KR20230054518A - A wrinkle-removing agent composition for cloths having antibacterial property - Google Patents
A wrinkle-removing agent composition for cloths having antibacterial property Download PDFInfo
- Publication number
- KR20230054518A KR20230054518A KR1020210137105A KR20210137105A KR20230054518A KR 20230054518 A KR20230054518 A KR 20230054518A KR 1020210137105 A KR1020210137105 A KR 1020210137105A KR 20210137105 A KR20210137105 A KR 20210137105A KR 20230054518 A KR20230054518 A KR 20230054518A
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- South Korea
- Prior art keywords
- antibacterial
- sterilization
- extract
- fraction
- rice bran
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
- D06M11/71—Salts of phosphoric acids
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/20—Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
Abstract
Description
본 발명은 건조된 의류 또는 건조 후 착용하여 주름이 발생한 의류의 주름발생부위에 분무 방식으로 분사되어 섬유의 주름을 개선하는 섬유 콜라겐 성분 및 카복시메틸셀룰로오스 파우더가 포함된 계면활성제를 포함하는 섬유주름 개선 물질에 살균 및 항균기능을 갖는 조성물을 포함하여 섬유주름 개선과 살균 및 항균기능을 포함시킨 섬유주름 개선제에 관한 것이다. The present invention is a fiber collagen component that is sprayed on the wrinkle-producing part of dried clothes or clothes that are worn after drying and wrinkles are generated by spraying to improve wrinkles of fibers and wrinkle improvement including a surfactant containing carboxymethyl cellulose powder. It relates to a fiber wrinkle improvement agent including a composition having a bactericidal and antibacterial function in a material and including a sterilizing and antibacterial function.
확산된 코로나19는 사람들 간 대면접촉을 기피하는 언택트 문화의 확산, 원격교육 및 재택근무 급증 등 사회 전반에 큰 변화를 일으켰다.The spread of COVID-19 has brought about major changes throughout society, such as the spread of an untact culture in which people avoid face-to-face contact, and a rapid increase in remote education and telecommuting.
포스트 코로나는 코로나19로 인해 일어난 변화들이 향후 우리 사회를 주도할 것으로 예상된다. 특히, 공공방역 뿐만 아니라 개인위생, 면역, 살균 및 항균 등이 중요한 화두가 될 것으로 예상된다.In the post-corona era, it is expected that the changes caused by COVID-19 will lead our society in the future. In particular, not only public quarantine, but also personal hygiene, immunity, sterilization and antibacterial are expected to become important topics.
바이러스는 눈, 입, 코로 감염된다고 알려져 있다. 그래서 손으로 눈이나 입을 만지면 안되고 외출 후에는 손을 깨끗이 씻는 것을 권장한다.Viruses are known to infect the eyes, mouth and nose. Therefore, it is recommended that you do not touch your eyes or mouth with your hands and wash your hands thoroughly after going out.
그러나 옷에 바이러스가 붙어 있다면 완벽한 방어가 어렵다. 의류에 붙어있는 바이러스는 세탁이나 고온 스팀을 통해 제거한다.However, if the virus is attached to clothes, perfect defense is difficult. Viruses attached to clothing are removed through washing or high-temperature steam.
근래들어, 바이러스를 제거하면서 옷의 주름제거와 균이나 바이러스를 제거하는 것이 동시에 가능하게 하는 의류 관리기기가 인기를 끌고 있다.[0003] Recently, a clothing care device capable of removing wrinkles from clothes and removing germs or viruses while removing viruses is gaining popularity.
그러나 이러한 의류 관리기기는 고가일 뿐만 아니라 휴대성이 낮아 외출이나 여행시 활용할 수 없는 단점이 있다.However, these clothes management devices are not only expensive but also have low portability, so they cannot be used when going out or traveling.
본 발명은 상술한 문제를 해결하고자 하는 것으로 휴대성이 높으면서 저렴한 섬유 주름 개선과 살균 및 항균기능을 모두 갖는 섬유주름 개선제를 제공하는 데 있다.An object of the present invention is to provide a highly portable and inexpensive fiber wrinkle improving agent having both sterilization and antibacterial functions.
본 발명의 일 실시예에 따른 살균 및 항균기능을 갖는 섬유주름 개선제는 수산화나트륨, 실라이트, 탄산나트륨, 규산나트륨, 카복시메틸셀룰로오스, 계면활성제를 포함하는 섬유주름 개선 조성물와 천연식물 유래 살균 및 항균물질과 당 알코올을 포함하는 제1 살균 및 항균물질을 포함할 수 있다. The fiber wrinkle improving agent having sterilization and antibacterial function according to an embodiment of the present invention is a fiber wrinkle improvement composition including sodium hydroxide, silite, sodium carbonate, sodium silicate, carboxymethylcellulose, and a surfactant, and a natural plant-derived sterilization and antibacterial material It may include a first bactericidal and antibacterial substance including sugar alcohol.
또한, 상기 천연식물 유래 살균 및 항균물질은 쪽풀 추출물 또는 이의 분획물과 회향 추출물 또는 이의 분획물을 포함할 수 있다. In addition, the natural plant-derived bactericidal and antibacterial substances may include an indigo plant extract or a fraction thereof and a fennel extract or a fraction thereof.
또한, 상기 천연식물 유래 살균 및 항균물질은 상기 쪽풀 추출물의 분획물과 상기 회향 추출물의 분획물을 혼합하는 단계, 상기 혼합된 쪽풀 추출물의 분획물과 회향 추출물의 분획물에 초음파를 인가하는 단계, 상기 초음파가 인가된 쪽풀 추출물의 분획물과 회향 추출물의 분획물에 전기자극을 가하는 단계를 포함하여 제조될 수 있다. In addition, the natural plant-derived sterilization and antibacterial material includes mixing the indigo extract fraction and the fennel extract fraction, applying ultrasonic waves to the mixed indigo extract fraction and fennel extract fraction, and applying the ultrasonic wave to the mixture. It may be prepared by including the step of applying electrical stimulation to a fraction of the indigo extract and a fraction of the fennel extract.
