 분말을 ~300메쉬(평균 입도 20μm)로 분쇄한 분말의 평균 입도 분석도이다.
도 3는 생강 착즙 후 케이크 분말의 광학현미경(위: 200배 확대사진) 사진도이다. 섬유소에 유기물이 결합된 상태임을 보여주고 있다.
도 4는 본 발명의 제조된 생강박 입욕제의 사진도이다(생강박이 포함된 1회용 부직포의 평균 무게 ~12g).
Figure 1 shows (1) cake after ginger juice (66% moisture) used in the experiment, (2) dried cake dried at 60°C, (3) powder obtained by grinding the dried cake to ~50 mesh, and (4) primary This is a photo of ground ginger gourd powder ground to ~300 mesh (average particle size 20μm).
Figure 2 is an average particle size analysis of the firstly ground ginger gourd powder to ~300 mesh (average particle size 20μm).
Figure 3 is an optical microscope photo (top: 200 times magnification) of cake powder after ginger juice. It shows that organic matter is combined with cellulose.
Figure 4 is a photograph of the ginger gourd bath agent prepared according to the present invention (average weight of disposable nonwoven fabric containing ginger gourd - 12g).

이하, 본 발명을 상세하게 설명한다.Hereinafter, the present invention will be described in detail.

본 발명의 발명자들은 유용 아미노산, 비타민, 미네랄을 다량으로 함유하면서도, 별도의 특이 용도가 없어 버려지고 있는 생강 착즙 후 케이크를 이용한 입욕제를 개발하고자, 최적의 생강 착즙 후 케이크의 건조조건 및 분쇄조건을 설정하였으며, 이후 제조된 생강박의 항균 활성, 항산화 활성 및 소취 활성을 평가한 결과, 우수한 활성이 나타남을 확인하였다. 이러한 효과는 생강박의 유용성분에 의해 나타나며, 입욕 및 족욕시에 피부에 흡수되어 피부 세정 및 탄력증진, 유해균의 사멸, 피부 보습 유지, 혈액순환 촉진 등의 직접적 건강 기여는 물론 은은한 향으로 인한 긴장완화, 정신건강에도 도움이 될 수 있음을 확인하였다.The inventors of the present invention sought to develop a bath agent using cake after ginger extraction, which contains a large amount of useful amino acids, vitamins, and minerals, but is discarded due to lack of specific use, and determined the optimal drying and grinding conditions for the cake after juice extraction. As a result of evaluating the antibacterial activity, antioxidant activity, and deodorizing activity of the manufactured ginger gourd, it was confirmed that it exhibited excellent activity. This effect is caused by the useful components of ginger gourd, which are absorbed into the skin during bathing and foot bathing, and not only contribute directly to health by cleansing the skin, improving elasticity, killing harmful bacteria, maintaining skin moisture, and promoting blood circulation, but also relieve tension due to the subtle scent. It has been confirmed that it can be helpful for relaxation and mental health.

본 발명은 생강박 분말 90~95중량% 및 한약재 분말 또는 허브류 분말 5~10중량%를 포함하는 입욕제 조성물을 제공한다.The present invention provides a bath composition comprising 90 to 95% by weight of ginger gourd powder and 5 to 10% by weight of herbal medicine powder or herb powder.

상기 생강박 분말은 생강을 착즙한 후 발생하는 생강박을 마이크로 분쇄하여 제조되는 것이 바람직하다.The ginger gourd powder is preferably manufactured by micro-grinding the ginger gourd produced after squeezing ginger.

바람직한 구체예로서, 본 발명의 생강박 분말은 생강 착즙 후 케이크를 60~70℃에서 6~10시간 건조하고, 이를 50~300메쉬로 분쇄하여 제조될 수 있다. As a preferred embodiment, the ginger gourd powder of the present invention can be prepared by extracting ginger, drying the cake at 60-70°C for 6-10 hours, and grinding it to 50-300 mesh.

