KR20180064946A - Composition of Glaze and a manufacturing methods - Google Patents

Composition of Glaze and a manufacturing methods Download PDF

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Publication number
KR20180064946A
KR20180064946A KR1020160165437A KR20160165437A KR20180064946A KR 20180064946 A KR20180064946 A KR 20180064946A KR 1020160165437 A KR1020160165437 A KR 1020160165437A KR 20160165437 A KR20160165437 A KR 20160165437A KR 20180064946 A KR20180064946 A KR 20180064946A
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Prior art keywords
glaze
weight
kaolin
composition
glaze composition
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KR1020160165437A
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Korean (ko)
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김기홍
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김기홍
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    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
    • C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B14/00—Use of inorganic materials as fillers, e.g. pigments, for mortars, concrete or artificial stone; Treatment of inorganic materials specially adapted to enhance their filling properties in mortars, concrete or artificial stone
    • C04B14/02—Granular materials, e.g. microballoons
    • C04B14/04—Silica-rich materials; Silicates
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/32—Burning methods
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81—Coating or impregnation
    • C04B41/85—Coating or impregnation with inorganic materials
    • C04B41/86—Glazes; Cold glazes

Abstract

The present invention relates to a glaze composition which contains 3-6 wt% of manganese dioxide, 4 wt% of titanium, 6-7 wt% of zircon, and 4 wt% of bone ashes in addition to a glaze base which is composed of 50-55 wt% of feldspar, 13-15 wt% of dolomite, 24-27 wt% of silica, and 5-7 wt% of kaolin. When the glaze composition is used, it is possible to form spots and patterns in a wide color tone and background color.

Description

유약 조성물 및 제조 방법 {Composition of Glaze and a manufacturing methods}[0001] Glaze compositions and methods [0002]

본 발명은 유약 조성물 및 그 제조 방법에 관한 것으로, 보다 상세하게는 도자기 등의 세라믹 재질의 표면을 처리하기 위한 유약 조성물 및 그 제조 방법에 관한 것이다. The present invention relates to a glaze composition and a method for producing the glaze composition, and more particularly, to a glaze composition for treating a surface of a ceramic material, such as a ceramic, and a method of manufacturing the glaze composition.

일반적으로 유약이라 함은 도자기, 타일, 기와 등의 세라믹 재질을 성형하여 소성하기 전에 표면을 피복시키기 위해 사용하는 유리질 소재를 말한다. 상기 유약을 바르는 목적으로 표면의 광택을 주어 제품을 아름답게 하는 것 외에도 강도를 더하고 표면을 반질반질하게 하여 더러워지는 것을 방지하는 데 있다. Generally, glaze refers to a glassy material used to cover a surface of a ceramic material such as a ceramic, a tile, or a tile before molding and firing. In addition to making the product more beautiful by lustering the surface for the purpose of applying the glaze, it adds strength and prevents the surface from becoming dirty by making the surface smooth.

본 발명은 세라믹 재질의 표면에 밝은 베이지 색감의 배경색에서 갈색, 흑갈색까지 폭 넓은 배경색의 유약 조성물을 제공한다. The present invention provides a glaze composition having a broad background color ranging from a background color of light beige to a brown color and a blackish brown color on the surface of a ceramic material.

본 발명은 세라믹 재의 표면에 밝은 갈색부터 흑갈색과 검은색 계통의 반점 혹은 자연스러운 얼룩무늬 등의 형상을 형성하는 유약 조성물 제조 방법을 제공한다. The present invention provides a method of manufacturing a glaze composition which forms light brown to blackish brown and black spots or natural speckles on the surface of a ceramic material.

본 발명은 형석의 함유량과 가마의 상태에 따라 무광의 재질과 유광의 재질을 형성할 수 있게 해준다. 여기서 유광의 상태가 되면 겉면이 더 광이 나고 투명한 느낌을 주며, 무광의 상태가 되면 단아하고 은은한 색감을 주고 세척이 더 용이한 효과가 있다. The present invention makes it possible to form a matte material and a glossy material according to the content of fluorite and the condition of the kiln. In this case, the outer surface gives more light and transparent feeling, and when it is in a matte state, it is monochromatic and gives a soft color and it is easier to clean.

본 발명에 따른 유약 조성물은 장석 50 내지 55 중량 %, 백운석 13 내지 15 중량% 규석 24 내지 27 중량%, 카오린(카올린 혹은 고령토) 5 내지 7 중량% 으로 구성된 유약 베이스에 이산화 망간 3내지 내지6%, 티탄 4 중량 %, 지르콘 6 내지 7 중량 %, 골회 4 중량%을 포함한다. The glaze composition according to the present invention comprises 3 to 6% of manganese dioxide in a glaze base consisting of 50 to 55% by weight feldspar, 13 to 15% by weight of dolomite, 24 to 27% by weight of silica, and 5 to 7% by weight of kaolin (kaolin or kaolin) 4% by weight of titanium, 6 to 7% by weight of zircon, and 4% by weight of molybdenum.

