KR20240051457A - Gel filter composition for water treatment and method of producing gel filter - Google Patents
Gel filter composition for water treatment and method of producing gel filter Download PDFInfo
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- 239000000203 mixture Substances 0.000 title claims abstract description 56
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 48
- 238000000034 method Methods 0.000 title abstract description 11
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 45
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 30
- 229920002472 Starch Polymers 0.000 claims abstract description 25
- 239000008107 starch Substances 0.000 claims abstract description 25
- 235000019698 starch Nutrition 0.000 claims abstract description 25
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 23
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 23
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 23
- 239000011718 vitamin C Substances 0.000 claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 claims abstract description 19
- 235000002639 sodium chloride Nutrition 0.000 claims abstract description 17
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 16
- 239000011780 sodium chloride Substances 0.000 claims abstract description 16
- 102000008186 Collagen Human genes 0.000 claims abstract description 15
- 108010035532 Collagen Proteins 0.000 claims abstract description 15
- 229920001436 collagen Polymers 0.000 claims abstract description 15
- 235000011187 glycerol Nutrition 0.000 claims abstract description 15
- 229920002148 Gellan gum Polymers 0.000 claims abstract description 14
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims abstract description 14
- 239000000216 gellan gum Substances 0.000 claims abstract description 14
- 235000010492 gellan gum Nutrition 0.000 claims abstract description 14
- 239000008101 lactose Substances 0.000 claims abstract description 14
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 11
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 11
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 11
- 229920002261 Corn starch Polymers 0.000 claims description 21
- 239000008120 corn starch Substances 0.000 claims description 21
- 239000002245 particle Substances 0.000 claims description 15
- 238000007710 freezing Methods 0.000 claims description 8
- 230000008014 freezing Effects 0.000 claims description 8
- -1 maltotextrin Chemical compound 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000011874 heated mixture Substances 0.000 claims description 5
- 239000006193 liquid solution Substances 0.000 claims description 4
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 3
- 238000002845 discoloration Methods 0.000 abstract description 5
- 230000003020 moisturizing effect Effects 0.000 abstract description 4
- 229910052801 chlorine Inorganic materials 0.000 description 17
- 239000000460 chlorine Substances 0.000 description 17
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 16
- 230000000694 effects Effects 0.000 description 15
- 210000003491 skin Anatomy 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 13
- 239000004615 ingredient Substances 0.000 description 12
- 239000008399 tap water Substances 0.000 description 8
- 235000020679 tap water Nutrition 0.000 description 8
- 238000009472 formulation Methods 0.000 description 6
- 238000001914 filtration Methods 0.000 description 5
- 239000004480 active ingredient Substances 0.000 description 4
- 230000003796 beauty Effects 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000032683 aging Effects 0.000 description 3
- 230000003110 anti-inflammatory effect Effects 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 235000015097 nutrients Nutrition 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 206010012438 Dermatitis atopic Diseases 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 201000008937 atopic dermatitis Diseases 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 235000020188 drinking water Nutrition 0.000 description 2
- 239000003651 drinking water Substances 0.000 description 2
- 238000001879 gelation Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- 206010027627 Miliaria Diseases 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000004347 all-trans-retinol derivatives Chemical class 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 229920003086 cellulose ether Polymers 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001804 chlorine Chemical class 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 238000004299 exfoliation Methods 0.000 description 1
- 239000000576 food coloring agent Substances 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000012669 liquid formulation Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011860 particles by size Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000037307 sensitive skin Effects 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 210000004927 skin cell Anatomy 0.000 description 1
- 230000036620 skin dryness Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D39/00—Filtering material for liquid or gaseous fluids
- B01D39/14—Other self-supporting filtering material ; Other filtering material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2239/00—Aspects relating to filtering material for liquid or gaseous fluids
- B01D2239/10—Filtering material manufacturing
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
본 발명은, 비타민 C, 글리세린, 젤란검, 콜라겐, 말토덱스트린, 락토오즈, 전분 및 씨솔트(Sea salt)를 포함하는 수처리용 겔필터용 조성물에 관한 것이다.
본 발명의 의하면, 필터 조성물의 안정성이 향상되어 사용수명이 증가된 수처리용 겔필터용 조성물을 제공할 수 있으며, 필터 성분의 변화를 방지하여 오랜 기간동안 변색되지 않고, 필터 조직의 안정성을 향상시켜 사용 후 보습 효과를 향상시킨 겔필터 제조방법을 제공할 수 있다.The present invention relates to a composition for a gel filter for water treatment containing vitamin C, glycerin, gellan gum, collagen, maltodextrin, lactose, starch, and sea salt.
According to the present invention, it is possible to provide a composition for a water treatment gel filter with an increased service life by improving the stability of the filter composition, prevents changes in filter components, prevents discoloration over a long period of time, and improves the stability of the filter structure. A method for manufacturing a gel filter with improved moisturizing effect after use can be provided.
Description
본 발명은 수처리용 겔필터 조성물 및 겔필터 제조방법에 관한 것으로, 보다 상세하게는 연수기, 샤워기 등에 사용되는 수처리용 겔필터 조성물 및 겔필터를 제조하는 방법에 관한 것이다.The present invention relates to a gel filter composition for water treatment and a method for manufacturing a gel filter, and more specifically, to a gel filter composition for water treatment and a method for manufacturing a gel filter used in water softeners, showers, etc.
수돗물 등 식수를 살균 처리할 때 가장 흔하게 쓰는 방법은 염소(chlorine) 성분을 섞는 것이다. 미국을 포함한 여러 나라가 수돗물을 정수할 때 이런 염소 소독 과정을 거치며, 우리나라도 예외는 아니다. 그런데 수돗물에 염소를 넣으면 암을 유발할 수도 있는 독성 부산물이 다량 생성된다는 연구 결과가 나왔다.The most commonly used method to sterilize drinking water such as tap water is to mix it with chlorine. Many countries, including the United States, go through this chlorine disinfection process when purifying tap water, and our country is no exception. However, research has shown that adding chlorine to tap water produces large amounts of toxic byproducts that can cause cancer.
