KR20210041218A - Shampoo composition for preventing hair loss using the abeliophyllum extract from natural and manufacturing method thereof - Google Patents

Abstract

The present invention relates to production of a shampoo composition for preventing hair loss by using an extract of Abeliophyllum distichum Nakai. In the composition, an Abeliophyllum distichum Nakai immersion obtained by immersion-extraction after mixing at least one among flowers, leaves, and branches of Abeliophyllum distichum Nakai is included in 100±5% wt%, and an Abeliophyllum distichum Nakai reflux obtained by reflux-extraction after mixing at least one among flowers, leaves, and branches of Abeliophyllum distichum Nakai is included in 100±5% wt%. Each of the Abeliophyllum distichum Nakai immersion and reflux is included in a weight of about 1-10%, and a shampoo liquid base is included as a remainder in an amount of about 90-99 wt% with respect to the total weight of the composition. Accordingly, active ingredients of an Abeliophyllum distichum Nakai extract can be effectively extracted, and a shampoo composition useful to prevent hair loss can be produced. Thus, by activating antibacterial and antioxidant power, it is possible to effectively clean impurities from the scalp, and to protect the scalp and secure elasticity in damaged pores while keeping hair healthy. Moreover, it is possible to effectively cope with hair loss, weak hair from menopause, or large changes in hair caused by hormonal changes and stress. According to the present invention, effects of preventing hair loss and promoting hair health and hair growth can be provided.

Description

A shampoo composition for preventing hair loss using the extract of natural natural resources from natural wood, and a method for manufacturing the same. [Shampoo composition for preventing hair loss using the abeliophyllum extract from natural and manufacturing method thereof]

The present invention relates to a shampoo composition for preventing hair loss using an extract of Miseon tree, and in particular, a shampoo composition that is useful for preventing hair loss by effectively extracting the active ingredient of the extract of Miseon tree is prepared, and then by activating the antibacterial and antioxidant power through this, impurities of the scalp It effectively cleans and keeps the hair healthy, protects the scalp, provides firm elasticity to damaged pores, and prevents hair loss by effectively coping with large changes in hair caused by hair loss or menopausal weak hair or hormonal changes and stress. The present invention relates to a shampoo composition for preventing hair loss and a method of manufacturing the same, using an extract of natural resource Misun tree derived from nature that seeks to promote wool and hair growth.

In general, hair has a function of absorbing and discharging heavy metals such as arsenic, mercury, and zinc, which are unnecessary to the body, while protecting the human body from external stimuli such as buffering action from external shocks and UV-blocking cold friction.

Therefore, in recent years, in order to maintain the cleanliness while maintaining such hair in a healthy state, various effects such as dandruff removal, itching-preventing scalp and hair moisturizing effect, fat cyst prevention effect, hair cracking nodule prevention effect, tangle prevention effect, etc. A lot of functional shampoos have been developed.

In general, healthy males usually have around 100,000 hairs, and females usually have about 120,000 hairs.These hairs are grown and deteriorated in the process of growing → resting → depilatory, while each hair is roughly It has a lifespan of about 1,000 days. Of these 100,000 hairs, about 80-90% maintains a growth phase that lasts about 1,000 days, and the rest of the hair is in a resting state that lasts about 100 days, and then depilates. New hairs are formed in the area where the hair has been depilated. However, due to the problem of not generating new hair in the area where the hair is lost, efforts to determine the cause of alopecia have been continued, and treatment and research according to this have been variously continued from ancient times to the present.

As an example, according to Korean Patent Registration No. 10-1310970,'Hwangryeon, Hwangbaek, Golden, Hwangjeong, Astragalus, White Paper, Yamsanhwa, Licorice, and Ginger are mixed and extracted to prevent hair loss.