또한, 상기 살균 및 항균기능을 갖는 섬유주름 개선제는 인산티타늄화합물, 이산화티타늄 화합물, 티타늄, 망간, 이산화망간 중 적어도 하나를 포함하는 광촉매에 물을 첨가하여 제조된 광촉매수를 더 포함하되,상기 광촉매는 광의 유무와 관계없이 광촉매 반응이 일어날 수 있다. In addition, the fiber wrinkle improving agent having bactericidal and antibacterial functions further includes a photocatalyst water prepared by adding water to a photocatalyst containing at least one of a titanium phosphate compound, a titanium dioxide compound, titanium, manganese, and manganese dioxide, wherein the photocatalyst A photocatalytic reaction can occur regardless of the presence or absence of light.
또한, 상기 살균 및 항균기능을 갖는 섬유주름 개선제는 발효미강 성분을 포함하는 미네랄수를 더 포함할 수 있다. In addition, the fiber wrinkle improving agent having bactericidal and antibacterial functions may further include mineral water containing a fermented rice bran component.
또한, 상기 미네랄수는 (1) 미강에 발효균을 혼합하여 미강을 발효시키는 단계; (2) 상기 (1) 단계에서 발효된 미강을 펠렛 형태로 성형하고 건조하여 발효미강 펠렛을 제조하는 단계; (3) 상기 (2) 단계에서 제조된 발효미강 펠렛을 제1 온도범위로 가열하여 소성한 후 냉각하여 미네랄 알갱이를 제조하는 단계; (4) 상기 (3) 단계에서 제조된 미네랄 알갱이를 제2 온도범위로 가열하여 용융시킨 후 냉각하여 미네랄 결정체를 제조하는 단계; 및(5) 상기 (4) 단계에서 제조된 미네랄 결정체에 스팀을 분사하여 미네랄수를 제조하는 단계를 포함하여 제조될 수 있다. In addition, the mineral water may be prepared by (1) fermenting rice bran by mixing fermenting bacteria with rice bran; (2) preparing fermented rice bran pellets by forming and drying the fermented rice bran in the form of pellets; (3) preparing mineral grains by heating and calcining the fermented rice bran pellets prepared in step (2) to a first temperature range and then cooling them; (4) preparing mineral crystals by heating and melting the mineral grains prepared in step (3) to a second temperature range and then cooling them; and (5) spraying steam on the mineral crystals prepared in step (4) to produce mineral water.
본 발명의 천연유래 살균 및 항균성분과 섬유주름 개선 성분이 모두 포함된 섬유주름 개선제는 휴대성이 높으면서도 옷감의 주름을 쉽게 제거하고, 바이러스 등으로부터 착용자를 보호하는 장점이 있다. The fabric wrinkle reducing agent containing all of the natural sterilization and antibacterial components and the fabric wrinkle improving component of the present invention has the advantage of easily removing wrinkles from fabric and protecting the wearer from viruses and the like while having high portability.
도 1은 본 발명의 섬유주름 개선 조성물을 옷감에 분사하기 전과 후의 표면 확대 사진이다.
도 2는 본 발명의 제1 살균 및 항균물질과 전기분해수를 혼합한 살균 및 항균실험 결과이다.
도 3은 본 발명의 제1 살균 및 항균물질의 항곰팡이 효능 실험 결과이다
도 4는 본 발명의 다중광촉매의 TEM 이미지이다.1 is an enlarged photograph of the surface before and after spraying the fabric wrinkle improvement composition of the present invention on cloth.
2 is a result of a sterilization and antibacterial experiment in which the first sterilization and antibacterial substance of the present invention and electrolyzed water are mixed.
3 is an antifungal efficacy test result of the first bactericidal and antibacterial substance of the present invention
4 is a TEM image of the multi-photocatalyst of the present invention.
본 발명의 살균 및 항균기능을 갖는 섬유주름 개선제는 섬유주름 개선 조성물과 제1 살균 및 항균물질, 제2 살균 및 항균물질, 제3 살균 및 항균물질을 포함할 수 있다.The fiber wrinkle improving agent having sterilization and antibacterial function of the present invention may include a fiber wrinkle improvement composition, a first bactericidal and antibacterial substance, a second bactericidal and antibacterial substance, and a third bactericidal and antibacterial substance.
여기서 살균 및 항균물질이라 함은 살균 및 항균물질이 섬유에 분무되었을때 즉각적으로 균이나 바이러스가 제거되는 살균기능과 이러한 균 제거효과가 일정시간 지속되는 항균기능이 모두 구비된 것을 의미한다.Here, the sterilization and antibacterial material means that both a sterilization function in which germs or viruses are immediately removed when the sterilization and antibacterial material is sprayed on the fiber and an antibacterial function in which the germ removal effect lasts for a certain period of time are provided.
<섬유주름 개선 조성물><Fabric wrinkle improvement composition>
본 발명에 따른 섬유주름 개선 조성물은 수산화나트륨, 실라이트, 탄산나트륨, 규산나트륨, 카복시메틸셀룰로오스, 계면활성제가 혼합된다.In the fabric wrinkle improvement composition according to the present invention, sodium hydroxide, silite, sodium carbonate, sodium silicate, carboxymethyl cellulose, and a surfactant are mixed.
