KR20200094887A - Manufacture method of a persimmon tannin dye and Dyeing method using fabric - Google Patents

Manufacture method of a persimmon tannin dye and Dyeing method using fabric Download PDF

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KR20200094887A
KR20200094887A KR1020190012155A KR20190012155A KR20200094887A KR 20200094887 A KR20200094887 A KR 20200094887A KR 1020190012155 A KR1020190012155 A KR 1020190012155A KR 20190012155 A KR20190012155 A KR 20190012155A KR 20200094887 A KR20200094887 A KR 20200094887A
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dyeing
fabric
persimmon
natural
natural dye
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KR1020190012155A
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Korean (ko)
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여현숙
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동성실업(주)
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/20Physical treatments affecting dyeing, e.g. ultrasonic or electric
    • D06P5/2066Thermic treatments of textile materials
    • D06P5/2077Thermic treatments of textile materials after dyeing

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  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

The present invention relates to a complex dyeing method for a fabric using natural dyestuff to appeal to customers with a high quality product. According to the present invention, the complex dyeing method using natural dyestuff comprises: a natural dyestuff preparation step of preparing persimmon dyestuff powder and sweet laver dyestuff powder; a refining step; a first dyeing step of performing persimmon dyeing and drying work; a second dyeing step of inputting fabric completing the first dyeing step in a sweet laver dyeing solution to perform sweet laver dyeing and drying work of the fabric completing sweet laver dyeing in a place where it is shaded and ventilated well; and a post-treatment step of washing the fabric, dehydrating the washed fabric, and drying the dehydrated fabric in a place where it is shaded and ventilated well.

Description

천연염료를 활용한 복합염색방법{Manufacture method of a persimmon tannin dye and Dyeing method using fabric}Complex dyeing method using natural dyes {Manufacture method of a persimmon tannin dye and Dyeing method using fabric}

일반적으로 천연 염색이란 식물성, 동물성 또는 광물성 염료를 이용하여 직물에 색깔을 입히는 작업과정을 말한In general, natural dyeing refers to the process of coloring fabrics using vegetable, animal or mineral dyes.

다. 이러한 천연 염색의 특징은 화학 염료에 비하여 색상의 채도가 높지 않고, 친환경적이며 그리고 인체 친화All. The characteristics of these natural dyes are that the color is not saturated compared to chemical dyes, is eco-friendly, and is human-friendly.

적인 요소가 많다.There are many elements.

[0003] 천연 염색은 합성 염료를 사용한 염색에 비하여 색상이 자연스럽고, 심미성이 뛰어나며 합성 염료를 사용할 때[0003] Natural dyeing has a natural color and excellent aesthetics compared to dyeing using synthetic dyes, and when using synthetic dyes

부수되는 폐수, 악취 등의 문제가 발생하지 않고 환경에 대한 친화성을 가진다는 장점을 가지고 있다.It has the advantage of being friendly to the environment without causing problems such as incidental wastewater and odor.

[0004] 천연 염색에 재료로서 사용된 것으로는 맥주 슬러지, 오동나무 수피, 포도껍질, 머루 껍질 등 다양한 천연재료[0004] A variety of natural materials such as beer sludge, paulownia bark, grape skin, wild grape skin, etc. used as materials for natural dyeing

가 사용되고 있다.Is being used.

[0005] 그러나 천연 염색은 일반적으로 일광(햇빛), 세탁, 땀, 드라이클리닝 등에 대한 견뢰도가 높지 않아 얼룩이나[0005] However, natural dyeing generally does not have high fastness to sunlight (sunlight), washing, sweat, dry cleaning, etc.

탈색이 발생하기 쉬운 문제점을 가지고 있다.It has a problem that discoloration is likely to occur.