또한 염소는 휘발성이 강해서 담아 주기만 해도 날아가는데 24시간 정도면 83%, 48시간이면 97.6% 정도가 제거된다고 하니 미리 물을 받아 놓았다가 일정시간이 경과한 후 냉장보관한 후 마시면 냄새가 나지 않는다. 정수기를 사용하는 이유는 염소제거 목적이라기 보다 수돗물에 섞여오는 각종 이물질을 제거해 보다 깨끗한 물을 마시기 위해서이다. 수돗물 자체가 문제가 아니라 거쳐오는 배관과 저수조가 문제가 될 수 있다.In addition, chlorine is highly volatile and flies away just by putting it in it. It is said that 83% of it is removed in 24 hours and 97.6% in 48 hours, so if you fill it with water in advance, refrigerate it after a certain period of time, and drink it, there will be no smell. The reason for using a water purifier is not to remove chlorine, but to drink cleaner water by removing various foreign substances mixed in tap water. It may not be the tap water itself that is the problem, but the pipes and water storage tank that it passes through.
마시는 물은 정수기를 사용하거나 끓여 먹는 방법으로 염소를 제거해 사용할 수 있지만 생활수로 사용하는 물의 경우, 아토피피부염 전문가들은 수돗물로 샤워나 목욕을 하면 아토피피부염이 악화될 수 있다고 지적하고 있다. 특히 따뜻한 온수는 피부 모공을 넓혀 샤워를 하는 동안 민감한 피부 속으로 잔류염소가 흡수될 수 있고 이로 인해 피부건조증, 땀띠, 가려움 등이 생길 수 있다.Drinking water can be used by removing chlorine by using a water purifier or boiling it, but in the case of water used as household water, atopic dermatitis experts point out that showering or bathing with tap water can worsen atopic dermatitis. In particular, warm water expands skin pores, which can cause residual chlorine to be absorbed into sensitive skin while showering, which can cause skin dryness, heat rash, and itching.
이에 따라, 연수기, 샤워기, 비데, 씽크대용 수도 직결형 수전, 변기, 세탁기, 가습기, 바디샤워기, 원풀형 욕조, 스파기능이 내장된 욕조 등과 같은 수처리 제품에는 각종 수처리용 필터가 장착되어 사용된다.Accordingly, water treatment products such as water softeners, showers, bidets, direct sink faucets, toilets, washing machines, humidifiers, body showers, round-pool bathtubs, bathtubs with a built-in spa function, etc. are equipped with various water treatment filters.
하지만, 이와 같은 종래의 수처리용 필터는 잔류염소 제거 효율이 상대적으로 저하되고, 그 사용수명이 매우 짧은 단점이 있다.However, such conventional water treatment filters have the disadvantage that the residual chlorine removal efficiency is relatively low and their service life is very short.
한편, 미용에 대한 관심이 높아지면서 수돗물 내 잔류 염소 및 각종 불순물 제거와 함께, 피부 미용 성분과 향을 부여한 수처리 필터의 사용이 증가하고 있다. 일반적으로 수처리 필터는 필터 케이스와 비타민C, 향료, 미용 성분 등의 유효 성분을 포함하여 물에 용해되면서 유효 성분을 방출하는 여과재로 구성된다. 상기 여과재는 고체 덩어리, 분말, 과립, 겔, 액상 등의 제형일 수 있다.Meanwhile, as interest in beauty increases, the use of water treatment filters that remove residual chlorine and various impurities in tap water and add skin beauty ingredients and fragrances is increasing. In general, a water treatment filter consists of a filter case and a filter material that contains active ingredients such as vitamin C, fragrance, and beauty ingredients and releases the active ingredients when dissolved in water. The filter medium may be in the form of solid lump, powder, granule, gel, liquid, etc.
한편, 분말, 과립, 액상의 제형을 가지는 여과재는 수돗물에 쉽게 용해되면서 단 시간 내에 소진됨에 따라, 잔류 염소 제거, 유해 물질 제거 및 피부 미용 효과가 일시적이며, 사용 수명이 짧은 문제가 있었다.Meanwhile, filter media with powder, granule, and liquid formulations are easily dissolved in tap water and are used up within a short period of time, so the removal of residual chlorine, removal of harmful substances, and skin beautification effects are temporary, and the service life is short.
이러한 문제를 해결하기 위해, 적정한 점도를 갖는 겔 상태의 여과재의 사용이 증가되고 있다. 일례로, 대한민국 등록특허 제10-1069579호에서는 덱스트린, 향, 물, 수용성 셀룰로오스 에테르, 비타민 C 또는 비타민 C의 유도체 및 식용색소의 혼합물을 폴리프로필렌 또는 폴리에틸렌의 용기에 채운 형태의 샤워기 겔 필터에 대해 개시하고 있다. 그러나, 종래의 겔 상태의 여과재는 물에 용해되는 과정에서 덩어리로 분리되어 용해되며, 적정한 수준의 용해 속도를 갖지 못하고, 여과재 내의 유효 성분을 일시에 방출하여 유효 성분에 의한 잔류 염소 제거, 유해 물질 제거 및 피부 미용 효과의 지속성이 낮은 문제가 있었다.To solve this problem, the use of gel-like filter media with appropriate viscosity is increasing. For example, Republic of Korea Patent No. 10-1069579 describes a shower gel filter filled with a mixture of dextrin, fragrance, water, water-soluble cellulose ether, vitamin C or a derivative of vitamin C, and food coloring in a polypropylene or polyethylene container. It is starting. However, the conventional gel-like filter medium separates into lumps and dissolves during the process of dissolving in water, does not have an appropriate level of dissolution speed, and releases the active ingredients in the filter medium at once, removing residual chlorine by the active ingredients and removing harmful substances. There was a problem of low removal and sustainability of skin beauty effects.
본 발명은 상기와 같은 문제점을 해결하기 위하여 안출된 것으로, 필터 조성물의 안정성을 향상시켜 사용수명을 증가시킨 수처리용 겔필터용 조성물을 제공하는데 그 목적이 있다.The present invention was developed to solve the above problems, and its purpose is to provide a composition for a gel filter for water treatment that improves the stability of the filter composition and increases its service life.
본 발명의 다른 목적은 필터 성분의 변화를 완화하여 피부에의 영양성분을 오래 지속시키고, 오랜 기간동안 변색되지 않도록 하는 겔필터 제조방법을 제공하는 것이다.Another object of the present invention is to provide a method for manufacturing a gel filter that alleviates changes in filter components to maintain nutrients in the skin for a long time and prevent discoloration over a long period of time.
본 발명의 또 다른 목적은 필터 조직의 안정성을 향상시켜 사용 후 보습 효과를 향상시킨 겔필터 제조방법을 제공하는 것이다.Another object of the present invention is to provide a method for manufacturing a gel filter that improves the moisturizing effect after use by improving the stability of the filter structure.