상기 계면활성제는 수용액으로 했을 때 세정, 습윤, 유화, 기포, 가용화, 분산 등의 활성을 나타내는데, 직물의 마찰을 감소시키고, 직물에 흡착되어 유연성을 부여하는 기능을 수행하며, 바람직하게는 N-D-Sulfonic acid를 적용한다.The surfactant exhibits activities such as cleaning, wetting, emulsifying, foaming, solubilizing, and dispersing when used as an aqueous solution, and performs functions such as reducing friction of fabrics and adsorbing to fabrics to impart flexibility, preferably N-D- Apply sulfonic acid.
본 발명에서의 섬유 주름 개선제는 콜라겐이 사람의 피부를 팽윤시켜 주름을 제거하는 것처럼 섬유를 팽윤시켜 구김을 제거하는 작용을 한다. 특히 기존의 실록산 계열의 주름 개선제는 건조 후 뻣뻣해지는 단점이 있었으나, 본 섬유 주름 개선조성물은 섬유가 뻣뻣해지지 않으면서 직물의 주름이 발생하는 근본적인 원인을 제거하여 실록산 계열의 주름 개선제보다 주름개선 효과가 높다. The fiber wrinkle improving agent in the present invention acts to remove wrinkles by swelling fibers, just as collagen swells human skin to remove wrinkles. In particular, conventional siloxane-based wrinkle-improving agents have the disadvantage of becoming stiff after drying, but this fiber wrinkle-improving composition eliminates the fundamental cause of wrinkles in fabrics without stiffening the fibers, so that the wrinkle-improving effect is higher than that of siloxane-based wrinkle-improving agents. high.
상기 섬유주름 개선 조성물은 수산화나트륨 0.5 내지 2 중량%, 실라이트 1.5 내지 2.5 중량%, 탄산나트륨 3 내지 5.5 중량%, 규산나트륨 1 내지 1.5 중량%, 카복시메틸셀룰로오스 0.8 내지 1 중량%, 계면활성제 1.5 내지 2.5 중량% 포함할 수 있다. The fabric wrinkle improvement composition contains 0.5 to 2% by weight of sodium hydroxide, 1.5 to 2.5% by weight of silite, 3 to 5.5% by weight of sodium carbonate, 1 to 1.5% by weight of sodium silicate, 0.8 to 1% by weight of carboxymethylcellulose, and 1.5 to 1.5% by weight of a surfactant. It may contain 2.5% by weight.
도 1은 본 발명의 섬유주름 개선 조성물을 분사 전후 표면 확대 사진이다. 도 1을 참조하면, 본 발명의 섬유주름 개선 조성물을 분사한 경우에 섬유가 균일하게 부풀어 주름이 개선되는 것을 알 수 있다.1 is an enlarged photograph of the surface before and after spraying the fabric wrinkle improvement composition of the present invention. Referring to FIG. 1 , it can be seen that when the composition for improving wrinkles of fibers of the present invention is sprayed, the fibers are uniformly swollen and wrinkles are improved.
<제1 살균 및 항균물질><First sterilization and antibacterial substance>
본 발명의 일 실시예에 따른 제1 살균 및 항균물질은 천연식물 유래 살균 및 항균물질과 당 알코올을 포함할 수 있다.The first sterilizing and antibacterial material according to an embodiment of the present invention may include a natural plant-derived sterilizing and antibacterial material and sugar alcohol.
1. 천연식물 유래 살균 및 항균물질1. Sterilization and antibacterial substances derived from natural plants
본 발명의 천연식물 유래 살균 및 항균물질은 세척 및 정선된 회향과 쪽풀을 각각 추출용매로 환류 추출하여 추출액을 수득하는 단계, 추출액을 여과와 농축 및 동결건조하여 분말화하는 단계, 분말을 증류수에 분산시킨 후 유기용매를 사용하여 회향 추출물의 분획물과 쪽풀 추출물의 분획물을 수득하는 단계, 상기 회향 추출물의 분획물과 쪽풀 추출물의 분획물을 혼합하고 초음파 자극을 가하여 나노화하는 단계, 나노화된 천연 식물성 성분들이 상호 간에 침투되도록 나노화된 회향 추출물의 분획물과 나노화된 쪽풀 추출물의 혼합물에 전기자극을 가하는 단계, 상기 전기자극이 가해진 나노화된 천연 식물성 성분들을 가열한 후 진공건조하는 단계를 포함하여 제조될 수 있다.The natural plant-derived sterilization and antibacterial substance of the present invention is obtained by reflux-extracting the washed and selected fennel and indigo plant with an extraction solvent, respectively, to obtain an extract, filtering, concentrating, and freeze-drying the extract to powder, powdering the powder in distilled water. After dispersing, obtaining fractions of fennel extract and fractions of indigo extract using an organic solvent, mixing the fractions of fennel extract and fractions of indigo extract and nanonizing them by applying ultrasonic stimulation, nanonized natural vegetable ingredients mutually It can be prepared by applying electrical stimulation to a mixture of nanonized fennel extract fraction and nanonized indigo plant extract so as to penetrate the liver, heating the nanonized natural vegetable ingredients to which the electrical stimulation has been applied, and then vacuum-drying.
(1) 추출액 수득 단계(1) Extraction step
회향과 쪽풀을 깨끗이 세척하고 각각 에탄올을 추출용매로 사용하여 1시간씩 2회 환류 추출하여 회향 추출액과 쪽풀 추출액을 수득한다. Fennel and indigo are washed thoroughly, and reflux extraction is performed twice for 1 hour each using ethanol as an extraction solvent to obtain fennel extract and indigo extract.