The herbal extracts for preventing hair loss include a first herbal extract for preventing hair loss prepared by mixing and extracting Coptis Coptis, Hwangbaek, Golden, Hwangjeong, Astragalus, Baekji, Yamukhwa, Licorice, and Ginger; And a second herbal extract for preventing hair loss, which is prepared by mixing and extracting Gogwa, germinated Seomoktae, Pyeonbaekyeop, Dangsam, Angelicae, blueberry, Sangbaekpi, Naryeoncho, Daylily, Rehmannia, Red ginseng, Hasuoh, Mokdanpi, Hyeonggae, Ubangja As a result, anti-inflammatory and antioxidant effects may occur, but there is a problem in that the sterilizing power is poor.

As another example, according to Korean Patent Application Laid-Open No. 10-2015-0010691,'Korean herbal medicine for preventing hair loss for skin and scalp protection, characterized in that it contains'Houichow extract, Coptis chinensis extract, Ginseng extract, Peony extract, Peony extract and Sewage extract. It presents'cosmetic composition'.

The herbal cosmetic composition for preventing hair loss for skin and scalp protection is a composition containing Houicho extract, Coptis chinensis extract, Ginseng extract, Peony extract, Peony extract and Sewage extract, which may also produce antioxidant effects, but is weak in anti-inflammatory and sterilizing power. There was this.

KR 10-1310970 B1 (2013.09.12.) KR 10-1661245 B1 (2016.09.23.)

Accordingly, the present inventors have comprehensively considered the above-described matters and focus on solving the limitations and problems of the existing herbal extracts for preventing hair loss, activating antibacterial and antioxidant power, effectively cleaning the scalp impurities and maintaining the hair healthy. As a result, the present invention was invented as a result of continuous research with great efforts to develop a shampoo for preventing hair loss using new natural resources that can protect the scalp and provide firm elasticity to damaged pores.

Therefore, the technical problem and object to be solved by the present invention is to create a shampoo composition that is useful for preventing hair loss by effectively extracting the active ingredient from the extract of Serrata, and then by activating the antibacterial and antioxidant power, effectively cleaning the scalp impurities and It protects the scalp while keeping it healthy and provides firm elasticity to damaged pores, and effectively prevents hair loss and promotes wool and hair growth by effectively coping with large changes in hair caused by hair loss or menopausal powerless hair or hormonal changes and stress. It is to provide a shampoo composition for preventing hair loss and a method of manufacturing the same, using the extract of natural resources derived from nature.

Here, the technical problems and objects to be solved by the present invention are not limited to the technical problems and objects mentioned above, and other technical problems and objects that are not mentioned will be clearly understood by those skilled in the art from the following description.

In the shampoo composition for preventing hair loss using the extract of natural resource Miseon tree according to the present invention for achieving the above object, in forming a shampoo composition for preventing hair loss using the extract of Miseon tree: Among the flower leaf branches of Miseon tree , Consisting of 100±5% by weight of the immersion-extracted Miseon tree immersion by mixing at least one or more; It is made in a state of 100±5% by weight of the reflux extracted by mixing at least any one or more of the flowering leaf branches of the serrata; Containing a shampoo liquid base containing about 1-10% by weight of the Miseon tree soaked material and reflux material, and contained in an amount of about 90-99% by weight based on the total weight of the composition in the balance. It is characterized by that.

At this time, the Miseon tree soaking material was freeze-dried by separating each flower leaf branch of Miseon tree, and 300 ml of each extraction solvent (water, 50% alcohol, 70% alcohol, 100% alcohol) in 50 g of each sample It is characterized in that the extraction was added by stirring and immersion for 3 days.

In addition, the reflux of Miseon tree was freeze-dried by separating each flower leaf branch of Miseon tree, and 300 ml of each extraction solvent (water, 50% alcohol, 70% alcohol, 100% alcohol) in 50 g of each sample After the addition, it is characterized in that the extraction for 4 hours at a temperature of about 100 °C in a reflux extractor.

In addition, the Miseon tree soaked material and the Miseon tree reflux are mixed at a ratio of 1:1, filtered, concentrated under reduced pressure, and freeze-dried to form powder.

In addition, the manufacturing method of the shampoo composition for preventing hair loss using the extract of natural natural resources of the present invention for achieving the above object is extracted after adding water to a mixture of leaves, branches, and flowers of Miseon trees. It is characterized by manufacturing.