[0006] 한편, 천연염색염료가 사용되는 감물은 덜 익은 감에서 나는 즙으로서 염료나 방부제로 쓰이고 있으며, 일반적[0006] On the other hand, persimmons in which natural dyes are used are juices from unripe persimmons and are used as dyes or preservatives, and are generally

으로 감물염색은 고려시대부터 제주의 민속의상인 갈옷에 사용되어 왔으며 염료가 되는 감은 타닌성분을 많이Since the Goryeo Dynasty, persimmon dyeing has been used in gal clothes, a folk costume of Jeju, and persimmons used as dyes contain a lot of tannins.

함유하고 있고 색소가 풍부한 7-8월경에 채취한 토종 풋감이 이용되며, 염색의 기본 원리는 풋감의 타닌성분이Native green persimmon collected around July-August, which contains and rich in pigments, is used, and the basic principle of dyeing is the tannin component of green persimmon.

섬유와 결합하여 응고되면서 섬유를 빳빳하게 만드는 성질과 감물로 염색된 섬유를 햇빛에 노출시키면 산화중첩It combines with the fiber and solidifies, making the fiber stiff, and when the fiber dyed with persimmon is exposed to sunlight, it overlaps with oxidation.

이 되면서 짙은 갈색(褐色)으로 변하는 것이다.As it becomes, it turns to dark brown (褐色).

[0007] 그러나 이러한 전통적인 천연감물염색 방법은 염색 후 색바램 현상과 물세탁시 물빠짐 현상이 단점으로 지적되However, these traditional natural persimmon dyeing methods are pointed out as disadvantages of fading after dyeing and fading during washing with water.

어왔다.Came.

본 발명은 토종 풋감 및 감태를 분쇄시켜 여과과정을 거쳐 동결건조한 후 분말화시켜 천연분말염료로 각각 제조In the present invention, native green persimmons and Ecklonia cava are pulverized, filtered, freeze-dried, and then powdered to prepare natural powder dyes.

한 후 순차적으로 원단을 염색함으로서 천연자원으로만 염색염료가 이루어져 환경호르몬이나 유해물질이 함유되After that, by sequentially dyeing the fabric, dyeing dyes are made only from natural resources and contain environmental hormones or harmful substances.

지 않아 환경성 질병을 방지하는 천연염료를 이용한 원단의 복합염색방법원단의 복합염색방법을 제공하는 데 그It provides a complex dyeing method for fabrics using natural dyes that prevent environmental diseases.

목적이 있다.There is a purpose.

전술한 바와 같이 본 발명에 따르면, 화학성분이 전혀 포함하지 않은 풋감 및 감태와 같은 염색염료로 하여금As described above, according to the present invention, dyeing dyes such as green sensation and Ecklonia that do not contain any chemical components

1, 2염색단계가 수행되어 원단에 환경호르몬이나 유해물질이 함유되지 않아 아토피와 같은 환경성 질병을 유발1st and 2nd dyeing steps are performed to cause environmental diseases such as atopy as the fabric does not contain environmental hormones or harmful substances.

하지 않는 원단을 제공하여 인체친화형 제품을 생산할 수 있어 새로운 부가가치를 창출할 수 있는 효과와 더불By providing fabric that is not used, it is possible to produce human-friendly products, which can create new added value.

어 제1염색단계에서는 감물천연염료, 제2염색단계에서는 감태천연염료를 순차적으로 이용하여 염색함으로서 원In the first dyeing step, persimmon natural dye, and in the second dyeing step, persimmon natural dye are used sequentially.

단에 이중으로 염색작업이 수행되어 자연적이면서도 미려한 색상으로 염색이 이루어져 소비자에서 고품질의 제Dyeing is performed twice on the hem, so that it is dyed in natural and beautiful colors.

품으로 어필할 수 있는 효과가 있다.It has an effect that can appeal to you.

[0014] 또한 정련단계에서 사용되는 정련제로 하여금 제1, 2염색단계 전에 원단의 불순물을 용이하게 제거할 뿐 아니라[0014] In addition, the refining agent used in the refining step not only easily removes impurities from the fabric before the first and second dyeing steps

제1, 2염색단계를 용이하게 수행할 수 있도록 원단의 물성을 유지시켜 작업의 편의성을 향상시킬 수 있는 효과The effect of improving the convenience of work by maintaining the physical properties of the fabric so that the first and second dyeing steps can be easily performed.