(2) 분말화 단계(2) Powdering step
이후, 회향 추출액과 쪽풀 추출액을 통상적인 방법으로 여과하고, 여과된 회향 추출액과 쪽풀 추출액을 회전식 감압 농축기로 농축하며, 농축된 회향 추출액과 쪽풀 추출액을 각각 동결건조하여 분말화 한다. 이렇게 분말화 단계를 거친 회향 추출액과 쪽풀 추출액을 각각 회향 추출물 분말과 쪽풀 추출물 분말이라 한다.Thereafter, the fennel extract and indigo extract are filtered in a conventional manner, the filtered fennel extract and indigo extract are concentrated with a rotary vacuum concentrator, and the concentrated fennel extract and indigo extract are respectively lyophilized and powdered. The fennel extract and indigo extract that have undergone the powdering step are referred to as fennel extract powder and indigo extract powder, respectively.
(3) 분획물 수득단계(3) Step of obtaining fractions
회향 추출물 분말과 쪽풀 추출물 분말 각각에 증류수를 혼합하여 회향 추출물 분말과 쪽풀 추출물 분말을 증류수에 분산시키고, 유기용매를 투입하여 회향 추출물의 분획물과 쪽풀 추출물의 분획물 수득한다. Distilled water was mixed with the fennel extract powder and the indigo extract powder, respectively, the fennel extract powder and the indigo extract powder were dispersed in distilled water, and an organic solvent was added to obtain a fraction of the fennel extract and a fraction of the indigo extract.
본 발명의 일 실시예에 따르면, 회향 추출물 분말을 증류수에 분산시켜 회향 추출물이 포함된 수용액(이하, 회향 추출물 수용액이라 함)을 제조할 수 있다. 마찬가지로 쪽풀 추출물 분말을 증류수에 분산시켜 쪽풀 추출물이 포함된 수용액(이하, 쪽풀 추출물 수용액이라 함)을 제조할 수 있다. According to one embodiment of the present invention, an aqueous solution containing fennel extract (hereinafter referred to as an aqueous fennel extract) may be prepared by dispersing fennel extract powder in distilled water. Similarly, an indigo extract powder may be dispersed in distilled water to prepare an aqueous solution containing an indigo extract (hereinafter referred to as an indigo extract aqueous solution).
회향 추출물 분말과 증류수의 중량비는 쪽풀 추출물 분말과 증류수의 중량비와 동일하다. 일 실시예에 따르면 분말과 증류수의 중량비는 1:1 내지 1:10일 수 있다. The weight ratio of fennel extract powder and distilled water is the same as that of indigo extract powder and distilled water. According to one embodiment, the weight ratio of the powder to the distilled water may be 1:1 to 1:10.
상기 회향 추출물 수용액과 쪽풀 추출물 수용액의 중량비는 1:0.1 내지 1: 5일 수 있다. The weight ratio of the fennel extract aqueous solution and the indigo extract aqueous solution may be 1:0.1 to 1:5.
회향 추출물 수용액에 유기용매를 투입하여 회향 추출물의 분획물 수득할 수 있다. 마찬가지로 쪽풀 추출물 수용액에 유기용매를 투입하여 쪽풀 추출물의 분획물할 수 있다. An organic solvent may be added to an aqueous solution of fennel extract to obtain fractions of fennel extract. Similarly, the indigo plant extract can be fractionated by adding an organic solvent to the aqueous solution of the indigo plant extract.
바람직하게는 회향 추출물 수용액과 유기용매의 중량비는 1: 1.5 내지 1: 8일 수 있다. 또한, 쪽풀 추출물 수용액과 유기용매의 중량비도 1: 1.5 내지 1: 8일 수 있다. Preferably, the weight ratio of the aqueous solution of fennel extract to the organic solvent may be 1: 1.5 to 1: 8. In addition, the weight ratio of the aqueous indigo plant extract to the organic solvent may be 1: 1.5 to 1: 8.
상기 유기용매는 핵산(hexane), 클로로포름(chloroform), 에틸아세테이트(ethylacetate), 부탄올(butanol) 중 선택되는 어느 1종 또는 2종 이상으로 조성된 것이 사용된다. As the organic solvent, one or two or more selected from among nucleic acid (hexane), chloroform, ethyl acetate, and butanol are used.
(4) 나노화 단계(4) Nanoization step
상기 수득된 회향 추출물의 분획물과 쪽풀 추출물의 분획물을 혼합한다. 이후, 혼합된 회향 추출물의 분획물과 쪽풀 추출물의 분획물이 나노화되도록 초음파 자극을 가한다. 상기 초음파 자극은 35000Hz 내지 50000Hz 주파수의 초음파로 3분 자극한 후 2분동안 안정시키는 과정을 총 12회 반복할 수 있다. 이를 통해 나노화된 회향 추출물의 분획물과 쪽풀 추출물의 분획물을 얻을 수 있다. The fractions of the fennel extract obtained above and the fractions of the indigo plant extract were mixed. Thereafter, ultrasonic stimulation is applied so that the fractions of the mixed fennel extract and the fractions of the indigo extract are nano-sized. The ultrasonic stimulation may repeat a process of stabilizing for 2 minutes after 3 minutes stimulation with ultrasonic waves of 35000Hz to 50000Hz frequency, a total of 12 times. Through this, it is possible to obtain a fraction of nano-sized fennel extract and a fraction of indigo plant extract.
(5) 전기자극 단계(5) electrical stimulation step
이후, 나노화된 회향 추출물의 분획물이 나노화된 쪽풀 추출물의 분획물에 침투되도록 전기자극을 가한다. 여기서, 전기자극은 80~110V 50~65mA로 10분~30분 1회 자극하거나, 50~110V 30~50mA로 10분~20분 2회 자극할 수 있다. 이 과정에서 나노화된 회향 추출물의 분획물이 나노화된 쪽풀 추출물의 분획물에 침투하거나, 반대로 나노화된 쪽풀 추출물의 분획물이 나노화된 회향 추출물의 분획물에 침투될 수 있다. Thereafter, electrical stimulation is applied so that the fraction of the nano-sized fennel extract is penetrated into the nano-sized fraction of the indigo plant extract. Here, the electrical stimulation may be stimulated once for 10 minutes to 30 minutes at 80 ~ 110V 50 ~ 65mA, or twice for 10 minutes ~ 20 minutes at 50 ~ 110V 30 ~ 50mA. In this process, the fraction of the nanonized fennel extract may permeate into the nanonized fraction of the indigo extract, or conversely, the fraction of the nanonized indigo extract may penetrate into the nanonized fraction of the fennel extract.