At this time, the method for producing a shampoo composition for preventing hair loss using the extract of natural natural resources of the present invention includes a mixture of leaves, branches, and flowers in a weight ratio of 16-22:12-17:15-20. It is characterized in that it is prepared by adding 2000-4000 mL of water to -60 g and then extracting for 4-8 hours at 90-100°C.

As described above, the present invention provides a shampoo composition useful for preventing hair loss by effectively extracting the active ingredient from the extract of Misen tree, and then by activating the antibacterial and antioxidant power to effectively clean the scalp impurities and keep the hair healthy while maintaining the scalp. It has the effect of protecting and providing firm elasticity to damaged pores.

In addition, the present invention has the effect of preventing hair loss and promoting hair growth with wool by effectively coping with large changes in hair due to hair loss or menopausal powerless hair or hormonal changes and stress.

1 is a view showing the results of the wool strength test of the extract of Misun tree,
Figure 2 is a view showing the results of growth of hair growth of Miseon tree extract,
Figure 3 is a view showing the results of the wool experiment of the Misun tree extract,
Figure 4 is a graph showing the results when mixed with Misun tree extract and minoxidil,
Figure 5 is a view showing the experimental results when mixed with Misun tree extract and minoxidil,
Figure 6 is a view showing the hair protection effect of Misun tree extract.

Hereinafter, an embodiment of a shampoo composition for preventing hair loss and a method of manufacturing the same using the extract of natural natural resources of the present invention will be described in detail with reference to the drawings. The embodiments described below are provided to completely inform a person of ordinary skill in the scope of the invention, and the present invention is not limited to the embodiments disclosed below and may be implemented in various forms.

Specific specific matters are shown in the following description, which are provided to help a more general understanding of the present invention, and are not intended to limit the present invention to specific embodiments, and all modifications included in the spirit and scope of the present invention It should be understood to include equivalents or substitutes. In describing the present invention, when it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the subject matter of the present invention, a detailed description thereof will be omitted.

Unless otherwise defined, all terms used herein including technical or scientific terms have the same meaning as commonly understood by one of ordinary skill in the art to which the present invention belongs. Terms as defined in a commonly used dictionary are defined in consideration of functions in the present invention, which should be interpreted as concepts consistent with the technical idea of the present invention and meanings commonly or commonly recognized in the art. And, unless explicitly defined in the present application, it is not interpreted as an ideal or excessively formal meaning.

The present invention relates to a shampoo composition for preventing hair loss and a method of manufacturing the same using the extract of natural natural resources, and a shampoo composition that is useful for preventing hair loss by effectively extracting the active ingredient of the extract, and then antibacterial and antioxidant power through it. It effectively cleans the scalp impurities and keeps the hair healthy, protects the scalp, provides elasticity to damaged pores, and is also effective against major changes in hair due to hair loss or menopausal powerless hair or hormonal changes and stress. It provides a shampoo composition for preventing hair loss and a method of manufacturing the same, using a natural resource Misun tree extract, which seeks to prevent hair loss and promote wool and hair growth by making it possible to cope with it.

The present invention is made in the state of 100 ± 5% by weight of the immersion extract of the serrata by mixing at least one or more of the flower leaf branches of Abeliophyllum. At this time, the above-described Miseon tree soaking material was freeze-dried by separating each flower leaf branch of Miseon tree, and each extraction solvent (water, 50% alcohol, 70% alcohol, 100% alcohol) 300 It is characterized by adding ml, stirring and immersing for 3 days to extract. In the case of such a serrata immersion, the branch of flowers is freeze-dried, and then extracted by stirring and immersing by adding 300 ml of an extraction solvent per 50 g of a sample. As an extraction solvent, use 50% water and 70% alcohol and 100% alcohol. It can be divided and mixed, and water means natural water such as tap water or ground water. In addition, the extraction solvent used for the extraction of the serrata immersion material brings about a difference in sterilization power, and since additional functions can be added using not only the above extraction solvent but also other extraction solvents, when using another extraction solvent, substantially It is obvious to those skilled in the art that extracts exhibiting the same effect can be obtained.