가 있다.There is.

[0015] 또한 천연자원인 감물과 감태를 사용하여 감물천연염료분말과 감태천연염료분말을 제조함으로서 제주산 감과 감In addition, by using natural resources, persimmon and persimmon, persimmon natural dye powder and persimmon natural dye powder and persimmon from Jeju

태의 소비를 촉진시켜 농어촌 소득증대에 기여할 수 있으면서도 천연염료 자체를 상품화할 수 있게 되어 천연염Natural salts can contribute to the increase of income in farming and fishing villages by promoting the consumption of fetuses, while also being able to commercialize natural dyes themselves.

색을 일반화하고 널리 보급할 수 있어 부가가치를 높일 수 있음과 동시에 감물, 감태염료를 분말화하여 휴대 또Color can be generalized and widely distributed to increase added value, and at the same time, persimmon and Ecklonia dye are powdered to

는 보관이 용이하여 때와 장소를 가리지 않고 사용이 가능하여 손쉽게 상용화가 구현되는 효과가 있다.Because it is easy to store, it can be used anytime and anywhere, so it has the effect of easy commercialization.

상기와 같은 목적을 달성하기 위하여, 본 발명은 감물천연염료분말와 감태천연염료분말을 각각 준비하는 천연염In order to achieve the above object, the present invention is a natural salt for preparing a persimmon natural dye powder and a persimmon natural dye powder, respectively

료준비단계; 염색하고자 하는 원단의 불순물을 제거한 후 45 ~ 55℃로 유지되는 온수에 25 ~ 35분 동안 삶은 후Preparation stage; After removing impurities from the fabric to be dyed, boil for 25 to 35 minutes in hot water maintained at 45 to 55°C.

2 ~ 3회 가량 수세하여 건조시키는 정련단계; 300 ~ 600메쉬로 이루어지는 메쉬체에 감물천연염료분말을 걸른후 걸러낸 감물천연염료분말을 상온의 물에 풀어 감물천연염료로 제조하고 제조된 감물천연염료에 원단을 넣어Refining step of washing and drying 2-3 times with water; After filtering the persimmon natural dye powder in a mesh made of 300 to 600 mesh, the filtered persimmon natural dye powder is dissolved in water at room temperature to make it into persimmon natural dye, and the fabric is added to the prepared persimmon natural dye.

감물염색 및 건조작업이 이루어지는 제1염색단계; 300 ~ 600메쉬로 이루어지는 메쉬체에 감태천연염료분말을 걸A first dyeing step in which persimmon dyeing and drying are performed; Ecklonia natural dye powder is applied to a mesh body made of 300 to 600 mesh.

른 후 걸러낸 감태천연염료분말을 60℃로 유지되는 물에 풀어 감태천연염료로 제조하고 제조된 감물천연염료에After rinsing, dissolve the filtered Ecklonia cava natural dye powder in water maintained at 60°C, and make it with Ecklonia Natural Dye.

제1염색단계를 거친 원단을 넣어 감태염색을 도모하고 감태염색 후 그늘지고 바람이 잘 통하는 장소에서 건조작Put the fabric that went through the first dyeing step to dye the Ecklonia cava, and then dry them in a shaded and well-ventilated place after Ecklonia dyeing.

업이 이루어지는 제2염색단계; 상기 제2염색단계를 거친 원단은 감태천연염료가 나오지 않을 때까지 수세하여A second dyeing step in which the business is performed; The fabric that has gone through the second dyeing step is washed with water until no natural Ecklonia dye comes out.

탈수한 후 그늘지고 바람이 잘 통하는 장소에서 건조시키는 후처리단계;로 이루어지는 천연염료를 이용한 원단Fabric using natural dyes consisting of: a post-treatment step of drying in a shady and airy place after dehydration

의 복합염색방법을 제공한다.It provides a complex dyeing method of.