상기 한약재 분말은 천궁, 당귀, 어성초, 녹차잎, 건강, 진피, 계피, 상백피, 애엽 및 야관문으로 이루어지는 군으로부터 1종 이상 선택되고, 상기 허브류 분말은 페퍼민트, 로즈마리, 바질, 애플민트, 타임, 딜, 차이브, 타라곤, 오레가노, 마조람, 펜넬, 터버릭 및 넛메그로부터 1종 이상 선택되는 것이 바람직하다.The herbal medicine powder is one or more selected from the group consisting of Cheongung, Angelica, Houttuynia cordata, green tea leaves, health, dermis, cinnamon, Morus bark, leaf and night gate, and the herbal powder is peppermint, rosemary, basil, apple mint, thyme, and dill. , chives, tarragon, oregano, marjoram, fennel, turmeric and nutmeg are preferably selected from one or more types.

상기 입욕제 조성물은 항세균, 항진균, 항산화 및 소취 활성을 갖는 것이 바람직하다.The bath additive composition preferably has antibacterial, antifungal, antioxidant and deodorizing activities.

상기 입욕제는 족욕제인 것이 바람직하다.It is preferable that the bath agent is a foot bath agent.

이하에서는 실시예를 통하여 본 발명을 더욱 상세하게 설명한다. 하기 실시예는 본 발명의 바람직한 일 구체예일 뿐이며, 본 발명의 권리범위가 하기 실시예의 범위로 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail through examples. The following example is only a preferred embodiment of the present invention, and the scope of the present invention is not limited to the scope of the following example.

[실시예][Example]

실시예 1: 생강 착즙 후 케이크 분말의 제조 Example 1: Preparation of cake powder after ginger juice

경북 안동에서 재배한 성숙한 생강 지하부를 회수하여 이물질을 제거한 후 이를 착즙기를 이용하여 착즙하였다. 이때, 생강 착즙 후 케이크는 생강 대비 약 35% 정도가 발생되었으며, 효율적인 분쇄를 위해 생강 착즙 후 케이크를 60~70℃에서 8시간 정도 건조한 이후 1차 파쇄하여 ~50 메쉬의 분말을 제조하였다. 이후, 표면적의 증대 및 빠른 물질 용해를 위해 1차 파쇄한 생강박 분말을 다시 2차 분쇄하여 ~300 메쉬의 생강박 분말을 제조하였다. 이 경우 제조박의 평균 입도는 20μm였다. 이때 사용된 생강 착즙 후 케이크와, 생강 착즙 후 케이크 분말 및 마이크로 분쇄 생강박의 사진도는 도 1에, 입도 분포 분석결과는 도 2에 나타내었다. The underground part of mature ginger grown in Andong, Gyeongsangbuk-do was recovered, foreign substances were removed, and the juice was extracted using a juicer. At this time, after juicing ginger, the cake produced about 35% of that of ginger. For efficient grinding, the cake after juicing ginger was dried at 60-70°C for about 8 hours and then first crushed to produce a powder of ~50 mesh. Afterwards, in order to increase the surface area and quickly dissolve the material, the firstly crushed ginger gourd powder was again pulverized a second time to prepare ginger gourd powder of ~300 mesh. In this case, the average particle size of the manufactured foil was 20 μm. A photograph of the cake after ginger extraction, the cake powder after ginger extraction, and the micro-ground ginger gourd used at this time is shown in Figure 1, and the particle size distribution analysis results are shown in Figure 2.

실시예 2: 생강 착즙 후 케이크 분말의 현미경 관찰 Example 2: Microscopic observation of cake powder after ginger extraction

실시예 1에서 제조된 생강 착즙 후 케이크 분말의 구조를 광학현미경(Olympus, Tokyo, JAPAN)을 이용하여 확인하였다. 도 3에 나타낸 바와 같이, 케이크 분말은 생강 섬유소에 유기물이 결합된 상태로 존재하였다. 유기물의 양을 확인하기 위해 케이크 분말을 100℃에서 10분간 열수 추출한 결과 수율은 8%를 나타내었다. 식품공전에 제시된 방법에 따라 생강 착즙후 케이크의 영양성분을 분석한 결과 조단백 4.06%, 조지방 2.0%, 조탄수화물 86.03%, 회분 4.15%, 수분 3.76%로 확인되었다. The structure of the cake powder after extracting the ginger prepared in Example 1 was confirmed using an optical microscope (Olympus, Tokyo, JAPAN). As shown in Figure 3, the cake powder existed in a state in which organic matter was bound to ginger fiber. To check the amount of organic matter, the cake powder was extracted with hot water at 100°C for 10 minutes, and the yield was 8%. As a result of analyzing the nutritional components of the cake after extracting ginger according to the method suggested in the Food Code, it was confirmed that crude protein was 4.06%, crude fat was 2.0%, crude carbohydrate was 86.03%, ash was 4.15%, and moisture was 3.76%.