In addition, the present invention is made in a state of 100 ± 5% by weight of the reflux extracted by mixing at least any one or more of the flower leaf branches of the Miseon tree. At this time, the reflux of Miseon tree was freeze-dried by separating each flower leaf branch of Miseon tree, and 300 ml of each extraction solvent (water, 50% alcohol, 70% alcohol, 100% alcohol) in 50 g of each sample Is added, and extracted for 4 hours at a temperature of about 100° C. in a reflux extractor. In the case of the reflux of Miseon trees, after freeze-drying the branches of flowers and leaves of the Miseon trees like the extract, 300 ml of the extraction solvent per 50 g of the sample is added and extracted through a reflux extractor.

The antimicrobial activity of each part of the Misun tree was tested using the Disc diffusion assay method for each part of the Misun tree (flower leaf branch). MHA was used as the used medium, and the strain used for the measurement of antibacterial activity was Escherichia coil, Propionibacterium acnes and Candida albicans. In addition, a 6mm paper disc was immersed in the extract of the Misun tree, that is, the immersion extract of leaves 0, 50, 70, 100%, the reflux extract of the flower 50, 70, 100%, and the immersion extract of the flower 0, 50, 70, 100%. As a result of measuring the antimicrobial activity of microorganisms over time, the flower showed the best condition. That is, as a result of testing the antibacterial activity of the branches of the flower leaves of the Miseon tree, it is considered that the use of the flowers of the Miseon tree is the most suitable, but is not limited thereto.

In addition, as a result of evaluating the antimicrobial activity of each extraction solvent (water, 50% alcohol, 70% alcohol, 100% alcohol) using immersion and reflux, the higher the concentration of the extraction solvent, the better the antibacterial activity. , The antimicrobial activity of reflux was better than that of immersion.

Table 1 below summarizes the experimental results to find out the difference in antibacterial activity for each part of the Miseon tree.

The woolen power test was performed through the extract (soaked water and refluxed water), and it is shown in FIG. 1. 1 is a view showing the results of the hair strength test of the extract of Miseon tree, in the experimental group to which the extract of Miseon tree (soaked and refluxed material) was applied showed more effect than minoxidil, and in particular, after 14 days of percutaneous skin, the wool was rapidly increased. It can be seen that it is expressed.

FIG. 2 is a view showing the results of hair growth of Miseon tree extract. As shown in FIG. 2, PCR was confirmed in mice coated with minoxidil (M) and Miseon tree extract (T) to hair loss-causing C57BL mice, IGF- 1 All expressions were remarkably high, and it was found that the expression rate of IGF-1 was rapidly increased when 21 days were used in the experimental group to which Misun tree extract (soaked water and refluxed material) was applied. It was confirmed that the expression rate of IGF-1 was increased to effectively act on hair growth.

FIG. 3 is a view showing the results of a wool experiment of the Miseon tree extract, as shown in FIG. 3, as a result of removing the hair of a healthy mouse and applying minoxidil and Miseon tree extracts, hair growth compared to the comparison group on the 15th day Was found to be more excellent, and it was confirmed that there was no difference in comparison with minoxidil.

In addition, the present invention further comprises a shampoo liquid base containing 1-10% by weight of the soak and reflux material, and the remaining amount is 90-99% by weight based on the total weight of the composition. The shampoo composition for preventing hair loss according to the present invention is completed by mixing the above-described immersion material, reflux material, and a known shampoo liquid base.

Figure 4 is a graph showing the results when mixed with the Miseon tree extract and minoxidil, as shown in Figure 4, when the Miseon tree extract (immersion and reflux) is used in combination with minoxidil, the function of hair growth is doubled. The ideal effect could be obtained.

FIG. 5 is a diagram showing the experimental results when mixed with Miseon tree extract and minoxidil. As shown in FIG. 5, a mixture of Miseon tree extract (immersion and reflux) and minoxidil was applied for 21 days, and then mouse hair root tissue As a result of staining and dissecting, it was confirmed that the formation of Laminin5 was very well as shown in the photo of FIG. 5, and accordingly, the formation of Laminin5 can be expected to prevent the hair from falling out longer, and a lot of collagen4 in the hair follicle cells is formed. You can see that it makes you even more healthy.