(6) 가열 및 진공건조 단계(6) heating and vacuum drying step
이후, 전기자극이 가해진 회향 및 쪽풀 추출물의 분획물을 섭씨 900도~1,100도에서 25분~35분간 가열한 후 7시간동안 진공건조하여 천연식물 유래 살균 및 항균물질을 얻을 수 있다.Thereafter, the fractions of the fennel and indigo plant extracts to which the electrical stimulation was applied are heated at 900 degrees Celsius to 1,100 degrees Celsius for 25 minutes to 35 minutes, and then vacuum dried for 7 hours to obtain natural plant-derived sterilization and antibacterial substances.
이렇게 제조된 천연식물 유래 살균 및 항균물질은 나노화된 회향 추출물의 분획물과 쪽풀 추출물의 분획물이 이온반응을 통해 상호 침투되면서 세균의 세포막 구조를 흐트려 버리는 특수한 구조를 형성하여 살균 및 항균 효능을 극대화시킬 수 있다. 또한, 상기 특수 구조는 동물의 세포막에는 안전한 장점이 있다. The natural plant-derived sterilization and antibacterial substance prepared in this way maximizes sterilization and antibacterial efficacy by forming a special structure that disrupts the cell membrane structure of bacteria as the fractions of nano-sized fennel extract and indigo plant extract interpenetrate through ionic reactions. can In addition, the special structure has the advantage of being safe for animal cell membranes.
또한, 상기 천연식물 유래 살균 및 항균물질은 나노화된 회향 추출물의 분획물과 나노화된 쪽풀 추출물의 분획물이 상호간에 서로 침투되어 기존의 식물 추출 농축액보다 살균 및 항균성을 지니는 유효성분 결합부위에 결합 친화도를 높여 살균 및 항균 기능을 높일 수 있다.In addition, the natural plant-derived sterilization and antibacterial substance has a binding affinity to the active ingredient binding site having sterilization and antibacterial properties than conventional plant extract concentrates by mutually infiltrating each other with the fractions of the nano-sized fennel extract and the nano-sized fraction of the indigo plant extract. It can increase sterilization and antibacterial function.
2.당 알코올2. Sugar alcohol
본 발명의 일 실시예에 따른 당 알코올은 솔비톨(Sorbitol), 자이리톨(Xylitol), 말티톨(Maltitol), 만니톨(Mannitol), 에리트리톨(Erithritol), 락티톨(Lactitol) 중 적어도 하나를 포함할 수 있다.The sugar alcohol according to an embodiment of the present invention may include at least one of sorbitol, xylitol, maltitol, mannitol, erythritol, and lactitol. .
본 발명의 말티톨과 솔비톨은 균주의 대사를 방해하여 균을 사멸시킬 수 있다. 또한, 말티톨은 만노오즈(mannose)로 전환되며 솔비톨은 글루코즈(Glucose)와 같은 글리칸 물질로 전환될 수 있다. 이렇게 전환된 글리칸은 세균과 바이러스를 둘러싸고 있는 구성물질로서 세균과 세균 또는 바이러스와 숙주간의 상호작용에 영향을 미쳐 세균과 바이러스의 활성을 저해시킨다. Maltitol and sorbitol of the present invention can kill the bacteria by interfering with the metabolism of the strain. In addition, maltitol can be converted into mannose and sorbitol can be converted into glycan substances such as glucose. The converted glycan is a constituent material surrounding bacteria and viruses, and inhibits the activity of bacteria and viruses by affecting interactions between bacteria and viruses or between viruses and hosts.
또한, 솔비톨과 말티톨은 국내에서 설탕을 대체하는 식품 첨가물로 허용되고 있을 정도로 동물에 무해한 장점이 있다. In addition, sorbitol and maltitol have the advantage of being harmless to animals to the extent that they are accepted as food additives replacing sugar in Korea.
또한, 상기 솔비톨과 말티톨은 상기 천연식물 유래 살균 및 항균물질의 살균 및 항균기능을 높이는 장점이 있다. In addition, the sorbitol and maltitol have the advantage of increasing the sterilization and antibacterial functions of the natural plant-derived sterilization and antibacterial substances.
본 발명의 일 실시예에 따른 제1 살균 및 항균물질은 상기 천연식물 유래 살균 및 항균물질 1~60 중량부, 솔비톨 4~ 20 중량부, 말티톨 5~ 40 중량부를 포함할 수 있다.The first bactericidal and antibacterial substance according to an embodiment of the present invention may include 1 to 60 parts by weight of the natural plant-derived bactericidal and antibacterial substance, 4 to 20 parts by weight of sorbitol, and 5 to 40 parts by weight of maltitol.
도 2는 상기 제1 살균 및 항균물질과 전기분해수를 혼합한 살균 및 항균실험 결과이다. 2 is a result of a sterilization and antibacterial experiment in which the first sterilization and antibacterial substance and electrolyzed water are mixed.