실시예 3: 생강 착즙 후 케이크 추출물의 성분 분석 Example 3: Component analysis of cake extract after ginger juice

실시예 1에서 제조된 생강 착즙 후 케이크 분말의 에탄올 추출물을 조제하고 이의 유용성분을 분석하였다. 이때, 추출물은 케이크 분말 시료에 대해 10배의 에탄올(95%, 덕산, 한국)을 가하고, 실온에서 1회 추출한 후 추출액을 모아 필터링한 후, 감압 농축하여 분말로 제조하였다. 대조구로는 안동생강의 가식부 부분을 대상으로 건조분말을 조제하고 상기와 동일하게 추출물을 제조하였다. 생강 착즙 후 케이크 분말 및 생강(가식부)의 추출 수율과 이들의 유용성분 분석 결과는 표 1에 나타내었다. 이때, 총 폴리페놀 함량은 추출 검액 400μl에 50μl의 Folin-ciocalteau, 100μl의 Na2CO3 포화용액을 넣고, 실온에서 1시간 방치한 후 725nm에서 흡광도를 측정하였다. 표준시약으로는 tannic acid를 사용하였다. 총 플라보노이드 함량은 각각의 시료를 18시간 메탄올 교반 추출하고, 여과한 추출 검액 400μl에 90% diethylene glycol 4ml를 첨가하고, 다시 1N NaOH 40μl를 넣고 37℃에서 1시간 반응 후 420nm에서 흡광도를 측정하였다. 표준시약으로는 rutin을 사용하였다. 환원당은 DNS법으로, 총당은 phenol-sulfuric acid법을 이용하여 정량하였다. An ethanol extract of the cake powder was prepared after extracting the ginger prepared in Example 1, and its useful components were analyzed. At this time, the extract was prepared by adding 10 times more ethanol (95%, Deoksan, Korea) to the cake powder sample, extracting once at room temperature, collecting the extract, filtering, and concentrating under reduced pressure. As a control, dried powder was prepared from the edible part of Andong ginger, and extract was prepared in the same manner as above. The extraction yields of cake powder and ginger (edible parts) after ginger juice and their useful content analysis results are shown in Table 1. At this time, the total polyphenol content was measured by adding 50 μl of Folin-ciocalteau and 100 μl of Na 2 CO 3 saturated solution to 400 μl of the extraction sample solution, leaving it at room temperature for 1 hour, and measuring the absorbance at 725 nm. Tannic acid was used as a standard reagent. To determine the total flavonoid content, each sample was extracted with methanol stirring for 18 hours, 4ml of 90% diethylene glycol was added to 400μl of the filtered extraction solution, 40μl of 1N NaOH was added again, and the absorbance was measured at 420nm after reacting for 1 hour at 37°C. Rutin was used as a standard reagent. Reducing sugars were quantified using the DNS method, and total sugars were quantified using the phenol-sulfuric acid method.

[표 1] 생강 착즙 후 케이크 분말 및 생강분말의 에탄올 추출물의 추출효율 및 추출물들의 유용성분 분석[Table 1] Extraction efficiency of ethanol extracts of cake powder and ginger powder after ginger juice and analysis of useful components of the extracts

표 1에 나타낸 바와 같이 생강 착즙 후 케이크 분말은 1.75%의 추출효율을 보였으며, 총 폴리페놀 함량이 104.3mg/g으로 매우 높게 나타났으며, 총 플라보노이드 함량은 24.4mg/g, 총당 함량은 94.8mg/g으로 나타나, 생강박 건조분말이 생강 식용부위의 건보분말보다 총 폴리페놀 및 총 플라보노이드 함량이 가각 2.05배 및 3,34배 높게 나타났다. 따라서, 생강박이 생강 가식부 보다 유용생리활성 측면에서 강력한 활성을 나타내리라 예측되었다. As shown in Table 1, the cake powder after ginger extraction showed an extraction efficiency of 1.75%, and the total polyphenol content was very high at 104.3 mg/g, the total flavonoid content was 24.4 mg/g, and the total sugar content was 94.8. Expressed in mg/g, the total polyphenol and total flavonoid contents of dried ginger gourd powder were 2.05 times and 3.34 times higher than the dried powder of edible parts of ginger, respectively. Therefore, it was predicted that ginger gourd would exhibit stronger activity in terms of useful physiological activity than the edible part of ginger.