그리고 상기 정련단계는 원단의 불순물을 제거하기 위해 정련제에 의해 정련작업이 [0010] 수행되며, 상기 정련제는 물And the refining step is a refining operation is performed by a refining agent to remove impurities from the fabric, the refining agent is water

5L, 산화호발제 10 ~ 15g, 알카리침투제 10 ~ 15g, 과산화수소수 20 ~ 35g, 과수안정제 10 ~ 20g, 유화분산제5L, Oxidation desizing agent 10 ~ 15g, Alkaline penetrant 10 ~ 15g, Hydrogen peroxide solution 20 ~ 35g, Fruit water stabilizer 10 ~ 20g, Emulsifying and dispersing agent

10 ~ 20g을 혼합한 것으로 이루어짐을 특징으로 한다.It is characterized by consisting of a mixture of 10 to 20g.

[0011] 상기 감물천연염료분말은, 7 ~ 8월경에 채취한 제주 토종 풋감의 꼭지와 씨를 제거하여 분쇄기에 넣고 분쇄하여[0011] The persimmon natural dye powder is pulverized by removing the stem and seeds of the Jeju native green persimmon collected around July to August, putting it in a grinder

감물의 원료를 준비하는 감물준비단계; 상기 감물준비단계에서 준비된 풋감 분쇄물과 물의 중량비율을 4 ~ 6 :Persimmon preparation step of preparing raw materials of persimmon; The weight ratio of the green persimmon pulverized product and water prepared in the persimmon preparation step is 4 to 6:

1로 혼합하여 액상의 혼합물로 제조하고 300 ~ 600메쉬로 이루어지는 메쉬체를 이용하여 여러차례 걸러주어 풋Mix in 1 to prepare a liquid mixture, and filter several times using a mesh sieve consisting of 300 to 600 mesh.

감 분쇄물 및 물이 혼합된 액상의 혼합물에 대한 고형분 및 이물질을 제거하는 혼합단계; 상기 혼합단계에서 고A mixing step of removing solids and foreign substances from the liquid mixture in which the persimmon pulverized product and water are mixed; High in the mixing step

형분이 제거된 혼합물을 2 ~ 0℃로 이루어지는 저온저장고에서 1 ~ 1시간 30분 동안 보관하여 보관하는 보관단A storage unit that stores the mixture from which the mold has been removed for 1 to 1 hour and 30 minutes in a low-temperature storage at 2 to 0℃

계; 상기 보관단계를 거친 혼합물을 300 ~ 600메쉬로 이루어지는 메쉬체를 이용하여 걸러준 후 -10 ~ -30℃의system; After filtering the mixture through the storage step using a mesh sieve consisting of 300 to 600 mesh,

온도에서 2 ~ 4시간 동안 동결건조시켜 혼합물을 분말화하는 분말단계;가 순차적으로 수행되어 제조됨을 특징으A powder step of lyophilizing the mixture by lyophilizing it for 2 to 4 hours at a temperature; characterized in that it is produced by sequentially performing

로 한다.Shall be

[0012] 상기 감태천연염료분말은, 제주 해안가에서 9 ~ 11월경의 성장한 감태를 채취하여 흐르는 물에 감태를 넣고 불[0012] The Ecklonia cava natural dye powder is obtained by collecting Ecklonia from September to November at the coast of Jeju, and putting Ecklonia in flowing water and fire

순물이 제거시키고 건조한 후 건조된 감태와 물을 1: 30의 중량비율로 혼합하여 용기에 90 ~ 120분 동안 90 ~After the pure water is removed and dried, the dried Ecklonia cava and water are mixed in a weight ratio of 1:30 and placed in a container for 90 to 120 minutes.

