KR20210121560A - Drinking water using natural material concentrate concentrated with water-soluble ion calcium culture solution and its manufacturing method - Google Patents

Abstract

The present invention relates to a drinking water using a natural material concentrate concentrated with a water-soluble ionized calcium culture solution and a manufacturing method thereof, wherein the drinking water is manufactured by using the natural material concentrate manufactured by concentrating natural materials using the water-soluble ionic calcium culture solution to significantly reduce pesticides remaining in the natural materials. According to the present invention, any one of the natural materials consisting of ginseng fruit, red ginseng, Dendropanax morbiferus, Kochia scoparia Schrader seeds, bellflower root, elm, Centella asiatica, Zizania latifolia, and Schisandra chinensis fruit are mixed by using the water-soluble ionized calcium culture solution, and the mixture is heated and concentrated in a double boiler to extract a concentrated solution with reduced residual pesticide components. The natural material concentrate is mixed with the water-soluble ionized calcium culture solution, thereby manufacturing the drinking water with increased quality and consumer preference.

Description

Drinking water using natural material concentrate concentrated with water-soluble ion calcium culture solution and its manufacturing method

The present invention relates to drinking water using a natural material concentrate concentrated with a water-soluble ionic calcium culture solution and a method for producing the same, and more particularly, by concentrating a natural material using a water-soluble ionic calcium culture solution to significantly reduce the pesticide components remaining in the natural material It relates to drinking water using a natural material concentrate concentrated with a water-soluble ionic calcium culture solution that enables the production of drinking water with the natural material concentrate obtained from the product, and a method for manufacturing the same.

As social interest in health increases, the demand for various natural materials with excellent effects on the human body is rapidly increasing.

On the other hand, for the stable supply of various natural materials, it is almost essential to use pesticides when growing crops. It is difficult to cultivate without use.

As a result, residual pesticide components tend to exist in the supplied natural materials, and a pesticide removal or decomposition process is required to reduce these residual pesticide components.

First, as a conventional technique for reducing residual pesticide components, Publication No. 10-2018-0089696 “Method for Removal of Pesticide Residue of Natural Plant Extract”, Registration No. 10-1195817 “Method for Manufacturing Residual Pesticide Degrading Agent and Residual pesticide decomposing agent manufactured by this”, Registration No. 10-0425377 “Removal method and product of oil-soluble residual pesticide contained in products manufactured with herbal extracts”, Registration No. 10-0529541 “Sterilization using ozone and Residual pesticide treatment method and treatment device”, Publication No. 2001-0107854 “Method for manufacturing ginseng concentrate from which residual pesticide has been removed and ginseng concentrate produced by this method”, etc.

The above conventional techniques suggest a method for reducing pesticides remaining in raw materials such as natural materials, but conventional sterilization and pesticide decomposition methods such as heating, high-temperature and high-pressure treatment, and catalytic chemical reaction are destructive of nutrients, loss of flavor, and harmful There was a problem in that the production of high-quality food was impossible by causing a serious deterioration in the quality of natural materials such as the generation of substances.

The present invention has been devised to solve the problems of the prior art, and any one of natural materials consisting of ginseng fruit, red ginseng, hwangchil tree, jibuja, bellflower, elm, centella asiatica, japonica and omija using a water-soluble ionic calcium culture solution of raw materials are mixed, heated, and concentrated to extract a concentrated solution with reduced residual pesticide components, and the natural material concentrate is mixed with a water-soluble ionic calcium culture solution to produce drinking water with improved quality and consumer preference. It was completed as a technical task with the main focus on providing drinking water and its manufacturing method using a natural material concentrate concentrated with a water-soluble ionic calcium culture solution.

According to the present invention for achieving the above object, natural materials consisting of ginseng fruit, red ginseng, hwangchil tree, jibuja, bellflower, elm tree, centella asiatica, japonica and omija, water-soluble ionic calcium in which 1 to 5 g per 1000 ml of water is dissolved. A water-soluble ionic calcium culture solution containing a mixture of a raw material of any one of the above natural materials and a water-soluble ionic calcium culture solution is heated at 55 ° C. for 24 hours, and the bathed mixture is heated at 100 to 120 ° C. for 10 hours, the heating a natural material concentrate extracted by concentrating the mixture under reduced pressure; Providing drinking water using the concentrated natural material concentrate with the water-soluble ionic calcium culture solution, characterized in that the water-soluble ionic calcium culture solution and the natural material concentrate are mixed in a weight ratio of 1000: 30 ~ 1000: 50,