실시예 4: 생강 착즙 후 케이크 추출물의 항산화 활성Example 4: Antioxidant activity of cake extract after ginger juice

실시예 3에서 제조된 생강 착즙 후 케이크 분말 및 생강 가식부 분말의 에탄올 추출물을 대상으로 항산화 활성을 분석하였다. 이때, DPPH 소거능의 경우 케이크 추출물 20μl에, 99.5% 에탄올에 용해시킨 2 x 10-4M DPPH 용액 380μl를 넣고 혼합하여 37℃에서 30분 동안 반응시킨 후, 516nm에서 microplate reader(Asys Hitech, Expert96, Asys Co., Austria)를 사용하여 흡광도를 측정하였다. DPPH radical 소거능은 시료첨가구와 비첨가구의 백분율로 표시하였다. Antioxidant activity was analyzed for the ethanol extract of the cake powder and edible part powder of ginger after the ginger juice prepared in Example 3. At this time, in the case of DPPH scavenging ability, 380 μl of 2 Asys Co., Austria) was used to measure absorbance. DPPH radical scavenging ability was expressed as a percentage of the sample added and the sample not added.

ABTS 소거능의 경우 7mM ABTS(Sigma Co., USA) 5ml와 140mM potassium persulfate 88ml를 섞은 후 상온에서 16시간 빛을 차단하여 ABTS 양이온을 형성시켰으며, 이후 이 용액을 414nm에서 흡광도 값이 1.5가 되도록 에탄올로 희석하였다. 조제된 희석용액 190ml와 케이크 추출물 10ml를 혼합한 후 상온에서 6분간 반응시킨 후 734nm에서 흡광도를 측정하고, 다음의 식에 의해 ABTS radical 소거능을 계산하였다. In the case of ABTS scavenging ability, 5ml of 7mM ABTS (Sigma Co., USA) and 88ml of 140mM potassium persulfate were mixed and light was blocked for 16 hours at room temperature to form ABTS cations. This solution was then diluted with ethanol to obtain an absorbance value of 1.5 at 414nm. It was diluted with . After mixing 190 ml of the prepared diluted solution and 10 ml of cake extract, reacted at room temperature for 6 minutes, absorbance was measured at 734 nm, and ABTS radical scavenging ability was calculated using the following equation.

ABTS radical 소거능 (%) = [(C-S)/C] x 100, ABTS radical scavenging ability (%) = [(C-S)/C] x 100,

C: 용매 대조구 DMSO 첨가시의 흡광도, C: Absorbance upon addition of solvent control DMSO,

S: 시료 첨가시의 흡광도.S: Absorbance upon sample addition.

한편, nitrite 소거능 측정의 경우, 아질산염 용액(1mM)에 케이크 추출물을 가하고, 여기에 0.1N HCl을 가해 pH 1.2로 조정한 후, 37℃에서 1시간 반응시킨 후 Griess reagent(Sigma Co., USA)를 가하고 혼합하였다. 이후, 15분간 실온에서 방치 후 520nm에서 흡광도를 측정하여 잔존 nitrite 양을 측정하였다. nitrite 소거능(%)는 다음의 식에 의해 계산하였다.Meanwhile, in the case of measuring nitrite scavenging ability, cake extract was added to a nitrite solution (1mM), 0.1N HCl was added to adjust the pH to 1.2, and reacted at 37°C for 1 hour using Griess reagent (Sigma Co., USA). was added and mixed. Afterwards, it was left at room temperature for 15 minutes and the absorbance was measured at 520 nm to measure the amount of remaining nitrite. Nitrite scavenging ability (%) was calculated using the following equation.

NSA (%) = [1-(A-C)/B] x 100, NSA (%) = [1-(A-C)/B] x 100,

A: 1mM nitrite 용액에 시료를 첨가하여 1시간 반응시킨 후의 흡광도,A: Absorbance after adding sample to 1mM nitrite solution and reacting for 1 hour,

B: 1mM nitrite 용액의 흡광도, B: Absorbance of 1mM nitrite solution,

C: 생강 케이크 추출물 시료의 흡광도.C: Absorbance of ginger cake extract sample.