도 2를 참조하면, MRSA 내성균과 CPE 항생제 내성균을 키우는 액체 배양액에 상기 제1 살균 및 항균물질과 전기분해수의 최종 적용 농도가 각각 1%, 0.5% 되도록 처리 하였을 때 MRSA와 CPE균 모두 1%, 0.5%에서 99.9% 살균 및 항균 효능을 나타냈다. Referring to FIG. 2, when the liquid culture medium for growing MRSA-resistant bacteria and CPE antibiotic-resistant bacteria is treated so that the final application concentrations of the first sterilization and antibacterial substance and electrolysis water are 1% and 0.5%, respectively, both MRSA and CPE bacteria are 1% , showed 99.9% bactericidal and antibacterial efficacy at 0.5%.
여기서, NX2020은 상기 제1 살균 및 항균물질을 의미한다. Here, NX2020 means the first sterilization and antibacterial substance.
또한, 차아산성 또는 차아알칼리라 함은 전기분해수중 알칼리성을 띠는 물질을 차아알칼리로, 산성을 띠는 물질은 차아산성으로 하였다.In addition, with respect to hypoxic acid or hypoalkali, the alkaline substance in the electrolysis water was hypoalkali, and the acidic substance was hypophosphorous.
또한, NX2020 1%라 함은 전기분해수를 용매로, 제1 살균 및 항균물질을 용질로 하였을때의 농도를 의미한다.In addition,
도 2를 참조하면, 상기 제1 살균 및 항균물질(NX2020)은 0.5% 이상의 농도에서는 완벽 한 살균 및 항균 효능을 나타내므로 최적의 효능 유지를 위해 스프레이 살균 및 항균 제품의 경우 0.5% 첨가만으로도 원하는 살균 및 항균 효과를 얻을 수 있다.Referring to FIG. 2, the first sterilization and antibacterial substance (NX2020) exhibits perfect sterilization and antibacterial efficacy at a concentration of 0.5% or more, so in the case of spray sterilization and antibacterial products, only 0.5% addition is desired to maintain optimum efficacy. and antibacterial effect.
도 3은 상기 제1 살균 및 항균물질의 항곰팡이 효능 실험 결과이다. 실험대상 곰팡이는 Cladosporium cladosporioides이다. 상기 Cladosporium cladosporioides는 실외,실내의 광범위한 재료에서 전 세계적으로 발생하는 어두운 색소의 곰팡이며 계절성 알레르기 질환에 포자가 중요한 야외 공기에서 가장 흔한 곰팡이 중 하나이다.3 is an antifungal efficacy test result of the first bactericidal and antibacterial substance. The fungus tested is Cladosporium cladosporioides. The Cladosporium cladosporioides is a dark-colored fungus that occurs worldwide in a wide range of outdoor and indoor materials, and is one of the most common fungi in outdoor air, where spores are important for seasonal allergic diseases.
곰팡이 배양 배지에 Cladosporium cladosporioides를 1차 접종하여 섭씨 28도에서 4일~5일간 배양했다. 상기 곰팡이 배양 배지는 Potato Dextrose Agar 인 PDA 배지 사용했다. 1차 배양 확인 된 곰팡이를 새로운 PDA 배지에 2차 분리 접종 배양한 후, 상기 천연식물 유래 살균 및 항균물질 원액 1%를 2차 분리 접종 배양할 때 곰팡이 접종한 곳에 함께 분사(혼합) 시켰다.이후, 상기 천연식물 유래 살균 및 항균물질 원액 1% 유/무에 따른 곰팡이 생장률 비교하였다. Cladosporium cladosporioides was first inoculated into the fungal culture medium and cultured at 28°C for 4 to 5 days. The fungal culture medium was used as Potato Dextrose Agar PDA medium. After the primary culture confirmed fungus was cultured in a new PDA medium for secondary inoculation, 1% of the stock solution of the natural plant-derived sterilization and antibacterial substance was sprayed (mixed) together with the fungus inoculated area during the secondary inoculation and culture. , The fungal growth rate was compared according to the presence/absence of 1% of the natural plant-derived sterilization and antimicrobial stock solution.
도 3을 참조하면 상기 제1 살균 및 항균물질을 첨가하지 않은 배지의 곰팡이는 그대로 남아있으나, 천연식물 유래 살균 및 항균물질을 분사한 배지의 곰파이는 사멸되어 흔적만 남았다.Referring to FIG. 3, the fungus in the medium without the first sterilization and antibacterial substance remains, but the fungus in the medium sprayed with the natural plant-derived sterilization and antibacterial substance is killed and only traces remain.
상기 제1 살균 및 항균물질은 사람 세포막에는 안전하면서 세균의 세포막(벽)을 흐트려 버리는 구조를 형성시켜 탈취 및 살균 및 항균 효능이 극대화되는 장점이 있다. The first bactericidal and antibacterial substance has the advantage of maximizing deodorization, sterilization and antibacterial efficacy by forming a structure that is safe for human cell membranes and disrupts bacterial cell membranes (walls).
따라서, 본 발명의 섬유주름 개선제는 알레르기를 일으키는 포자까지 제거하여 섬유주름 개선과 더불어 알레르기 질환 발생을 억제하는 장점이 있다..Therefore, the fiber wrinkle improving agent of the present invention has the advantage of suppressing the occurrence of allergic diseases as well as improving fiber wrinkles by removing allergy-causing spores.
<제2 살균 및 항균물질><Second sterilization and antibacterial substance>
본 발명의 제2 살균 및 항균물질은 다중광촉매수이다. 상기 다중광촉매수는 다중광촉매에 물을 첨가한 것을 의미한다. The second sterilization and antibacterial material of the present invention is multi-photocatalyst water. The number of multiple photocatalysts means that water is added to multiple photocatalysts.
여기서 다중광촉매라 함은 광의 유무와 무관하게 광촉매 반응이 일어나는 것으로 바람직하게는 인산티타늄화합물, 이산화티타늄 화합물, 티타늄, 망간, 이산화망간 중 적어도 하나를 포함할 수 있다. Here, the multi-photocatalyst means that a photocatalytic reaction occurs regardless of the presence or absence of light, and may preferably include at least one of a titanium phosphate compound, a titanium dioxide compound, titanium, manganese, and manganese dioxide.