Moryeo is calcined at ultra-high temperature using high-purity carbon powder, then pulverized to prepare water-soluble ionic calcium, and water to dissolve the water-soluble ionic calcium is weighed and stored by a preset amount, and 1 to 5 g of water-soluble ions per 1000 ml of water A water-soluble ionic calcium culture solution preparation step of mixing and dissolving calcium to prepare a water-soluble ionic calcium culture solution; 10 kg of any one raw material of ginseng fruit, red ginseng, hwangchil tree, jibuja, bellflower, elm tree, centella asiatica, japonica, and omija and 20L of the water-soluble ionic calcium culture medium prepared in the above-mentioned water-soluble ionic calcium culture medium are mixed and heated at 55°C for 24 hours. jungtang step of jungtang; a heating step of heating the mixture that has undergone the bathing step at 100 to 120° C. for 10 hours; a concentration step of concentrating the mixture that has undergone the heating step under reduced pressure; A drinking water production step of preparing drinking water by mixing 30 ml to 50 ml of the concentrated solution concentrated in the concentration step with 1 L of the water-soluble ionic calcium culture solution prepared in the water-soluble ionic calcium culture solution production step; To solve the problem by providing a method for producing drinking water using a natural material concentrate concentrated with a water-soluble ionic calcium culture solution, characterized in that consisting of

According to the drinking water and its manufacturing method using the natural material concentrate concentrated with the water-soluble ionic calcium culture solution according to the present invention, residual pesticide components of natural materials are reduced by sterilization and pesticide decomposition methods such as conventional heating, high-temperature and high-pressure treatment, and catalytic chemical reaction. It is possible to extract the natural material concentrate by concentrating the natural material using the water-soluble ionic calcium culture solution without It is a useful invention that allows to manufacture drinking water with improved quality and improved consumer preference by mixing the material concentrate, thereby providing economical and high added value to consumers and producers.

1 is a process diagram used in the present invention;

The present invention concentrates natural materials using a water-soluble ionic calcium culture solution to produce drinking water with a natural material concentrate that significantly reduces pesticide components remaining in natural materials. Drinking water using a water-soluble ionic calcium culture solution and a manufacturing method thereof.

The present invention will be described in detail with reference to the accompanying drawings as follows.

1 is a diagram of a drinking water manufacturing process. The present invention is a drinking water manufacturing method using a natural material concentrate concentrated with a water-soluble ionic calcium culture solution.

First, a brief look at the ginseng fruit, red ginseng, hwangchil tree, jibuja, bellflower, elm tree, centella asiatica, julphus and omija used in extracting the concentrate of natural materials,

Ginseng fruit contains a lot of nutrients including saponins, and it is known that the content of ginsenosides, which has effects such as blood flow improvement, fatigue recovery, immunity enhancement, and antioxidant, is three times higher than that of the root.

Red ginseng is a light yellow-brown or light reddish-brown ginseng that has been carefully selected and dried by steaming for a long time without peeling the good quality 6-year-old fresh ginseng produced in the right place for ginseng cultivation. It contains maltol, an antioxidant component, various amino acids, organic fatty acids, etc., and is known to be particularly effective for those with weak digestive systems such as the stomach and low energy.

Hwangchil is an evergreen tree of the dicotyledonous umbel family, known to be effective in various liver diseases, and is known to be effective in anticancer effects, prevention of adult diseases, and immunity enhancement.

Jibuja is the dried seed of the daffodil plant, a plant in the sagebrush family, which makes urine easier to urinate and eliminates moist heat death. It is known that it is effective for fever, edema, urticaria, eczema, and malignant boils.

Bellflower is characterized by the characteristic bitter taste of ginseng, rich in fiber, vitamins and minerals, and saponin, a major component of the bitter taste of bellflower, is known to be good for bronchial and respiratory health.

The young leaves of the elm tree are edible in spring, and the bark of the elm is called yupi (楡皮) in oriental medicine. It is known to have an excellent effect on diseases.

Centella asiatica takes root from the node as the main stem extends sideways, and scale-like leaves come out. It is mainly used for edible medicinal purposes, mainly to treat pain and stones. It is known to be effective against anemia and fever.

It is said to be effective in all kinds of diseases such as heart disease, constipation, obesity, arteriosclerosis, diabetes, high blood pressure, stroke, etc. have.