110℃로 가열하는 가열단계; 상기 가열단계를 거친 혼합물을 여과용 천이나 거름망에 여과시켜 감태염액을 추출Heating step of heating to 110 ℃; The mixture that has gone through the heating step is filtered through a filter cloth or a sieve to extract the salt solution

하는 감태염액추출단계; 상기 감태염액추출단계에서 추출된 감태염액을 상온에서 식힌 후 혼합물을 300 ~ 600메The extracting step of the salt solution; After cooling the Ecklonia cava salt solution extracted in the Ecklonia cava salt solution extraction step at room temperature,

쉬로 이루어지는 메쉬체를 이용하여 걸러준 후 0 ~ 2℃의 온도에서 2 ~ 4시간 동안 동결건조시켜 감태염액을 분After filtering with a mesh sieve made of sheath, freeze-drying at a temperature of 0 to 2℃ for 2 to 4 hours to separate

말화하는 분말단계;가 순차적으로 수행되어 제조됨을 특징으로 한다.Powder step of rolling; characterized in that it is produced by sequentially performing.

Claims (1)

감물천연염료분말와 감태천연염료분말을 각각 준비하는 천연염료준비단계(S1);
염색하고자 하는 원단의 불순물을 제거한 후 45 ~ 55℃로 유지되는 온수에 25 ~ 35분 동안 삶은 후 2 ~ 3회 가
량 수세하여 건조시키는 정련단계(S2);
300 ~ 600메쉬로 이루어지는 메쉬체에 감물천연염료분말을 걸른 후 걸러낸 감물천연염료분말을 상온의 물에 풀
어 감물천연염료로 제조하고 제조된 감물천연염료에 원단을 넣어 감물염색 및 건조작업이 이루어지는 제1염색단
계(S3);
300 ~ 600메쉬로 이루어지는 메쉬체에 감태천연염료분말을 걸른 후 걸러낸 감태천연염료분말을 60℃로 유
지되는 물에 풀어 감태천연염료로 제조하고 제조된 감물천연염료에 제1염색단계(S3)를 거친 원단을 넣어 감태염
색을 도모하고 감태염색 후 그늘지고 바람이 잘 통하는 장소에서 건조작업이 이루어지는 제2염색단계(S4);
상기 제2염색단계(S4)를 거친 원단은 감태천연염료가 나오지 않을 때까지 수세하여 탈수한 후 그늘지고 바람이
잘 통하는 장소에서 건조시키는 후처리단계(S5);
로 이루어지는 천연염료를 이용한 원단의 복합염색방법.
Natural dye preparation step (S1) of preparing persimmon natural dye powder and Ecklonia natural dye powder, respectively;
After removing impurities from the fabric to be dyed, boil for 25 to 35 minutes in hot water maintained at 45 to 55°C, and add 2 to 3 times.
Refining step of washing and drying the amount (S2);
After filtering the persimmon natural dye powder through a mesh sieve made of 300 ~ 600 mesh, paste the filtered persimmon natural dye powder into room temperature water.
The first dyeing group where persimmon dyeing and drying are performed by putting the fabric into the persimmon natural dye and then adding the fabric to the prepared persimmon natural dye.
System (S3);
After filtering the Ecklonia natural dye powder in a mesh sieve made of 300 ~ 600 mesh, the filtered Ecklonia Natural Dye Powder is oiled at 60℃.
Dissolved in water to be dissolved in Ecklonia cava natural dye and put the fabric that has undergone the first dyeing step (S3) to the manufactured persimmon natural dye
A second dyeing step (S4) in which a drying operation is performed in a shaded and well-ventilated place after the color scheme and the Ecklonia cava dyeing;
The fabric that has gone through the second dyeing step (S4) is washed with water until no natural Ecklonia dye comes out and dehydrated.
Post-treatment step (S5) of drying in a well-ventilated place;
Complex dyeing method of fabric using natural dyes consisting of.
KR1020190012155A 2019-01-30 2019-01-30 Manufacture method of a persimmon tannin dye and Dyeing method using fabric KR20200094887A (en)

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