상기의 항산화 실험에서 대조구로는 vitamin C(Sigma Co., USA)를 사용하였으며, 용매 대조구로는 DMSO를 사용하였다. 각각의 활성 평가는 각각 3회 반복한 실험의 평균과 편차로 표시하였다. In the above antioxidant experiment, vitamin C (Sigma Co., USA) was used as a control, and DMSO was used as a solvent control. Each activity evaluation was expressed as the average and deviation of experiments repeated three times.

한편, 환원력 평가의 경우 Oyaizu 등의 방법을 변형(안선미 등, 2011. J. Life Sci. 21: 576-583)하여 측정하였다. 케이크 추출물 2.5ml에 0.2M sodium phosphate buffer(pH 6.6) 2.5ml와 10% potassium ferricyanide 2.5ml를 첨가하고, 50℃에서 20분간 반응시킨 후, 10% trichloroacetic acid 2.5ml를 첨가하여 반응을 종료하고 4000rpm에서 10분간 원심분리하여 상등액을 회수하였다. 회수한 상등액은 증류수로 2배 희석한 후, 신선하게 조제된 0.1% ferric chloride 용액과 5:1(v/v) 비율로 혼합하고 700nm에서 흡광도를 측정하여 평가하였다. Meanwhile, in the case of reducing power evaluation, the method of Oyaizu et al. was modified (Ahn Seon-mi et al., 2011. J. Life Sci. 21: 576-583). Add 2.5 ml of 0.2M sodium phosphate buffer (pH 6.6) and 2.5 ml of 10% potassium ferricyanide to 2.5 ml of cake extract, react at 50°C for 20 minutes, add 2.5 ml of 10% trichloroacetic acid to terminate the reaction, and rotate at 4000 rpm. The supernatant was recovered by centrifugation for 10 minutes. The recovered supernatant was diluted two-fold with distilled water, mixed with freshly prepared 0.1% ferric chloride solution in a 5:1 (v/v) ratio, and evaluated by measuring absorbance at 700 nm.

[표 2] 생강 착즙 후 케이크 분말 및 생강 가식부 분말의 에탄올 추출물의 항산화 활성[Table 2] Antioxidant activity of ethanol extract of cake powder and ginger edible part powder after ginger extraction

그 결과, 표 2에 나타낸 바와 같이 생강 착즙후 케이크 분말은 생강 가식부 분말보다 매우 우수한 DPPH 음이온 소거능, ABTS 양이온 소거능, 환원력 및 nitrite 소거능을 나타냄을 확인하였다. 따라서, 생강 착즙 후 케이크 분말은 생강 가식부 분말보다도 항노화, 산화적 스트레스 및 발암억제에 기여할 것으로 판단되었다.As a result, as shown in Table 2, it was confirmed that the cake powder after extracting ginger showed very superior DPPH anion scavenging ability, ABTS cation scavenging ability, reducing power, and nitrite scavenging ability than ginger edible part powder. Therefore, it was determined that cake powder after ginger extraction would contribute to anti-aging, oxidative stress, and carcinogenesis inhibition more than ginger edible part powder.

실시예 5: 생강 착즙후 케이크 추출물의 항세균 및 항진균 활성Example 5: Antibacterial and antifungal activity of cake extract after ginger juice

실시예 3에서 제조된 생강 착즙후 케이크 분말 및 생강 가식부 분말의 에탄올 추출물을 대상으로 항균 활성을 평가하였으며, 그 결과를 표 3에 나타내었다. 항균 활성 평가에 사용된 균주로는, 그람 음성균으로서 Escherichia coli KCTC 1682, Proteus vulgaris KCTC 2433, Pseudomonas aeruginosa KACC 10186, Salmonella typhimurium KCTC 1926을 사용하였고, 그람 양성균으로는 Staphylococcus aureus KCTC 1916, Staphylococcus epidermidis ATCC 12228, Listeria monocytogenes KACC 10550, Bacillus subtilis KCTC 1924를 사용하였다. 한편, 항진균 활성 평가를 위해서는 Saccharomyces cerevisiae IF0 0233 및 캔디다증 진균감염증 원인균 Candida albicans KCTC 1940을 사용하였다. The antibacterial activity of the ethanol extract of the cake powder and edible part of ginger powder prepared in Example 3 was evaluated, and the results are shown in Table 3. The strains used to evaluate antibacterial activity were Gram-negative bacteria: Escherichia coli KCTC 1682, Proteus vulgaris KCTC 2433, Pseudomonas aeruginosa KACC 10186, and Salmonella typhimurium KCTC 1926, and Gram-positive bacteria were Staphylococcus aureus KCTC 1916 and Staphylococcus epidermidis ATCC 1222. 8, Listeria monocytogenes KACC 10550 and Bacillus subtilis KCTC 1924 were used. Meanwhile, to evaluate antifungal activity , Saccharomyces cerevisiae IF0 0233 and Candida albicans KCTC 1940, the causative agent of candidiasis fungal infection, were used.