본 발명은 상기의 목적을 위하여, 비타민 C, 글리세린, 젤란검, 콜라겐, 말토덱스트린, 락토오즈, 전분 및 씨솔트(Sea salt)를 포함하는 수처리용 겔필터용 조성물을 제공한다.For the above purpose, the present invention provides a composition for a gel filter for water treatment containing vitamin C, glycerin, gellan gum, collagen, maltodextrin, lactose, starch, and sea salt.
또한, 상기 조성물은 비타민 C 35 내지 50중량%, 글리세린 5 내지 12 중량%, 젤란검 0.1 내지 1 중량%, 콜라겐 0.5 내지 2 중량%, 말토덱스트린 5 내지 10 중량%, 락토오즈 10 내지 15 중량%, 전분 10 내지 15 중량% 및 씨솔트(Sea salt) 5 내지 12 중량%를 포함하는 것을 특징으로 한다.In addition, the composition contains 35 to 50% by weight of vitamin C, 5 to 12% by weight of glycerin, 0.1 to 1% by weight of gellan gum, 0.5 to 2% by weight of collagen, 5 to 10% by weight of maltodextrin, and 10 to 15% by weight of lactose. , It is characterized in that it contains 10 to 15% by weight of starch and 5 to 12% by weight of sea salt.
본 발명은 상기의 목적을 위하여, (a) 비타민 C, 글리세린, 젤란검, 콜라겐, 말토텍스트린, 락토오즈, 씨솔트를 섞은 혼합물을 8 내지 10시간 동안 10℃이하의 저온에서 숙성하는 단계; (b) 상기 (a)단계의 숙성된 혼합물을 70 내지 75℃의 온도에서 3 내지 4시간 동안 가열하는 단계; (c) 상기 (b)단계의 가열된 혼합물에 10 내지 15중량% 함량의 전분(corn starch)을 7번에 거쳐 혼입하는 단계; 및 (d) 상기 (c)단계의 혼합물을 급속 냉동하여 액체 상태의 용액을 겔 타입으로 굳히는 단계를 포함하는 수처리용 겔필터 제조방법을 제공한다.For the above purpose, the present invention includes the steps of (a) maturing a mixture of vitamin C, glycerin, gellan gum, collagen, maltotextrin, lactose, and sea salt at a low temperature of 10°C or lower for 8 to 10 hours; (b) heating the aged mixture of step (a) at a temperature of 70 to 75°C for 3 to 4 hours; (c) mixing 10 to 15% by weight of starch into the heated mixture of step (b) in seven steps; and (d) rapidly freezing the mixture of step (c) to harden the liquid solution into a gel type.
또한, 상기 (a)단계는 비타민 C 35 내지 50중량%, 글리세린 5 내지 12 중량%, 젤란검 0.1 내지 1 중량%, 콜라겐 0.5 내지 2 중량%, 말토덱스트린 5 내지 10 중량%, 락토오즈 10 내지 15 중량% 및 씨솔트(Sea salt) 5 내지 12 중량%를 섞은 혼합물을 8 내지 10시간 동안 10℃이하의 저온에서 숙성하는 단계인 것을 특징으로 한다.In addition, step (a) includes 35 to 50% by weight of vitamin C, 5 to 12% by weight of glycerin, 0.1 to 1% by weight of gellan gum, 0.5 to 2% by weight of collagen, 5 to 10% by weight of maltodextrin, and 10 to 10% by weight of lactose. The process is characterized in that the mixture of 15% by weight and 5 to 12% by weight of sea salt is aged at a low temperature of 10° C. or lower for 8 to 10 hours.
또한, 상기 (c)단계에서 가열된 혼합물에 전체 조성물 대비 10 내지 15중량% 함량의 옥수수 전분(corn starch)을, 옥수수 전분 총중량 대비 10중량%, 10중량%, 15중량%, 25중량%, 20중량%, 15중량%, 5중량%의 비율로 순차적으로 혼입하는 것을 특징으로 한다.In addition, corn starch in an amount of 10 to 15% by weight based on the total composition was added to the mixture heated in step (c), and 10% by weight, 10% by weight, 15% by weight, 25% by weight, based on the total weight of corn starch, It is characterized by sequential mixing in proportions of 20% by weight, 15% by weight, and 5% by weight.
또한, 상기 (c)단계에서 옥수수 전분(corn starch)은 7개의 입자 크기별로 구분하여 옥수수 전분 총중량 대비 17~20㎛를 10중량%, 15~18㎛를 10중량%, 13~16㎛를 15중량%, 11~14㎛를 25중량%, 9~12㎛를 20중량%, 7~10㎛를 15중량%, 5~8㎛를 5중량%의 비율로 순차적으로 혼입하는 것을 특징으로 한다.In addition, in step (c), corn starch was divided into 7 particle sizes: 17 to 20㎛ was 10% by weight, 15 to 18㎛ was 10% by weight, and 13 to 16㎛ was 15% by weight, compared to the total weight of corn starch. Weight percent, 11-14㎛ is sequentially mixed at 25% by weight, 9-12㎛ at 20% by weight, 7-10㎛ at 15% by weight, and 5-8㎛ at 5% by weight.
또한, 상기 (b)단계는 상대습도 0 내지 5%를 유지하는 것을 특징으로 한다.In addition, step (b) is characterized by maintaining the relative humidity at 0 to 5%.
또한, 상기 (d)단계에서 -60 내지 -50℃의 온도에서 급속냉동하는 것을 특징으로 한다.Additionally, in step (d), rapid freezing is performed at a temperature of -60 to -50°C.
본 발명의 의하면, 필터 조성물의 안정성을 향상시켜 사용수명을 증가시킨 겔필터용 조성물을 제공할 수 있으며, 필터 성분의 변화를 방지하여 피부에의 영양성분을 오래 지속시키고, 오랜 기간동안 변색되지 않고, 필터 조직의 안정성을 향상시켜 사용 후 보습 효과를 향상시킨 겔필터 제조방법을 제공할 수 있다.According to the present invention, it is possible to provide a composition for a gel filter that increases the service life by improving the stability of the filter composition, prevents changes in the filter components, maintains nutrients in the skin for a long time, and does not discolor for a long period of time. , it is possible to provide a gel filter manufacturing method that improves the moisturizing effect after use by improving the stability of the filter structure.
도 1은 본 발명의 실시예 1 및 비교예의 겔필터의 색변화를 비교한 사진 이미지.Figure 1 is a photographic image comparing the color change of the gel filters of Example 1 and Comparative Example of the present invention.