본 발명에 따른 유약 조성물은 장석 50 내지 55 중량 %, 백운석 13 내지 15 중량% 규석 24 내지 27 중량%, 카오린(카올린 혹은 고령토) 5 내지 7 중량% 으로 구성된 유약 베이스에 이산화 망간 3내지 내지6%, 티탄 4 중량 %, 지르콘 6 내지 7 중량 %, 골회 4 중량%을 포함한 유약 조성물을 혼합하는 단계와 The glaze composition according to the present invention comprises 3 to 6% of manganese dioxide in a glaze base consisting of 50 to 55% by weight feldspar, 13 to 15% by weight of dolomite, 24 to 27% by weight of silica, and 5 to 7% by weight of kaolin (kaolin or kaolin) 4 wt% titanium, 6 to 7 wt% zircon, and 4 wt% molybdenum;

상기 혼합물과 물을 1 : 0.7 내지 1.1의 비율로 볼 밑에서 분쇄하는 단계 및 상기 분쇄된 혼합물과 물을 120 내지 150 메쉬의 체로 여과하는 단계를 포함할 수 있다.
Pulverizing the mixture and water at a ratio of 1: 0.7 to 1.1 under a ball, and filtering the pulverized mixture and water with a sieve of 120 to 150 mesh.

본 발명에 따르면, 세라믹 재의 표면에 각인하여 무늬를 형성하는 과정 없이 본 발명의 유약 조성물을 이용하여 상기 세라믹 재질의 표면에 밝은 갈색에서부터 흑갈색과 검정색 계통의 반점의 형상 또는 무늬를 기존보다 폭넓고 자연스레 형성할 수 있다. According to the present invention, by using the glaze composition of the present invention, the shape or pattern of light brown to black-brown and black-colored spots on the surface of the ceramic material is widened and natural .

상기 유약 조성물은 세라믹 재질의 표면에 밝은 갈색에서부터 흑갈색 검정색 계통의 반점의 형상 또는 무늬를 형성할 뿐만 아니라, 이와 대비되는 색감인 아이보리색 ~ 베이지색의 밝은 배경색에서 갈색, 흑갈색 재질의 폭넓은 배경색을 통해 폭넓은 선택 폭을 제공하여 대비 등을 통한 시각적 아름다운 효과를 극대화 시킬 수 있다. The glaze composition not only forms the shape or pattern of light brown to black-brown black spots on the surface of a ceramic material, but also forms a broad background color of brown and black brown materials in a light background color of ivory to beige, It offers a wide selection of colors to maximize the visual effects through contrast.

기존의 반점이 생기는 유약 조성물인 경우, 배경이 되는 부분이 갈색 ~ 흑갈색이나 남색, 검정색에 한정적이고 반점 또한 어두운 경우가 많았는데, 백운석, 지르콘, 골회 등을 사용하여 밝은 배경색과 반점 또는 무늬의 형상을 만듦으로써 이를 보완하였다.
In the case of a glaze composition in which existing spots are formed, the background portion is limited to brown to dark brown, indigo, and black, and the spots are also often dark. By using dolomite, zircon, To make up for this.

도1-1은 본 발명의 일 실시 예에 따른 유약 조성물을 이용하여 형성된 도자기 시편 컵과 시편에 대한 사진이다.
도2는 본 발명의 망간 함유량에 차이에 따라 배경색이 달라지는 실시 예에 따른 유약 조성물 색감이다.
도3은 본 유약이 제조되는 과정에서 사용되기의 과정을 나타낸 것이다.
도4는 본 유약이 제조되는 상세 과정이다.FIG. 1-1 is a photograph of a ceramic specimen cup and a specimen formed using the glaze composition according to an embodiment of the present invention.
FIG. 2 is a color chart of a glaze composition according to an embodiment in which the background color varies depending on the manganese content of the present invention.
FIG. 3 shows a process of being used in the process of manufacturing the glaze.
Fig. 4 is a detailed process for manufacturing the glaze.