먼저, 항세균 활성 평가의 경우, Nutrient broth(Difco Co., USA)에 각각의 세균을 접종하여 37℃에서 24시간 동안 배양한 후, 각 균주를 O.D.600 0.1로 조정하여 Nutrient agar(Difco Co., USA) 배지를 포함하는 멸균 petri dish(90mm, 녹십자, 한국)에 100μl씩 도말하고, 각각의 시료 5μl를 멸균 disc-paper(지름 6.5mm, Whatsman No. 2)에 가하여, 37℃에서 24시간 동안 배양하였으며, 진균의 경우에는, Sabouraud dextrose(Difco Co. USA)를 이용하여 동일한 방법으로 30℃에서 24시간 동안 배양 후, 생육저지환의 크기를 측정하여 항균활성을 평가하였다. 대조구로는 항세균제인 엠피실린(ampicillin)과 항진균제인 마이코나졸(miconazole, Sigma Co., USA)을 각각 1μg/disc 농도로 사용하였으며, 생육저지환의 크기는 육안으로 생육이 나타나지 않는 부분의 지름을 mm 단위로 측정하였고, 3회 이상 평가 후 대표 결과로 나타내었다.First, in the case of antibacterial activity evaluation, each bacteria was inoculated into Nutrient broth (Difco Co., USA) and cultured at 37°C for 24 hours, then each strain was adjusted to OD 600 0.1 and incubated on Nutrient agar (Difco Co.). , USA), 100 μl of each sample was spread on a sterilized petri dish (90 mm, Green Cross, Korea) containing medium, and 5 μl of each sample was added to sterile disc-paper (diameter 6.5 mm, Whatsman No. 2) and incubated at 37°C for 24 hours. In the case of fungi, the antibacterial activity was evaluated by measuring the size of growth-inhibiting rings after culturing at 30°C for 24 hours using the same method using Sabouraud dextrose (Difco Co. USA). As a control, the antibacterial agent ampicillin and the antifungal agent miconazole (Sigma Co., USA) were used at a concentration of 1μg/disc each, and the size of the growth-inhibiting ring was calculated from the diameter of the area where growth was not visible to the naked eye. Measurements were made in mm and presented as representative results after evaluation three or more times.

[표 3] 생강 착즙 후 케이크 분말 및 생강 가식부 분말의 에탄올 추출물의 항균 활성[Table 3] Antibacterial activity of ethanol extract of cake powder and ginger edible part powder after ginger extraction

그 결과, 표 3에 나타낸 바와 같이, 임상에서 항세균제로 사용되고 있는 ampicillin 은 1μg/disc에서도 광범위한 항균 활성을 나타내었으며, Pseudomonas aeruginosaSalmonella typhimurium에 대해서는 상대적으로 약한 생육억제환(9~12mm)을 나타내었다. 임상에서 항진균제로 사용되고 있는 miconazole 은 1μg/disc에서도 Saccharomyces cerevisiaeCandida albicans의 생육을 저해하였다. 한편 생강 착즙 후 케이크를 건조 분쇄한 생강박 분말의 추출물은 생강 추출물보다 강력하게 항세균 활성을 나타내었으며, 특히 진균인 Saccharomyces cerevisiaeCandida albicans의 생육을 우수하게 저해하였다. As a result, as shown in Table 3, ampicillin, which is used as an antibacterial agent in clinical practice, showed broad antibacterial activity even at 1 μg/disc, and showed relatively weak growth inhibitory rings (9 to 12 mm) against Pseudomonas aeruginosa and Salmonella typhimurium. It was. Miconazole, which is used clinically as an antifungal agent, inhibited the growth of Saccharomyces cerevisiae and Candida albicans even at 1 μg/disc. Meanwhile, the extract of ginger gourd powder obtained by drying and pulverizing the cake after squeezing ginger showed stronger antibacterial activity than ginger extract, and especially inhibited the growth of the fungi Saccharomyces cerevisiae and Candida albicans .