본 발명은, 비타민 C, 글리세린, 젤란검, 콜라겐, 말토덱스트린, 락토오즈, 전분 및 씨솔트(Sea salt)를 포함하는 수처리용 겔필터용 조성물에 관한 것이다.The present invention relates to a composition for a gel filter for water treatment containing vitamin C, glycerin, gellan gum, collagen, maltodextrin, lactose, starch, and sea salt.
이하, 본 발명을 첨부한 도면을 참조하여 상세히 설명한다.Hereinafter, the present invention will be described in detail with reference to the accompanying drawings.
본 발명의 일실시예에 따른 비타민 C는, 잔류염소를 제거하는 효과와 피부노화를 예방하는 효과를 가지고 있다. 조성물 전체 중량 대비 35 내지 50중량%의 범위로 포함하는 것이 바람직한데, 35중량% 미만의 함량으로 포함되는 경우 물에 녹아 필터링 될 때 양이 부족하여 잔류염소 제거 효과가 없으므로 바람직하지 못하며, 50중량%를 초과하는 경우 물에 용해되는 속도가 너무 빨라지고, pH가 너무 높아져서 피부에 부담이 갈 수 있으므로 바람직하지 못하다.Vitamin C according to one embodiment of the present invention has the effect of removing residual chlorine and preventing skin aging. It is preferable to include it in the range of 35 to 50% by weight based on the total weight of the composition. However, if it is included in an amount of less than 35% by weight, it is undesirable because the amount is insufficient to remove residual chlorine when dissolved in water and filtered. If it exceeds %, it is undesirable because the dissolution rate in water becomes too fast and the pH becomes too high, which may put a burden on the skin.
본 발명의 일실시예에 따른 글리세린은 피부에 보습 효과를 주어 조기에 수분이 손실되는 것을 방지하는 효과를 가지고 있다. 조성물 전체 중량 대비 5 내지 12중량%의 범위로 포함하는 것이 바람직한데, 5중량% 미만의 함량으로 포함되는 경우 효과가 미미하게 되어 바람직하지 못하며, 12중량%를 초과하는 경우 다른 성분들의 함량이 상대적으로 줄게 되어 염소제거 필터링 효과가 충분하지 않으므로 바람직하지 못하다. Glycerin according to one embodiment of the present invention has a moisturizing effect on the skin and prevents premature moisture loss. It is preferable to include it in the range of 5 to 12% by weight based on the total weight of the composition. However, if it is included in an amount of less than 5% by weight, the effect is minimal and thus undesirable, and if it exceeds 12% by weight, the content of other components is relative. This is undesirable because the chlorine removal filtering effect is not sufficient.
본 발명의 일실시예에 따른 젤란검은 점도유지제로 포함된 것으로 겔화된 후의 필터 조성물이 적정 점도를 갖도록 하는 효과를 가지고 있다. 조성물 전체 중량 대비 0.1 내지 1중량%의 범위로 포함하는 것이 바람직한데, 0.1중량% 미만의 함량으로 포함되는 경우 제형이 너무 묽게 제작되어 제형이 고정되지 않으므로 바람직하지 못하며, 1중량%를 초과하는 경우 필터가 물에 잘 녹지 않을 수 있으므로 바람직하지 못하다.Gellan gum according to one embodiment of the present invention is included as a viscosity maintaining agent and has the effect of ensuring that the filter composition after gelation has an appropriate viscosity. It is preferable to include it in the range of 0.1 to 1% by weight based on the total weight of the composition. However, if it is included in an amount of less than 0.1% by weight, it is undesirable because the formulation is made too diluted and the formulation is not fixed, and if it is included in an amount of less than 1% by weight, it is undesirable. This is not desirable because the filter may not dissolve well in water.
본 발명의 일실시예에 따른 콜라겐은 피부에 탄력을 부여하는 효과를 가지고 있다. 조성물 전체 중량 대비 0.5 내지 2중량%의 범위로 포함하는 것이 바람직한데, 0.5중량% 미만의 함량으로 포함되는 경우 충분한 효과를 발휘하지 못하므로 바람직하지 못하며, 2중량%를 초과하는 경우 다른 성분들의 함량이 상대적으로 줄게 되어 염소제거 필터링 효과가 충분하지 않으므로 바람직하지 못하다.Collagen according to one embodiment of the present invention has the effect of providing elasticity to the skin. It is preferable to include it in the range of 0.5 to 2% by weight based on the total weight of the composition. However, if it is included in an amount of less than 0.5% by weight, it is undesirable because it does not have a sufficient effect. If it exceeds 2% by weight, the content of other components This is undesirable because the chlorine removal filtering effect is relatively reduced and the chlorine removal filtering effect is not sufficient.
본 발명의 일실시예에 따른 말토덱스트린은 다른 성분재와 배합시 조직을 안정화시키는 역할을 하며, 피부에 피막을 형성하는 효과를 가지고 있다. 조성물 전체 중량 대비 5 내지 10중량%의 범위로 포함하는 것이 바람직한데, 5중량% 미만의 함량으로 포함되는 경우 다른 성분들과 제대로 섞이지 않아 제형이 불안정하게 되므로 바람직하지 못하며, 10중량%를 초과하는 경우 다른 성분들의 함량이 상대적으로 줄게 되어 염소제거 필터링 효과가 충분하지 않으므로 바람직하지 못하다.Maltodextrin according to one embodiment of the present invention plays a role in stabilizing tissue when mixed with other ingredients and has the effect of forming a film on the skin. It is preferable to contain it in the range of 5 to 10% by weight based on the total weight of the composition. However, if it is included in an amount of less than 5% by weight, it is not desirable because it does not mix properly with other ingredients and the formulation becomes unstable. In this case, the content of other components is relatively reduced, which is not desirable because the chlorine removal filtering effect is not sufficient.