본 발명에 따른 유약 조성물은 장석 50 내지 55 중량 %, 백운석 13 내지 15 중량% 규석 24 내지 27 중량%, 카오린(카올린 혹은 고령토) 5 내지 7 중량% 으로 구성된 유약 베이스에 이산화망간 3 내지 내지 6%, 티탄 4 중량%, 지르콘 6 내지 7 중량 %, 골회 4 중량%을 포함한 유약 조성물을 혼합하는 단계와 The glaze composition according to the present invention comprises 3 to 6% manganese dioxide in a glaze base consisting of 50 to 55% by weight of feldspar, 13 to 15% by weight of dolomite, 24 to 27% by weight of silica, and 5 to 7% by weight of kaolin (kaolin or kaolin) Mixing glaze compositions comprising 4 wt% titanium, 6 to 7 wt% zircon, and 4 wt%

상기 혼합물과 물을 1 : 0.7 내지 1.1의 비율로 볼 밑에서 분쇄하는 단계 및 상기 분쇄된 혼합물과 물을 120 내지 150 메쉬의 체로 여과하는 단계를 포함할 수 있다.
Pulverizing the mixture and water at a ratio of 1: 0.7 to 1.1 under a ball, and filtering the pulverized mixture and water with a sieve of 120 to 150 mesh.

위와 같이 많은 유약 조성물을 d2 (일반백자)나 d1 등의 백자 계통 혹은 슈퍼 화이트(슬립) 재질로 만든 초벌기에 시유하여 1240℃ 내지 1250℃의 가마 소송(재벌)을 하게 되면, 상기 유약 조성물을 입힌 도자기가 완성된다.
When a large number of glaze compositions are subjected to glaze processing (chaebol) at 1240 ° C to 1250 ° C by using a white glaze such as d2 (general white porcelain) or d1 or a super white (slip) material, The pottery is finished.

상기 유약 조성물에 형석 함유량이 많아질수록 도자기의 재질이 유광 -> 무광의 재질로 바뀐다.
As the content of fluoride increases in the glaze composition, the material of the ceramics is changed into a material of a glossy- >

상기 유약 조성물에 이산화망간 함유량을 높일수록 배경색이 짙은 갈색 계열이 된다.
The higher the manganese dioxide content in the glaze composition, the darker the background color.

℃ = 섭씨온도
% = percentC = Celsius temperature
% = percent

Claims (1)

본 발명에 따른 유약 조성물은 장석 50 내지 55 중량 %, 백운석 13 내지 15 중량% 규석 24 내지 27 중량%, 카오린(카올린 혹은 고령토) 5 내지 7 중량% 으로 구성된 유약 베이스에 이산화망간 3 내지 내지 6%, 티탄 4 중량%, 지르콘 6 내지 7 중량 %, 골회 4 중량%을 포함한 유약 조성물을 혼합하는 단계와
상기 혼합물과 물을 1 : 0.7 내지 1.1의 비율로 볼 밑에서 분쇄하는 단계 및 상기 분쇄된 혼합물과 물을 120 내지 150 메쉬의 체로 여과하는 단계를 포함할 수 있다.

위와 같이 많은 유약 조성물을 d2 (일반백자)나 d1 등의 백자 계통 혹은 슈퍼 화이트(슬립) 재질로 만든 초벌기에 시유하여 1240℃ 내지 1250℃의 가마 소송(재벌)을 하게 되면, 상기 유약 조성물을 입힌 도자기가 완성된다.
The glaze composition according to the present invention comprises 3 to 6% manganese dioxide in a glaze base consisting of 50 to 55% by weight of feldspar, 13 to 15% by weight of dolomite, 24 to 27% by weight of silica, and 5 to 7% by weight of kaolin (kaolin or kaolin) Mixing glaze compositions comprising 4 wt% titanium, 6 to 7 wt% zircon, and 4 wt%
Pulverizing the mixture and water at a ratio of 1: 0.7 to 1.1 under a ball, and filtering the pulverized mixture and water with a sieve of 120 to 150 mesh.

When a large number of glaze compositions are subjected to glaze processing (chaebol) at 1240 ° C to 1250 ° C by using a white glaze such as d2 (general white porcelain) or d1 or a super white (slip) material, The pottery is finished.
KR1020160165437A 2016-12-06 2016-12-06 Composition of Glaze and a manufacturing methods KR20180064946A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110627361A (en) * 2019-11-04 2019-12-31 佛山市东鹏陶瓷有限公司 Low-zirconium white glaze for sanitary ceramics and preparation process thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110627361A (en) * 2019-11-04 2019-12-31 佛山市东鹏陶瓷有限公司 Low-zirconium white glaze for sanitary ceramics and preparation process thereof
CN110627361B (en) * 2019-11-04 2022-04-15 佛山市东鹏陶瓷有限公司 Low-zirconium white glaze for sanitary ceramics and preparation process thereof

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