도 4는 상기 다중광촉매의 TEM 이미지이다.4 is a TEM image of the multi-photocatalyst.
도 4를 참조하면, 상기 광촉매의 지름은 3~5nm 크기의 나노 사이즈이다.Referring to FIG. 4 , the diameter of the photocatalyst is a nano size of 3 to 5 nm.
물에 다중광촉매를 투입하는 경우에 물 속에서 활성산소가 발생하여 세균, 곰팡이, 바이러스 등의 인체에 유해한 미생물을 제거하고 섬유 속 냄새를 제거할 수 있다.In the case of adding multiple photocatalysts to water, active oxygen is generated in the water to remove microorganisms harmful to the human body such as bacteria, fungi, and viruses, and to remove odors in the fibers.
<제3 살균 및 항균물질><Third sterilization and antibacterial substance>
(1) 미강 발효단계(1) Rice bran fermentation step
미강에 발효균을 혼합하고 35~40℃의 온도로 발열하며 미강 발효를 진행한다. 발효 시간은 24~36시간동안 지속되는 것이 바람직하다.Rice bran is mixed with fermenting bacteria, and the rice bran is fermented by heating at a temperature of 35~40℃. The fermentation time is preferably continued for 24 to 36 hours.
상기 발효균은 유산균, 김치분말, 청국장분말, 맥주효모, 메주분말, 맥아균사체 중 적어도 하나를 포함할 수 있다. 다만 상기 발효균은 상술한 것에 한정되지 않고 상용화된 발효균을 사용할 수 있다. The fermenting bacteria may include at least one of lactic acid bacteria, kimchi powder, cheonggukjang powder, brewer's yeast, meju powder, and malt mycelium. However, the fermentation bacteria are not limited to those described above, and commercialized fermentation bacteria may be used.
상기 미강은 13% 정도의 조단백질과 조지방을 함유하고 있으며 무기염류와 비타민류도 다수 포함된다The rice bran contains about 13% of crude protein and crude fat, and also contains many inorganic salts and vitamins.
상기 발효과정을 통해 미강의 유기물 중 일부가 무기염류로 치환되면서 미강의 무기염류 비율이 증가된다Through the fermentation process, some of the organic matter in the rice bran is replaced with inorganic salts, thereby increasing the ratio of inorganic salts in the rice bran.
(2) 펠렛 제조단계(2) Pellets manufacturing step
상기 발효된 미강을 펠렛 형태로 성형한다. The fermented rice bran is molded into a pellet form.
상기 펠렛 성형단계는 상기 미강 발효 단계에서 생성된 발효 미강을 펠렛 밀에 투입하여 분쇄 및 혼합하여 직경이 5mm 내지 10mm인 다이 (die)를 통하여 배출하여 발효미강을 펠렛으로 성형한다. 이렇게 성형된 펠렛을 발효미강 펠렛이라 한다. 이후 성형된 발효미강 펠렛을 건조하여 발효미강의 함수율을 낮춘다. In the pellet forming step, the fermented rice bran generated in the rice bran fermentation step is put into a pellet mill, pulverized and mixed, and discharged through a die having a diameter of 5 mm to 10 mm to form the fermented rice bran into pellets. The pellets formed in this way are called fermented rice bran pellets. Thereafter, the molded fermented rice bran pellets are dried to lower the moisture content of the fermented rice bran.
이렇게 제조된 발효미강 펠렛은 기존의 발효미강에 비해 스팀 분사시 추출되는 미네랄의 양이 증가된다.The fermented rice bran pellets prepared in this way increase the amount of minerals extracted when steam is sprayed compared to conventional fermented rice bran.
(3) 제1차 소성단계(3) 1st firing step
상기 제조된 발효미강 펠렛을 제1 온도범위로 가열하여 소성한다. 바람직하게 900 ~ 1000℃ 온도로 가열한다. 상기 소성을 통해 미강의 유기물이 탄화와 산화 과정을 통해 제거되면서 구형의 미네랄 알갱이가 생성된다.The prepared fermented rice bran pellets are heated and calcined in a first temperature range. Preferably heated to a temperature of 900 ~ 1000 ℃. Through the firing, spherical mineral grains are produced as the organic matter of rice bran is removed through carbonization and oxidation processes.
(4) 제1차 냉각단계(4) 1st cooling step
상기 생성된 구형의 미네랄 알갱이를 냉각하여 안정화시킨다. 바람직하게 상기 미네랄 알갱이를 1시간 내지 3시간 동안 상온에서 냉각시킬 수 있다.The resulting spherical mineral grains are cooled and stabilized. Preferably, the mineral grains may be cooled at room temperature for 1 hour to 3 hours.
(4) 제2차 소성단계(4) Second firing step
상기 생성된 구형의 미네랄 알갱이를 제2 온도범위로 가열하여 소성한다. 상기 제2 온도는 상기 제1 온도보다 높다. 상기 제2 온도로 상기 미네랄 알갱이를 가열하면 상기 미네랄 알갱이가 용융된다. The produced spherical mineral grains are fired by heating to a second temperature range. The second temperature is higher than the first temperature. When the mineral grains are heated to the second temperature, the mineral grains are melted.
바람직하게 상기 제2 온도는 1200~1300℃일 수 있다. Preferably, the second temperature may be 1200 to 1300 °C.
(5) 제2차 냉각단계(5) 2nd cooling step
상기 제2차 소성단계에서 용융된 미네랄 알갱이를 냉각하여 용융된 미네랄 알갱이를 미네랄 결정체를 제조한다.Mineral crystals are prepared from the molten mineral grains by cooling the mineral grains melted in the second sintering step.