본 발명의 일실시예에 따른 락토오즈는 피부 컨디셔닝 효과 및 각질의 박리를 쉽게 하는 효과를 가지고 있다. 조성물 전체 중량 대비 10 내지 15중량%의 범위로 포함하는 것이 바람직한데, 10중량% 미만의 함량으로 포함되는 경우 충분한 효과를 내지 못할 수 있어 바람직하지 못하며, 15중량%를 초과하는 경우 피부에 자극을 줄 수 있으므로 바람직하지 못하다.Lactose according to one embodiment of the present invention has a skin conditioning effect and an effect of facilitating exfoliation of dead skin cells. It is preferable to include it in the range of 10 to 15% by weight based on the total weight of the composition. However, if it is included in an amount of less than 10% by weight, it is undesirable because it may not provide a sufficient effect, and if it exceeds 15% by weight, it may irritate the skin. It is not desirable because it can give
본 발명의 일실시예에 따른 전분은 겔 필터 조성물의 조직의 제형을 유지하는 효과를 가지고 있다. 조성물 전체 중량 대비 10 내지 15중량%의 범위로 포함하는 것이 바람직한데, 10중량% 미만의 함량으로 포함되는 경우 제형이 물에 닿았을 때 너무 빨리 녹아내려서 필터로 다회성 사용이 어렵기 때문에 바람직하지 못하며, 15중량%를 초과하는 경우 필터가 물에 녹지 않게 되므로 바람직하지 못하다.Starch according to one embodiment of the present invention has the effect of maintaining the structure of the gel filter composition. It is preferable to include it in the range of 10 to 15% by weight based on the total weight of the composition, but if it is included in an amount of less than 10% by weight, it is not desirable because the formulation dissolves too quickly when in contact with water, making it difficult to use it multiple times as a filter. If it exceeds 15% by weight, it is undesirable because the filter becomes insoluble in water.
본 발명의 일실시예에 따른 씨솔트는 살균 및 항염 효과를 가지고 있으며, 피부에 존재하는 노폐물을 제거하는 데 우수한 효과를 가지고 있다. 조성물 전체 중량 대비 5 내지 12중량%의 범위로 포함하는 것이 바람직한데, 5중량% 미만의 함량으로 포함되는 경우 항염 및 향균 효과를 충분히 발휘하지 못하므로 바람직하지 못하며, 12중량%를 초과하는 경우 피부에 자극이 되며 염분이 물에 많아 물 사용 후 주변에 백화현상을 일으키게 되므로 바람직하지 못하다. Sea salt according to an embodiment of the present invention has sterilizing and anti-inflammatory effects and is excellent at removing waste products present on the skin. It is preferable to include it in the range of 5 to 12% by weight based on the total weight of the composition. However, if it is included in an amount of less than 5% by weight, it is undesirable because it does not sufficiently exert anti-inflammatory and antibacterial effects. If it exceeds 12% by weight, it is undesirable because it does not exert sufficient anti-inflammatory and antibacterial effects. It is undesirable because it is irritating to the skin and the salt content in the water causes bleaching in the surrounding area after use.
본 발명의 또 다른 양태는 다음과 같은 단계를 포함하는 겔필터 제조방법에 관한 것이다.Another aspect of the present invention relates to a gel filter manufacturing method comprising the following steps.
(a) 비타민 C, 글리세린, 젤란검, 콜라겐, 말토텍스트린, 씨솔트를 섞은 혼합물을 8 내지 10시간 동안 10℃이하의 저온에서 숙성하는 단계; (a) aging a mixture of vitamin C, glycerin, gellan gum, collagen, maltotextrin, and sea salt at a low temperature of 10°C or lower for 8 to 10 hours;
(b) 상기 (a)단계의 숙성된 혼합물을 70 내지 75℃의 온도에서 3 내지 4시간 동안 가열하는 단계; (b) heating the aged mixture of step (a) at a temperature of 70 to 75°C for 3 to 4 hours;
(c) 상기 (b)단계의 가열된 혼합물에 10 내지 15중량% 함량의 전분(corn starch)을 7번에 거쳐 혼입하는 단계; 및 (c) mixing 10 to 15% by weight of starch into the heated mixture of step (b) in seven steps; and
(d) 상기 (c)단계의 혼합물을 급속 냉동하여 액체 상태의 용액을 겔 타입으로 굳히는 단계(d) Quickly freezing the mixture of step (c) to harden the liquid solution into a gel type.
본 발명의 일실시예에 따른 상기 (a)단계는 비타민 C 35 내지 50중량%, 글리세린 5 내지 12 중량%, 젤란검 0.1 내지 1 중량%, 콜라겐 0.5 내지 2 중량%, 말토덱스트린 5 내지 10 중량%, 락토오즈 10 내지 15 중량% 및 씨솔트(Sea salt) 5 내지 12 중량%를 섞은 혼합물을 8 내지 10시간 동안 10℃이하의 저온에서 숙성하는 단계일 수 있다.Step (a) according to an embodiment of the present invention includes 35 to 50% by weight of vitamin C, 5 to 12% by weight of glycerin, 0.1 to 1% by weight of gellan gum, 0.5 to 2% by weight of collagen, and 5 to 10% by weight of maltodextrin. %, 10 to 15 wt% of lactose, and 5 to 12 wt% of sea salt may be aged at a low temperature of 10°C or lower for 8 to 10 hours.
비타민 C는 습기와 햇빛에 노출되면 산화되어 색이 변색되는데, 산화되면 효능이 일부 저하되며, 미적으로 변질된 제품처럼 보이기 때문에 상품 가치가 떨어지게 된다는 단점이 있다.Vitamin C is oxidized and discolors when exposed to moisture and sunlight. When oxidized, some of its efficacy is reduced, and it looks like an aesthetically deteriorated product, which reduces its product value.
비타민 C는 100℃ 이상의 고온에서 성분이 파괴되기 시작하기 때문에, 본 발명은 비타민 C의 파괴를 최소화할 수 있도록 100℃ 이하 저온에서 미리 숙성시킴으로써 제조 후 숙성되며 산화되는 것을 막도록 숙성을 진행하였으며, (a)단계의 저온 숙성 진행 후 (b)단계의 숙성을 단계별로 진행함으로써 조직의 안정성을 향상시킬 수 있도록 하였다.Since vitamin C begins to be destroyed at high temperatures above 100°C, the present invention pre-ripes it at a low temperature below 100°C to minimize the destruction of vitamin C, thereby preventing it from being oxidized. After the low-temperature aging in step (a), the aging in step (b) was carried out step by step to improve the stability of the tissue.
본 발명의 일실시예에 따른 상기 (c)단계는 가열된 혼합물에 전체 조성물 대비 10 내지 15중량% 함량이 되도록 옥수수 전분(corn starch)을 혼입하고, 이때 옥수수 전분 총중량 대비 10중량%, 10중량%, 15중량%, 25중량%, 20중량%, 15중량%, 5중량%의 비율로 순차적으로 혼입하는 단계일 수 있다.In step (c) according to an embodiment of the present invention, corn starch is mixed into the heated mixture to an amount of 10 to 15% by weight relative to the total composition, and at this time, 10% by weight and 10% by weight relative to the total weight of corn starch. %, 15% by weight, 25% by weight, 20% by weight, 15% by weight, and 5% by weight.