Omija is called Omija because it has five flavors: sweet, sour, bitter (astringent), mild, and spicy. It is known to be good for diabetes because of its effect of giving, and it is known to quickly recover from fatigue and strengthen eyesight and heart function.

Hereinafter, looking at the drinking water using the natural material concentrate concentrated with the water-soluble ionic calcium culture solution of the present invention, natural materials consisting of ginseng fruit, red ginseng, hwangchil tree, jibuja, bellflower, elm, centella asiatica, julberry and omija, 1 per 1000ml of water Water-soluble ionic calcium culture solution containing water-soluble ionic calcium in which ~ 5 g is dissolved, natural material concentrate extracted by mixing any one of the raw materials and water-soluble ionic calcium culture solution in a bath, heating and concentration; The water-soluble ionic calcium culture solution and the natural material concentrate are mixed in a weight ratio of 1000: 30 to 1000: 50.

In addition, the natural material concentrate is mixed with any one of the raw materials of the natural materials and a water-soluble ionic calcium culture solution and bathed at 55°C for 24 hours, and the bathed mixture is heated at 100 to 120°C for 10 hours, The heated mixture was concentrated under reduced pressure.

Hereinafter, a step-by-step description of the drinking water manufacturing method using the natural material concentrate concentrated with the water-soluble ionic calcium culture solution according to the present invention is as follows.

① Water-soluble ionic calcium culture solution manufacturing step (S100)

The water-soluble ionic calcium culture solution preparation step (S100) is to prepare water-soluble ionic calcium by pulverizing the moryeo after calcining it at an ultra-high temperature using high-purity carbon powder, and weighing and storing the water to dissolve the water-soluble ionic calcium by a preset amount. , by mixing and dissolving 1 to 5 g of water-soluble ionic calcium per 1000 ml of water to prepare a water-soluble ionic calcium culture solution.

When the water-soluble ionic calcium culture solution manufacturing step (S100) is described in more detail, the moryeo washing step of immersing the moryeo in methyl alcohol to remove the impurities contained in the moryeo, and a drying step of evaporating the methyl alcohol from the moryeo from which the impurities are removed; A high-purity carbon powder manufacturing step of obtaining activated high-purity carbon powder from the oak charcoal powder by laminating oak charcoal powder on the carbon powder heated at a high temperature by an electrode, and after laying coke on the bottom of the electric furnace and covering it with high-purity carbon powder , A lamination step of covering the dried moryeo on the high-purity carbon powder, an ultra-high temperature firing step of firing the moryeo by heating the inside of the electric furnace at 2500 to 3000° C. for 20 minutes, and cutting off the heat supply to the electric furnace. 1 to 5 g of water-soluble ionic calcium prepared through a cooling step of cooling the moryeo and a grinding step of pulverizing the calcined morye into a powder state using a pulverizing means made of stone or ceramic material is mixed and dissolved in 1 to 5 g per 1000 ml of water to dissolve the water-soluble ionic calcium Prepare a culture solution.

Hereinafter, the water-soluble ionic calcium culture solution prepared in the manufacturing step (S100) of the water-soluble ionic calcium culture solution and the clusters (particle size of water) of serum, bottled water, groundwater, distilled water, tap water, and purified water are as follows.

Water-soluble ionized calcium culture solution and clusters of serum, bottled water, groundwater, distilled water, tap water, and purified water (particle size of water) receptivity
Ion calcium culture solution serum bottled water underground water Distilled water tap water purified water
(Osmotic pressure method) 71Hz 79Hz 94Hz 105Hz 118Hz 128Hz 150Hz

In addition, when the pH value of the aqueous ionic calcium culture solution was measured, strong alkalinity of pH 12.7 was measured, and through this, it was confirmed that the aqueous ionic calcium culture solution had excellent sterilization and absorption rate of clusters (particle size of water) 71 Hz and pH 12.7. could

② hot water step (S200)

The bathing step (S200) includes 10 kg of any one raw material of ginseng fruit, red ginseng, hwangchil tree, jibuja, bellflower, elm, centella asiatica, julberry and omija and the water-soluble ionic calcium prepared in the water-soluble ionic calcium culture solution preparation step (S100). 20L of the culture medium is mixed and bathed at 55°C for 24 hours.