실시예 6: 생강 착즙 후 케이크를 건조, 분쇄하여 제조한 족욕제의 소취 활성 Example 6: Deodorizing activity of a foot bath prepared by drying and pulverizing the cake after extracting ginger

실시예 1에서 제조된 생강 착즙 후 케이크 분말을 부직포에 12g 넣어 제조한 생강박 족욕제를 2리터의 온수(~40℃)에 첨가하고, 족욕을 실시하였다. 이때 족욕시 물의 높이는 족삼리(복숭아뼈 부위)가 잠기도록 하였으며, 10분간 실시하였다. 실험평가자는 식품영양학과 전문연구원 5명을 대상으로 7점 척도법으로 진행하였다. 대조구로는 무첨가 온수와 페퍼민트 1%를 첨가한 온수를 사용하였으며, 생강박에 대한 거부감이 있는 경우를 감안하여, 생강 착즙 후 케이크 분말을 부직포에 10g, 계피 2g을 넣어 제조한 생강박 족욕제를 사용하였다. 소취 만족도 및 전체적 선호도에 대한 관능평가 결과는 표 4에 나타내었다. The ginger gourd foot bath prepared by putting 12 g of cake powder into a non-woven fabric after extracting the ginger prepared in Example 1 was added to 2 liters of warm water (~40°C), and a foot bath was performed. At this time, the water level during the foot bath was set to submerge the sole (peach bone area), and the bath was performed for 10 minutes. The experiment was evaluated using a 7-point scale using five professional researchers from the Department of Food and Nutrition. As a control, hot water without additives and hot water with 1% peppermint added were used. Considering that there is aversion to ginger gourd, a ginger gourd foot bath prepared by adding 10 g of cake powder and 2 g of cinnamon to a non-woven fabric after extracting ginger was used. used. The sensory evaluation results for deodorization satisfaction and overall preference are shown in Table 4.

[표 4] 생강박 족욕제의 소취 활성 및 선호도 검사[Table 4] Deodorizing activity and preference test of ginger gourd foot bath

그 결과 생강박 족욕제는 우수한 생강박 향미로 인한 스트레스 완화와 함께 발냄새 제거에 효과가 있음을 확인하였다. 특히 생강박에 대한 선호도가 낮은 경우에 계피를 일부 첨가한 경우 보다 높은 소취능과 전체적인 선호도가 나타남을 확인하였다. 생강박에 첨가하여 우수한 소취능과 선호도가 나타나는 경우는 계피, 당귀, 페퍼민트, 어성초, 야관문으로 확인되었으며, 생강박 90~95% 중량에 추가적으로 당귀, 어성초, 야관문, 계피 등의 한방약재를 각각 5~10% 중량비로 포함하거나, 생강박 90~95% 중량에 페퍼민트, 로즈마리 등의 허브류를 각각 5~10% 중량비로 첨가하는 경우 우수하였다. As a result, it was confirmed that the ginger gourd foot bath is effective in relieving stress and removing foot odor due to the excellent ginger gourd flavor. In particular, it was confirmed that when the preference for ginger gourd was low, higher deodorizing ability and overall preference were shown when some cinnamon was added. Cases showing excellent deodorizing ability and preference when added to ginger gourd were confirmed to be cinnamon, angelica root, peppermint, Houttuynia cordata, and Houttuynia cordata, and oriental medicinal herbs such as angelica root, Houttuynia cordata, Houttuynia cordata, and cinnamon were added to 90-95% weight of ginger gourd, respectively. It was excellent when included at a weight ratio of ~10%, or when herbs such as peppermint and rosemary were added at a weight ratio of 5-10% to 90-95% of ginger gourd.