또한, 상기 (c)단계에서 옥수수 전분(corn starch)은 7개의 입자 크기별로 구분하여 옥수수 전분 총중량 대비 17~20㎛를 10중량%, 15~18㎛를 10중량%, 13~16㎛를 15중량%, 11~14㎛를 25중량%, 9~12㎛를 20중량%, 7~10㎛를 15중량%, 5~8㎛를 5중량%의 비율로 혼입하는 것이 바람직하다.In addition, in step (c), corn starch was divided into 7 particle sizes: 17 to 20㎛ was 10% by weight, 15 to 18㎛ was 10% by weight, and 13 to 16㎛ was 15% by weight, compared to the total weight of corn starch. Weight percent, it is preferable to mix 11-14㎛ at 25% by weight, 9-12㎛ at 20% by weight, 7-10㎛ at 15% by weight, and 5-8㎛ at 5% by weight.
본 발명의 일실시예는 전분으로 옥수수 전분을 사용하는데, 옥수수 전분은 입자가 상대적으로 크지 않으면서도, 점도가 너무 높지도 낮지도 않아 적정한 점도의 조직을 제조할 수 있다.One embodiment of the present invention uses corn starch as starch, and corn starch has relatively small particles and has a viscosity that is neither too high nor too low, allowing the production of a tissue with an appropriate viscosity.
또한 옥수수 전분은 비타민 C의 산 성분에 강한 특징이 있어 재료 배합 시 가장 효율이 좋다.In addition, corn starch is resistant to the acid component of vitamin C, so it is the most efficient when mixing ingredients.
본 발명은 (a)단계에서 전분을 제외한 나머지 성분들을 먼저 혼합하여 숙성을 한 후에 (c)단계에서 전분을 추가로 배합하는 것을 특징으로 하는데, 이는 전분을 미리 다른 성분들과 함께 혼합하면 다른 재료들이 교반될 때 전분이 고르게 섞이지 않고 뭉치게 되므로 겔 조성물의 균질성이 떨어지기 때문이며, 전분이 균질하게 퍼져 있지 않고 뭉치게 되면, 필터가 녹을 때 고르게 녹는 것이 아니라, 전분만 덩어리지면서 떨어져 나오는 현상이 있다.The present invention is characterized by first mixing and maturing the remaining ingredients except starch in step (a), and then additionally mixing starch in step (c). This means that if starch is mixed with other ingredients in advance, the remaining ingredients are mixed and aged. This is because the starch does not mix evenly and clumps up when the filter is stirred, which reduces the homogeneity of the gel composition. If the starch is not spread evenly and clumps up, the starch does not dissolve evenly when the filter is melted, but only the starch clumps and falls off. .
또한 본 발명의 다른 특징은 옥수수 전분의 입자를 크기별로 나누어서 7번의 단계별로 첨가하는 것인데, 선단계에서는 입자의 크기가 상대적으로 큰 전분을 혼입하고, 뒤로 갈수록 입자의 크기가 작은 입자를 혼입하여 단계별 겔화를 진행한다. 이와 같은 방법으로 진행하는 경우, 다른 크기의 입자에 의하여 내부의 빈 공간을 줄여 조직의 결합력을 향상시키고 치밀한 조직을 만들 수 있다. 이 경우 선단계에서 작은 크기의 입자를 첨가하면 전분입자끼지 뭉쳐 고르게 분포되기 어렵기 때문에 큰 입자부터 혼입을 하고, 뒤로 갈수록 작은 입자를 공급하여 조직의 치밀도를 높일 수 있다.In addition, another feature of the present invention is to divide the corn starch particles by size and add them in seven stages. In the first stage, starch with relatively large particle size is mixed, and in the latter stage, particles with smaller particle size are mixed, thereby adding the corn starch particles in seven stages. Proceed with gelation. When proceeding in this way, the internal empty space can be reduced by particles of different sizes, improving the cohesion of the tissue and creating a dense tissue. In this case, if small-sized particles are added at the preliminary stage, the starch particles clump together and it is difficult to distribute them evenly, so large particles are added first, and smaller particles are supplied later to increase the density of the structure.
본 발명의 일실시예에 있어서, 상기 (b)단계는 상대습도 0 내지 5%를 유지하는 것이 바람직하다. 상대습도가 5%를 초과하는 경우 제형이 변질되므로 바람직하지 못하다.In one embodiment of the present invention, it is desirable to maintain the relative humidity at 0 to 5% in step (b). If the relative humidity exceeds 5%, it is undesirable because the formulation deteriorates.
또한, 상기 (d)단계에서 급속냉동을 하여 제형 겔 타입으로 굳힘으로써 세균이 증식하는 것을 예방할 수 있다. 급속냉동 온도는 -60 내지 -50℃의 온도 범위에서 진행되는 것이 바람직한데, -60℃ 미만의 온도를 유지하는 것은 비용이 많이 들어 경제적이지 못하며, -50℃를 초과하는 경우 급속냉동이 진행되지 못하므로 바람직하지 못하다. In addition, the proliferation of bacteria can be prevented by quick freezing in step (d) to solidify the formulation into a gel type. Quick freezing is preferably carried out in the temperature range of -60 to -50℃. However, maintaining a temperature below -60℃ is expensive and uneconomical, and if it exceeds -50℃, rapid freezing cannot proceed. It is not desirable because it is not possible.
상기와 같은 방법에 의하여 제조된 겔필터 조성물은 조직의 안정성이 향상되어 각 필터가 필터링할 수 있는 물의 양을 증가시킬 수 있으며, 필터 조직 내의 영양성분을 오랜 기간 유지시킴으로써 피부 개선 및 사용 후 보습 효과를 향상시킬 수 있다.The gel filter composition manufactured by the above method improves the stability of the tissue, which can increase the amount of water that each filter can filter, and improves the skin and moisturizes after use by maintaining the nutrients in the filter tissue for a long period of time. can be improved.
이하, 본 발명을 하기 실시예에서 보다 상세하게 기술한다.Hereinafter, the present invention will be described in more detail in the following examples.
다만, 하기 실시예는 본 발명의 내용을 예시하는 것일 뿐 본 발명의 권리범위를 제한하거나 한정하는 것이 아니다. 본 발명의 상세한 설명 및 실시예로부터 본 발명이 속하는 기술분야의 통상의 기술자가 용이하게 유추할 수 있는 것은 본 발명의 권리범위에 속하는 것으로 해석된다. However, the following examples only illustrate the content of the present invention and do not limit or limit the scope of the present invention. Anything that can be easily inferred by a person skilled in the art from the detailed description and examples of the present invention will be interpreted as falling within the scope of the present invention.