6 is a view showing the hair protection effect of the Miseon tree extract, and when applying the Miseon tree extract (immersion and reflux) to the hair as shown in FIG. 6, the stratum corneum through the strong antioxidant effect of the Miseon tree extract You can see the result of covering the outside and protecting the hair.

At this time, the Miseon tree immersion material and the Miseon tree reflux are mixed at a ratio of 1:1, filtered, concentrated under reduced pressure, freeze-dried, and powdered. After mixing the soaked water and reflux water, filtered through a filter, freeze-dried and powdered, so that they are smoothly accommodated in a known shampoo base and naturally melted once or twice a day. When used once, it is possible to obtain an effective feeling of shampoo, such as not only preventing hair loss and implementing wool functions, but also removing dead skin cells by washing.

According to the present invention, the active ingredient of the extract of Misen tree is effectively extracted to form a shampoo composition useful for preventing hair loss, and through this, antibacterial and antioxidant power is activated to effectively cleanse impurities of the scalp and protect the scalp while maintaining healthy hair. In addition to bringing firm elasticity to damaged pores, it provides the effect of pursuing hair loss prevention and promotion of wool and hair growth by effectively coping with large changes in hair due to hair loss or menopausal powerless hair or hormonal changes and stress. do.

The method for preparing a shampoo composition for preventing hair loss using the extract of natural natural resources of the present invention includes the steps of: (a) preparing a natural extract by adding water to the leaves, branches, and flowers of Miseon trees and then extracting; (b) adding and dissolving menthol to purified water, adding a thickener to dissolve it, and adding a decoction of herbal medicine to prepare a mixture; (c) adding and mixing a surfactant to the mixture prepared in step (b); (b) In the mixed mixture of step (c), the natural extract of step (a), henna extract, rosemary extract, espinozilia extract, nettle extract, chamomile extract, iris extract, keratin, natural betaine, D- Adding and mixing panthenol and silkamino acid; And (e) adding a natural essential oil and a preservative to the mixed mixture of step (d) and then mixing the mixture.

In the method for producing a shampoo composition for preventing hair loss using the extract of natural natural resource Miseon tree according to the present invention, the herbal decoction of the step (b) is specifically Gamguk 200-300 g, swastika 80-120 g, cypress leaves 160-240 g, Cheongung 80-120 g, Baekji 40-60 g, Sesin 40-60 g, Sangbaekpi 80-120 g, Hannyeoncho 80-120g, Black beans 80-120 g, Gojija 160-240 g, Pine needles 160- It can be prepared by adding 8-12 L of purified water to a herbal medicine mixture of 240 g, 80-120 g of angelica, 80-120 g of hasuoh and 40-60 g of ginseng powder, and extracting it at 80-100° C. for 4-8 hours, and further Specifically, 250 g of Gamguk, 100 g of swastika, 200 g of cypress leaves, 100 g of cheonggung, 50 g of white paper, 50 g of sesin, 100 g of Sangbaek, 100 g of nasturtium, 100 g of black beans, 200 g of gojija, 200 g of pine needles, It can be prepared by adding 10 L of purified water to a herbal medicine containing 100 g of angelica angelica, 100 g of sewage and 50 g of ginseng powder, and extracting it at 100°C for 6 hours.

In addition, in the method for producing a shampoo composition for preventing hair loss using the extract of natural natural resources of the present invention, the thickener in step (b) may be polyquaternium and glucamate, The surfactant of step (c) may be disodium laureth sulfosuccinate (LES) and coco-betaine, and the natural essential oil of step (e) is rosemary essential oil, peppermint essential oil, lavender essential oil, It may be tea tree essential oil and cedarwood essential oil, but is not limited thereto.

Hereinafter, the present invention will be described in detail by examples. However, the following examples are only illustrative of the present invention, and the contents of the present invention are not limited to the following examples.