(5) 미네랄수 제조(5) Manufacture of mineral water
상기 제2차 냉각단계에서 제조된 미네랄 알갱이에 고온의 스팀을 분사하여 미네랄 결정체로부터 미네랄을 추출하여 천연미네랄이 함유된 천연 미네랄수를 제조할 수 있다. It is possible to prepare natural mineral water containing natural minerals by extracting minerals from mineral crystals by spraying high-temperature steam on the mineral grains prepared in the second cooling step.
이렇게 제조된 미네랄수는 살균, 살균 및 항균, 항염, 악취제거가 있어 상기 미네랄수를 섬유에 분사하는 경우에 섬유속 세균이 사멸되면서 섬유속 냄새제거 효과가 있다. The mineral water prepared in this way has sterilization, sterilization and antibacterial properties, anti-inflammation, and odor removal, so that when the mineral water is sprayed on the fiber, bacteria in the fiber are killed and the fiber is deodorized.
Claims (5)
천연식물 유래 살균 및 항균물질과 당 알코올을 포함하는 제1 살균 및 항균물질을 포함하는 살균 및 항균기능을 갖는 섬유주름 개선제.
A fiber wrinkle improvement composition containing sodium hydroxide, silite, sodium carbonate, sodium silicate, carboxymethylcellulose, and a surfactant; and
A fabric wrinkle improvement agent having a bactericidal and antibacterial function, comprising a natural plant-derived bactericidal and antibacterial substance and a first bactericidal and antibacterial substance containing sugar alcohol.
상기 천연식물 유래 살균 및 항균물질은
쪽풀 추출물 또는 이의 분획물과 회향 추출물 또는 이의 분획물을 포함하는 살균 및 항균기능을 갖는 섬유주름 개선제.
According to claim 1,
The natural plant-derived sterilization and antibacterial substance is
An agent for improving fiber wrinkles having bactericidal and antibacterial functions, comprising an indigo plant extract or a fraction thereof and a fennel extract or a fraction thereof.
상기 천연식물 유래 살균 및 항균물질은
상기 쪽풀 추출물의 분획물과 상기 회향 추출물의 분획물을 혼합하는 단계;
상기 혼합된 쪽풀 추출물의 분획물과 회향 추출물의 분획물에 초음파를 인가하는 단계; 및
상기 초음파가 인가된 쪽풀 추출물의 분획물과 회향 추출물의 분획물에 전기자극을 가하는 단계를 포함하여 제조된 것을 특징으로 하는 살균 및 항균기능을 갖는 섬유주름 개선제.
According to claim 2,
The natural plant-derived sterilization and antibacterial substance is
mixing the fractions of the indigo plant extract and the fractions of the fennel extract;
applying ultrasonic waves to the mixed fraction of indigo plant extract and fraction of fennel extract; and
A fiber wrinkle improving agent having bactericidal and antibacterial functions, characterized in that it is prepared by applying electrical stimulation to the fraction of the indigo plant extract and the fraction of the fennel extract to which the ultrasonic waves have been applied.
상기 살균 및 항균기능을 갖는 섬유주름 개선제는
인산티타늄화합물, 이산화티타늄 화합물, 티타늄, 망간, 이산화망간 중 적어도 하나를 포함하는 광촉매에 물을 첨가하여 제조된 광촉매수를 더 포함하되,
상기 광촉매는 광의 유무와 관계없이 광촉매 반응이 일어나는 것을 특징으로 하는 살균 및 항균기능을 갖는 섬유주름 개선제.
According to claim 1,
The fiber wrinkle improving agent having the sterilization and antibacterial function
Further comprising a photocatalyst water prepared by adding water to a photocatalyst containing at least one of a titanium phosphate compound, a titanium dioxide compound, titanium, manganese, and manganese dioxide,
The photocatalyst is a fiber wrinkle improvement agent having a sterilization and antibacterial function, characterized in that the photocatalytic reaction occurs regardless of the presence or absence of light.
상기 살균 및 항균기능을 갖는 섬유주름 개선제는 발효미강 성분을 포함하는 미네랄수를 더 포함하되,
상기 미네랄수는
(1) 미강에 발효균을 혼합하여 미강을 발효시키는 단계;
(2) 상기 (1) 단계에서 발효된 미강을 펠렛 형태로 성형하고 건조하여 발효미강 펠렛을 제조하는 단계;
(3) 상기 (2) 단계에서 제조된 발효미강 펠렛을 제1 온도범위로 가열하여 소성한 후 냉각하여 미네랄 알갱이를 제조하는 단계;
(4) 상기 (3) 단계에서 제조된 미네랄 알갱이를 제2 온도범위로 가열하여 용융시킨 후 냉각하여 미네랄 결정체를 제조하는 단계; 및
(5) 상기 (4) 단계에서 제조된 미네랄 결정체에 스팀을 분사하여 미네랄수를 제조하는 단계를 포함하여 제조된 것을 특징으로 하는 섬유주름 개선제. According to claim 1,
The fiber wrinkle improving agent having sterilization and antibacterial function further includes mineral water containing a fermented rice bran component,
The mineral water is
(1) fermenting rice bran by mixing fermenting bacteria with rice bran;
(2) preparing fermented rice bran pellets by forming and drying the fermented rice bran in the form of pellets;
(3) preparing mineral grains by heating and calcining the fermented rice bran pellets prepared in step (2) to a first temperature range and then cooling them;
(4) preparing mineral crystals by heating and melting the mineral grains prepared in step (3) to a second temperature range and then cooling them; and
(5) A fabric wrinkle improving agent characterized in that it is prepared by including the step of preparing mineral water by spraying steam on the mineral crystals prepared in step (4).
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