명세서 전체에서, 어떤 부분이 어떤 구성 요소를 "포함"한다고 할 때, 이는 특별히 반대되는 기재가 없는 한 다른 구성 요소를 제외하는 것이 아니라 다른 구성 요소를 더 포함할 수 있는 것을 의미한다. Throughout the specification, when a part is said to “include” a certain component, this means that it may further include other components rather than excluding other components, unless specifically stated to the contrary.
[실시예][Example]
[실시예 1][Example 1]
비타민 C, 글리세린, 젤란검, 콜라겐, 말토텍스트린, 락토오즈, 씨솔트를 섞은 혼합물을 8 내지 10시간 동안 8 내지 10℃에서 숙성하였다. 그 후 숙성된 혼합물을 70 내지 75℃의 온도에서 3.5시간 동안 가열하였다. A mixture of vitamin C, glycerin, gellan gum, collagen, maltotextrin, lactose, and sea salt was aged at 8 to 10°C for 8 to 10 hours. The aged mixture was then heated at a temperature of 70 to 75°C for 3.5 hours.
가열된 혼합물에 옥수수 전분(corn starch)을 7개의 입자 크기별로 구분하여 옥수수 전분 총중량 대비 17~20㎛를 10중량%, 15~18㎛를 10중량%, 13~16㎛를 15중량%, 11~14㎛를 25중량%, 9~12㎛를 20중량%, 7~10㎛를 15중량%, 5~8㎛를 5중량%의 비율로 순차적으로 혼입하였다. In the heated mixture, corn starch was divided into 7 particle sizes: 17 to 20㎛ was 10% by weight, 15 to 18㎛ was 10% by weight, 13 to 16㎛ was 15% by weight, and 11 to 11% of the total weight of corn starch. ~14㎛ was sequentially mixed at 25% by weight, 9~12㎛ at 20% by weight, 7~10㎛ at 15% by weight, and 5~8㎛ at 5% by weight.
혼합물을 겔필터 용기 안에 채워넣고, 급속 냉동하여 액체 상태의 용액을 겔 타입으로 굳혀 겔필터를 제조하였다.The mixture was filled into a gel filter container and rapidly frozen to harden the liquid solution into a gel type to prepare a gel filter.
각 성분들의 함량비를 다음의 표 1에 나타내었다. The content ratio of each component is shown in Table 1 below.
[비교예][Comparative example]
실시예 1의 제조공정에서 씨솔트를 제외한 나머지 성분을 조합하여 제조하였다. 옥수수 전분을 포함하여 모든 성분을 한꺼번에 혼입하여, 혼합물을 겔필터 용기 안에 채워넣고, 100~105℃의 온도에서 1 시간 동안 고온으로 가열하여 제조하였다. It was manufactured by combining the remaining ingredients except sea salt in the manufacturing process of Example 1. It was prepared by mixing all ingredients, including corn starch, into a gel filter container and heating it at a high temperature of 100-105°C for 1 hour.
[실험결과][Experiment result]
1. 필터링 수량 비교 실험1. Filtering quantity comparison experiment
실시예 및 비교예의 겔필터를 이용하여 필터링할 수 있는 물의 양을 측정하기 위하여 24g의 겔필터를 실시예 및 비교예 별로 각각 10개씩 사용하였다. 겔필터에 2bar의 수압 조건에서 물을 흐르게 한 후, 필터가 다 녹는 동안 유입된 물의 양을 측정하는 방식으로 측정한 평균수치는 다음과 같다.To measure the amount of water that can be filtered using the gel filters of Examples and Comparative Examples, 10 24g gel filters were used for each Example and Comparative Example. The average values measured by flowing water through the gel filter at a water pressure of 2 bar and then measuring the amount of water flowing in while the filter is completely dissolved are as follows.
위 결과에서 알 수 있듯이 실시예에 비해 비교예는 필터당 필터링할 수 있는 물의 양이 약 25% 정도 적다는 것을 알 수 있다.As can be seen from the above results, compared to the Example, the amount of water that can be filtered per filter in the Comparative Example is about 25% less.
또한, 실험과정에서 전분이 덩어리져서 떨어져 나오는 일도 있었는데 실시예에 비해서 비교예의 경우 그 정도가 심했으며, 이는 비교예의 겔필터 제조시 전분을 다른 성분들과 함께 넣고 교반함으로써 전분이 고르게 분포되지 않고 전분끼리 뭉치는 현상이 발생했기 때문으로 판단된다.In addition, during the experiment, starch clumped and fell off, which was more severe in the comparative example than in the example. This was due to the fact that starch was mixed with other ingredients and stirred when manufacturing the gel filter of the comparative example, so the starch was not evenly distributed and the starch was not evenly distributed. It is believed that this is because a phenomenon of grouping together occurred.
2. 겔필터 변색 실험2. Gel filter discoloration experiment
실시예 1 및 비교예의 겔필터를 상온에서 6개월 보관한 후 필터의 색변화를 추적하였고 이를 도 1에 나타내었다. 도 1의 이미지에서 좌측이 제조 직후의 필터이며, 가운데가 실시예 1의 필터, 우측이 비교예의 필터이다.After the gel filters of Example 1 and Comparative Example were stored at room temperature for 6 months, the color change of the filter was tracked, and this is shown in Figure 1. In the image of Figure 1, the left side is the filter immediately after manufacturing, the middle side is the filter of Example 1, and the right side is the filter of Comparative Example.
실시예 1의 필터는 약간의 노란색을 띠는 것을 알 수 있는 반면, 비교예의 필터는 주황색으로 색 변화가 심한 것을 알 수 있다.The filter of Example 1 can be seen to have a slight yellow color, while the filter of Comparative Example can be seen to have a severe color change to orange.
이는 비교예의 경우 고온에서 가열하여 제조함으로써 비타민 C 성분의 파괴가 더 많기 때문인 것으로 판단되며, 비교예인 우측 필터는 사진 이미지에서는 잘 드러나지는 않았으나, 특히 물이 들어가는 홀 부분에 공기와 닿아서 변색이 심한 부분이 있었다. 따라서 실시예 1의 경우 저온제조공정뿐만 아니라, 전분을 입자크기별로 나누어서 순차적으로 혼입하면서 제조함으로써 조직의 치밀성이 증가하여 변색의 정도가 낮아진 것으로 판단할 수 있다.This is believed to be because, in the case of the comparative example, there was more destruction of the vitamin C component as it was manufactured by heating at a high temperature. The filter on the right, which is the comparative example, was not clearly visible in the photographic image, but the discoloration was severe due to contact with air, especially in the hole where water enters. There was a part. Therefore, in the case of Example 1, it can be judged that the degree of discoloration was lowered by increasing the density of the structure by manufacturing starch by dividing it by particle size and mixing it sequentially in addition to the low-temperature manufacturing process.