Here, each of the raw materials may be included when there are stems, leaves, and peels, and after a light washing and drying process, it can be mixed with the water-soluble ionic calcium culture solution as it is in the raw material form without going through a separate grinding operation. Preferably, this is to prevent loss of raw materials and harmful substances from occurring during the pulverization operation, and to improve manufacturing efficiency by omitting unnecessary processes.

③ Heating step (S300)

The heating step (S300) is a step of heating the mixture that has undergone the hot water step (S200) at 100 to 120° C. for 10 hours.

④ Concentration step (S400)

The concentration step (S400) is a step of concentrating the mixture that has undergone the heating step (S300) under reduced pressure.

Here, in the vacuum concentration method, the mixture that has passed through the heating step (S300) can be concentrated as it is, or by centrifugation, only the supernatant can be taken and concentrated. It is not specifically limited.

Hereinafter, if the examples and comparative examples of the natural material concentrate of the present invention are shown,

1. Example

After mixing 20L of the water-soluble ionic calcium culture solution prepared in the water-soluble ionic calcium culture solution manufacturing step (S100) and 10 kg of ginseng fruit, bathing at 55°C for 24 hours, and heating the mixture through the bath at 100-120°C for 10 hours, The heated mixture is concentrated under reduced pressure to obtain a concentrated solution.

2. Comparative Example

20 L of tap water and 10 kg of ginseng fruit are mixed and bathed at 55° C. for 24 hours, and the mixture subjected to the bath is heated at 100 to 120° C. for 10 hours, and then the heated mixture is concentrated under reduced pressure to obtain a concentrate.

Hereinafter, when the test results for the residual pesticide components of the concentrates concentrated in the Comparative Examples and Examples are shown in Tables 2 and 3, respectively,

Comparative Example Residual pesticides in the concentrated concentrate Inspection items detectable component Results (mg/kg) Reference 320 pesticide residues Buprofezin 0.233 Other 303 Ingredients
non-detection Clothianidin 2.330 Cypermethrin 0.069 Cyprodinil 0.171 Difenoconazole 0.034 Dimethomorph-E, Z 0.466 Ethaboxam 6.187 Fenhexamid 2.703 Flutolanil 0.023 Kresoxim-methyl 0.392 Mandipropamid 0.025 Metalaxyl 4.523 Metconazole 4.460 propamocarb 0.334 pyraclostrobin 0.029 Tebyconazole 0.277 Trifloxystrobin 0.122

Residual pesticide components of the concentrated concentrate in an embodiment Inspection items detectable component Results (mg/kg) Reference 320 pesticide residues Cypermethrin 0.015 Other 315 Ingredients
non-detection Fenhexamid 0.078 Metalaxyl 0.015 Metconazole 0.176 pyraclostrobin 0.018

Looking at Tables 2 and 3, it was found that the residual pesticide components Cypermethrin, Fenhexamid, Metalaxyl, Metconazole, and pyraclostrobin were significantly reduced in the concentrated solution concentrated in the Example compared to the concentrated solution in Comparative Example, and the concentrated solution concentrated in the comparative example It was found that the remaining 12 pesticide components detected in the Examples were not detected in the concentrated solution.

⑤ Drinking water manufacturing step (S500)

The drinking water preparation step (S500) is a step of preparing drinking water by mixing 30ml to 50ml of the concentrated solution concentrated in the concentration step (S400) with 1L of the water-soluble ionic calcium culture solution prepared in the water-soluble ionic calcium culture solution preparation step (S100).

Hereinafter, examples and comparative examples of the production of drinking water of the present invention are shown,

1. Example

20L of the water-soluble ionic calcium culture solution prepared in the water-soluble ionic calcium culture solution preparation step (S100) and 10 kg of ginseng fruit are mixed and bathed at 55° C. for 24 hours, and the mixture through the bath is heated at 100 to 120° C. for 10 hours, The heated mixture is concentrated under reduced pressure to obtain a concentrate, and 40 ml of the concentrated solution using the water-soluble ionic calcium culture solution is mixed with 1 L of the water-soluble ionic calcium culture solution to prepare drinking water.

2. Comparative Example 1

20L of tap water and 10 kg of ginseng fruit are mixed and bathed at 55°C for 24 hours, and the mixture subjected to the bath is heated at 100 to 120°C for 10 hours, and then the heated mixture is concentrated under reduced pressure to obtain a concentrate, the tap water 40 ml of the concentrated solution was mixed with 1 L of the water-soluble ionic calcium culture solution to prepare drinking water.