Preparation Example 1: Preparation of natural extract for preventing hair loss

To a mixture of 17.6 g of Miseon tree leaves, 14.6 g of Miseon tree branches, and 19.2 g of Miseon tree flowers was added 3 L of purified water, extracted for 6 hours at 100° C., and filtered to prepare a mixed extract.

Preparation Example 2: Preparation of shampoo for preventing hair loss

(a) 250 g of Gamguk, 100 g of swastika, 200 g of cypress leaves, 100 g of cheonggung, 50 g of white paper, 50 g of sesin, 100 g of Sangbaekpi, 100 g of nasturtium, 100 g of black beans, 200 g of wolfberry, 200 g of pine needles, Angelicae 100 g, 100 g of sewage and 50 g of ginseng powder, 10 L of purified water was added to 14 herbal medicinal herbs, and then marinated at 100° C. for 6 hours, and then filtered to prepare a decoction of herbal medicinal herbs.

(b) After dissolving by adding menthol to purified water at 60°C, polyquaternium and glucamate are added to dissolve it, and the herbal decoction prepared in step (a) above Was added. Then, disodium laureth sulfosuccinate (LES) and coco-betaine were added and mixed.

(c) Henna extract, rosemary extract, espinosilla extract, nettle extract, chamomile extract, iris extract, keratin, natural betaine in the mixture of step (b) ), D-panthenol and silk amino acid were added, and the mixed extract prepared in Preparation Example 1 was mixed thereto.

(d) Rosemary essential oil, peppermint essential oil, lavender essential oil, tea tree essential oil, cedarwood essential oil, and a preservative were added to the mixture of step (c) and mixed.

Meanwhile, in the detailed description of the present invention, although it has been specifically described with reference to a preferred embodiment referenced by the accompanying drawings, various modifications are possible without departing from the scope of the present invention. Therefore, the scope of the present invention is limited to the described embodiments and should not be defined, and should be defined by the scope of the claims and equivalents as well as the scope of the claims to be described later.

Claims (6)

In forming the shampoo composition for preventing hair loss by using the extract of Miseon tree: 100±5% by weight of the dip extracted by mixing at least one or more of the flower leaf branches of Miseon tree;
It is made in a state of 100±5% by weight of the reflux extracted by mixing at least any one or more of the flower leaf branches of the Misun tree;
Containing a shampoo liquid base containing about 1-10% by weight of the Misun immersion and reflux material, and containing about 90-99% by weight based on the total weight of the composition in the balance. A shampoo composition for preventing hair loss using an extract of natural natural resources from natural sources, characterized in that.
The method of claim 1,
As for the Miseon tree soaking material, 300 ml of each extraction solvent (water, 50% alcohol, 70% alcohol, 100% alcohol) was added to 50 g of each sample by separating and freeze-drying the flower and leaf branches of the Miseon tree. A shampoo composition for preventing hair loss using a natural natural resource Misun tree extract, which is extracted by stirring and immersing for 3 days.
The method of claim 1,
As for the reflux of Miseon trees, separate and freeze-dried branches of flowers and leaves of Miseon trees, and 300 ml of each extraction solvent (water, 50% alcohol, 70% alcohol, 100% alcohol) were added to 50 g of each sample. After that, a shampoo composition for preventing hair loss using a natural natural resource Miseon tree extract, which is extracted for 4 hours at a temperature of about 100° C. in a reflux extractor.
The method of claim 1,
The shampoo composition for preventing hair loss using a natural natural resource Miseon tree extract, characterized in that the Miseon tree soaked material and the Miseon tree reflux are mixed at a ratio of 1:1, filtered, concentrated under reduced pressure, and freeze-dried to powder.
A method for producing a shampoo composition for preventing hair loss using a natural resource extract of misun tree, characterized in that it is prepared by extracting after adding water to a mixture of leaves, branches, and flowers.
The method of claim 5,
After adding 2000-4000 mL of water to 40-60 g of a mixture of leaves, branches, and flowers in the ratio of 16-22:12-17:15-20 by weight, extraction at 90-100℃ for 4-8 hours A method for producing a shampoo composition for preventing hair loss using the extract of natural natural resources of the natural origin, characterized in that produced by.

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