Claims (8)
A gel filter composition for water treatment containing vitamin C, glycerin, gellan gum, collagen, maltodextrin, lactose, starch, and sea salt.
상기 조성물은 비타민 C 35 내지 50중량%, 글리세린 5 내지 12 중량%, 젤란검 0.1 내지 1 중량%, 콜라겐 0.5 내지 2 중량%, 말토덱스트린 5 내지 10 중량%, 락토오즈 10 내지 15 중량%, 전분 10 내지 15 중량% 및 씨솔트(Sea salt) 5 내지 12 중량%를 포함하는 것을 특징으로 하는 수처리용 겔필터 조성물.
According to paragraph 1,
The composition contains 35 to 50% by weight of vitamin C, 5 to 12% by weight of glycerin, 0.1 to 1% by weight of gellan gum, 0.5 to 2% by weight of collagen, 5 to 10% by weight of maltodextrin, 10 to 15% by weight of lactose, and starch. A gel filter composition for water treatment comprising 10 to 15% by weight and 5 to 12% by weight of sea salt.
(b) 상기 (a)단계의 숙성된 혼합물을 70 내지 75℃의 온도에서 3 내지 4시간 동안 가열하는 단계;
(c) 상기 (b)단계의 가열된 혼합물에 10 내지 15중량% 함량의 전분(corn starch)을 7번에 거쳐 혼입하는 단계;및
(d) 상기 (c)단계의 혼합물을 급속 냉동하여 액체 상태의 용액을 겔 타입으로 굳히는 단계
를 포함하는 수처리용 겔필터 제조방법.
(a) maturing a mixture of vitamin C, glycerin, gellan gum, collagen, maltotextrin, lactose, and sea salt at a low temperature of 10°C or lower for 8 to 10 hours;
(b) heating the aged mixture of step (a) at a temperature of 70 to 75°C for 3 to 4 hours;
(c) mixing 10 to 15% by weight of starch into the heated mixture of step (b) in seven steps; and
(d) Quickly freezing the mixture of step (c) to harden the liquid solution into a gel type.
A method of manufacturing a gel filter for water treatment comprising.
상기 (a)단계는 비타민 C 35 내지 50중량%, 글리세린 5 내지 12 중량%, 젤란검 0.1 내지 1 중량%, 콜라겐 0.5 내지 2 중량%, 말토덱스트린 5 내지 10 중량%, 락토오즈 10 내지 15 중량% 및 씨솔트(Sea salt) 5 내지 12 중량%를 섞은 혼합물을 8 내지 10시간 동안 10℃이하의 저온에서 숙성하는 단계인 것을 특징으로 하는 수처리용 겔필터 제조방법.
According to paragraph 3,
Step (a) includes 35 to 50% by weight of vitamin C, 5 to 12% by weight of glycerin, 0.1 to 1% by weight of gellan gum, 0.5 to 2% by weight of collagen, 5 to 10% by weight of maltodextrin, and 10 to 15% by weight of lactose. A method of manufacturing a gel filter for water treatment, characterized in that the step of maturing a mixture of 5 to 12% by weight of sea salt at a low temperature of 10° C. or lower for 8 to 10 hours.
상기 (c)단계에서 가열된 혼합물에 전체 조성물 대비 10 내지 15중량% 함량의 옥수수 전분(corn starch)을, 옥수수 전분 총중량 대비 10중량%, 10중량%, 15중량%, 25중량%, 20중량%, 15중량%, 5중량%의 비율로 순차적으로 혼입하는 것을 특징으로 하는 수처리용 겔필터 제조방법.
According to paragraph 4,
Corn starch in an amount of 10 to 15% by weight relative to the total composition was added to the mixture heated in step (c), and 10% by weight, 10% by weight, 15% by weight, 25% by weight, and 20% by weight relative to the total weight of corn starch. A method of manufacturing a gel filter for water treatment, characterized in that it is sequentially mixed in ratios of %, 15% by weight, and 5% by weight.
상기 (c)단계에서 옥수수 전분(corn starch)은 7개의 입자 크기별로 구분하여 옥수수 전분 총중량 대비 17~20㎛를 10중량%, 15~18㎛를 10중량%, 13~16㎛를 15중량%, 11~14㎛를 25중량%, 9~12㎛를 20중량%, 7~10㎛를 15중량%, 5~8㎛를 5중량%의 비율로 순차적으로 혼입하는 것을 특징으로 하는 수처리용 겔필터 제조방법.
According to clause 5,
In step (c), corn starch is divided into seven particle sizes, and 17-20㎛ is 10% by weight, 15-18㎛ is 10% by weight, and 13-16㎛ is 15% by weight, based on the total weight of corn starch. , A water treatment gel characterized by sequentially mixing 11-14㎛ at 25% by weight, 9-12㎛ at 20% by weight, 7-10㎛ at 15% by weight, and 5-8㎛ at 5% by weight. Filter manufacturing method.
상기 (b)단계는 상대습도 0 내지 5%를 유지하는 것을 특징으로 하는 수처리용 겔필터 제조방법.
According to paragraph 3,
The step (b) is a method of manufacturing a gel filter for water treatment, characterized in that the relative humidity is maintained at 0 to 5%.
상기 (d)단계에서 -60 내지 -50℃의 온도에서 급속냉동하는 것을 특징으로 하는 수처리용 겔필터 제조방법.
According to paragraph 3,
A method of manufacturing a gel filter for water treatment, characterized in that rapid freezing at a temperature of -60 to -50 ° C in step (d).
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101069579B1 (en) | 2009-07-07 | 2011-10-05 | 정지행 | Gel composition for shower filter, method for manufacturing shower gel filter and shower filter |
| KR102357806B1 (en) | 2021-08-10 | 2022-02-09 | 주식회사 에이치이공일 | Eco-friendly metal chelate gel filter, manufacturing method thereof, and soft water shower head using the same |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101069579B1 (en) | 2009-07-07 | 2011-10-05 | 정지행 | Gel composition for shower filter, method for manufacturing shower gel filter and shower filter |
| KR102357806B1 (en) | 2021-08-10 | 2022-02-09 | 주식회사 에이치이공일 | Eco-friendly metal chelate gel filter, manufacturing method thereof, and soft water shower head using the same |
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