3. Comparative Example 2

20L of tap water and 10 kg of ginseng fruit are mixed and bathed at 55°C for 24 hours, and the mixture subjected to the bath is heated at 100 to 120°C for 10 hours, and then the heated mixture is concentrated under reduced pressure to obtain a concentrate, the tap water 40 ml of the concentrated solution was mixed with 1 L of the tap water to prepare drinking water.

Hereinafter, a sensory test of the drinking water prepared in Examples and Comparative Examples 1 and 2 was performed.

Sensory test of drinking water prepared in Examples and Comparative Examples 1 and 2 color incense taste Overall
symbol Example 4.0 4.3 4.7 4.3 Comparative Example 1 3.8 4.1 4.2 4.0 Comparative Example 2 3.7 3.8 3.2 3.5

Referring to Table 4, the sensory test was performed by 10 well-trained panelists using a 5-point intensity method (very weak: 1 point, weak: 2 points, moderate: 3 points, strong) : 4 points, very strong : 5 points).

Looking at the results of Table 4, the color, flavor, taste, and overall preference of the drinking water prepared by the method of Comparative Example 1 were higher than those of Comparative Example 2, and the color, aroma, Taste and overall preference were higher than those of Comparative Examples 1 and 2.

According to the drinking water and its manufacturing method using the natural material concentrate concentrated with the water-soluble ionic calcium culture solution according to the present invention, residual pesticide components of natural materials are reduced by sterilization and pesticide decomposition methods such as conventional heating, high-temperature and high-pressure treatment, and catalytic chemical reaction. It is possible to extract the natural material concentrate by concentrating the natural material using the water-soluble ionic calcium culture solution without It is a useful invention that allows to manufacture drinking water with improved quality and improved consumer preference by mixing the material concentrate, thereby providing economical and high added value to consumers and producers.

S100: Water-soluble ionic calcium culture medium manufacturing step
S200: hot water step
S300: heating stage
S400: Concentration step
S500: Drinking water manufacturing stage

Claims (3)

Natural ingredients consisting of ginseng fruit, red ginseng, hwangchil tree, jibuja, bellflower, elm tree, centella asiatica, japonica and omija;
Water-soluble ionic calcium culture solution containing water-soluble ionic calcium in which 1 to 5 g per 1000 ml of water is dissolved;
a natural material concentrate extracted by mixing any one of the above natural materials and a water-soluble ionic calcium culture medium, heating and concentrating;
Drinking water using the concentrated natural material concentrate with the water-soluble ionic calcium culture solution, characterized in that the water-soluble ionic calcium culture solution and the natural material concentrate are mixed in a weight ratio of 1000: 30 to 1000: 50.
The method of claim 1,
The natural material concentrate,
Mixing any one of the above natural materials and a water-soluble ionic calcium culture solution and bathing at 55° C. for 24 hours,
The heated mixture is heated to 100 ~ 120 ℃ for 10 hours,
Drinking water using a natural material concentrate concentrated with a water-soluble ionic calcium culture solution, characterized in that the heated mixture was concentrated under reduced pressure.
Moryeo is calcined at ultra high temperature using high-purity carbon powder, then pulverized to prepare water-soluble ionic calcium, and water to dissolve the water-soluble ionic calcium is weighed and stored by a preset amount, and 1 to 5 g of water-soluble ions per 1000 ml of water Mixing and dissolving calcium to prepare a water-soluble ionic calcium culture solution (S100);
10 kg of any one raw material of ginseng fruit, red ginseng, hwangchil tree, jibuja, bellflower, elm, centella asiatica, japonica and omija and 20L of the water-soluble ionic calcium culture solution prepared in the water-soluble ionic calcium culture solution preparation step (S100) were mixed at 55 ° C. bathing step (S200) of bathing in a furnace for 24 hours;
A heating step (S300) of heating the mixture that has undergone the hot water step (S200) at 100 to 120°C for 10 hours;
a concentration step (S400) of concentrating the mixture under reduced pressure after the heating step (S300);
Drinking water manufacturing step (S500) of mixing 30ml-50ml of the concentrated solution concentrated in the concentration step (S400) with 1L of the water-soluble ionic calcium culture solution prepared in the water-soluble ionic calcium culture solution production step (S100) (S500); A method for producing drinking water using a natural material concentrate concentrated with a water-soluble ionic calcium culture solution, characterized in that comprising:

Images