[연구개발과제][R&D tasks]

- 과제고유번호: 2022-0231- Assignment identification number: 2022-0231

- 주관부처명: 안동시농업기술센터- Name of department in charge: Andong City Agricultural Technology Center

- 연구관리전문기관 : 안동대학교 산학협력단- Research management agency: Andong University Industry-Academic Cooperation Foundation

- 연구사업명: 2022 현장애로기술개발사업- Research project name: 2022 Field Difficulty Technology Development Project

- 연구과제명: 생강박, 생강박 첨가 생강청 관련 시제품의 영양분석, 효능평가 연구용역- Research project name: Nutrient analysis and efficacy evaluation research service for prototype products related to ginger gourd and ginger extract added with ginger gourd

- 기여율: 100%- Contribution rate: 100%

- 연구기간: 2022. 6. 1 ~ 2022. 10. 30- Research period: 2022. 6. 1 ~ 2022. 10. 30

- 주관기관: ㈜따비온- Host organization: Tabion Co., Ltd.

- 위탁연구기관 : 안동대학교 산학협력단- Entrusted research institute: Andong University Industry-Academic Cooperation Foundation

- 실제 연구수행기관 : 안동대학교 산학협력단 - Actual research institution: Andong University Industry-Academic Cooperation Foundation

Claims (5)

생강박 분말 90~95중량% 및 한약재 분말 또는 허브류 분말 5~10중량%를 포함하는 입욕제 조성물.A bath additive composition containing 90 to 95% by weight of ginger gourd powder and 5 to 10% by weight of herbal medicine powder or herb powder. 제 1항에 있어서, 상기 생강박 분말은 생강을 착즙한 후 발생하는 생강박을 마이크로 분쇄하여 제조되는 것을 특징으로 하는 입욕제 조성물.The bath additive composition according to claim 1, wherein the ginger gourd powder is manufactured by micro-pulverizing the ginger gourd produced after squeezing ginger. 제 1항에 있어서, 상기 한약재 분말은 천궁, 당귀, 어성초, 녹차잎, 건강, 진피, 계피, 상백피, 애엽 및 야관문으로 이루어지는 군으로부터 1종 이상 선택되고, 상기 허브류 분말은 페퍼민트, 로즈마리, 바질, 애플민트, 타임, 딜, 차이브, 타라곤, 오레가노, 마조람, 펜넬, 터버릭 및 넛메그로부터 1종 이상 선택되는 것을 특징으로 하는 입욕제 조성물.The method of claim 1, wherein the herbal medicine powder is selected from the group consisting of Cheongung, angelica root, Houttuynia cordata, green tea leaves, health, dermis, cinnamon, Morus chinensis, Aleaf and Yagwanmun, and the herbal powders include peppermint, rosemary, basil, A bath composition comprising one or more selected from apple mint, thyme, dill, chives, tarragon, oregano, marjoram, fennel, turmeric and nutmeg. 제 1항에 있어서, 상기 입욕제 조성물은 항세균, 항진균, 항산화 및 소취 활성을 갖는 것을 특징으로 하는 입욕제 조성물.The bath additive composition according to claim 1, wherein the bath additive composition has antibacterial, antifungal, antioxidant and deodorizing activities. 제 1항에 있어서, 상기 입욕제는 족욕제인 것을 특징으로 하는 입욕제 조성물.The bath additive composition according to claim 1, wherein the bath additive is a foot bath agent.
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040081248A (en) 2003-03-14 2004-09-21 (주)에코텍 Preparation method of functional bath material containing Curcuma longa L.
KR100540841B1 (en) 2004-07-09 2006-01-10 김경수 The wohle body bathing manufacture method that use milled wormwood
KR100586268B1 (en) 2004-07-07 2006-06-08 유인권 Method of herb footbath on the preparation
KR20220068595A (en) 2020-11-19 2022-05-26 주식회사 팜스킨 Functional bath cleanser composition comprising plant powder

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040081248A (en) 2003-03-14 2004-09-21 (주)에코텍 Preparation method of functional bath material containing Curcuma longa L.
KR100586268B1 (en) 2004-07-07 2006-06-08 유인권 Method of herb footbath on the preparation
KR100540841B1 (en) 2004-07-09 2006-01-10 김경수 The wohle body bathing manufacture method that use milled wormwood
KR20220068595A (en) 2020-11-19 2022-05-26 주식회사 팜스킨 Functional bath cleanser composition comprising plant powder

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