KR20180053933A - Baked makeup cosmetic composition - Google Patents
Baked makeup cosmetic composition Download PDFInfo
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- KR20180053933A KR20180053933A KR1020160151105A KR20160151105A KR20180053933A KR 20180053933 A KR20180053933 A KR 20180053933A KR 1020160151105 A KR1020160151105 A KR 1020160151105A KR 20160151105 A KR20160151105 A KR 20160151105A KR 20180053933 A KR20180053933 A KR 20180053933A
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- powder
- cosmetic composition
- coated
- surfactant
- water
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- 239000000203 mixture Substances 0.000 title claims abstract description 36
- 239000002537 cosmetic Substances 0.000 title claims abstract description 25
- 239000000843 powder Substances 0.000 claims abstract description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000004094 surface-active agent Substances 0.000 claims abstract description 18
- 239000003921 oil Substances 0.000 claims abstract description 10
- 239000008213 purified water Substances 0.000 claims abstract description 8
- 229910052623 talc Inorganic materials 0.000 claims description 10
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 9
- 239000000454 talc Substances 0.000 claims description 9
- 239000002736 nonionic surfactant Substances 0.000 claims description 6
- 238000009472 formulation Methods 0.000 claims description 4
- 229920001296 polysiloxane Polymers 0.000 claims description 4
- 239000003995 emulsifying agent Substances 0.000 claims description 3
- 238000000465 moulding Methods 0.000 abstract description 9
- 239000002904 solvent Substances 0.000 abstract description 5
- 230000000052 comparative effect Effects 0.000 description 22
- 229940008099 dimethicone Drugs 0.000 description 12
- 239000004205 dimethyl polysiloxane Substances 0.000 description 12
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 12
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 12
- 239000011248 coating agent Substances 0.000 description 8
- 238000000576 coating method Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 8
- 238000010304 firing Methods 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 5
- 238000001125 extrusion Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 230000002688 persistence Effects 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 239000000049 pigment Substances 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 2
- 238000003776 cleavage reaction Methods 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000007017 scission Effects 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004606 Fillers/Extenders Substances 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000008199 coating composition Substances 0.000 description 1
- DTPCFIHYWYONMD-UHFFFAOYSA-N decaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO DTPCFIHYWYONMD-UHFFFAOYSA-N 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 239000010696 ester oil Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 229910052809 inorganic oxide Inorganic materials 0.000 description 1
- WTFXARWRTYJXII-UHFFFAOYSA-N iron(2+);iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Fe+2].[Fe+3].[Fe+3] WTFXARWRTYJXII-UHFFFAOYSA-N 0.000 description 1
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229940094332 peg-8 dimethicone Drugs 0.000 description 1
- 229940061571 peg-9 dimethicone Drugs 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/022—Powders; Compacted Powders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/60—Particulates further characterized by their structure or composition
- A61K2800/61—Surface treated
- A61K2800/62—Coated
- A61K2800/622—Coated by organic compounds
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Emergency Medicine (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
Description
본 발명은 소성타입의 메이크업 화장료 조성물에 관한 것으로, 더욱 구체적으로 정제수, 오일, 및 분체로 구성된 소성타입의 화장료 조성물에 있어서, 분체를 계면활성제로 코팅하는 것을 특징으로 하는 소성타입의 화장료 조성물에 관한 것이다.The present invention relates to a makeup cosmetic composition of a plasticity type, more specifically to a plasticized cosmetic composition comprising purified water, oil and powder, wherein the powder is coated with a surfactant will be.
소성제형의 메이크업 화장료 조성물은 일반적으로 파우더 분체와 물 또는 O/W 에멀젼을 혼합하여 반죽상으로 만들고 이를 압출기를 이용하여 성형 후 건조하는 방법으로 제조한다. 이 때, 반죽상의 경도가 너무 높으면 성형성이 낮아지게 되는 문제가 발생한다. 그렇기 때문에 상기 반죽상의 경도를 낮추기 위하여 물의 함량을 조절하는데, 이 때 물을 일정량 이상 함유하게 될 경우 건조 후 제품의 수축현상이 일어나게 되어 물을 일정량 이상 함유하도록 할 수가 없다. 또한, 화장품의 체질안료인 탈크는 마그네슘과 실리카의 산화물로서 Mg3Si4O10(OH)2 화학식을 갖는 판상의 무기산화물이다. 이 물질의 벽개면(cleavage urfaces)은 하이드록시(-OH) 관능기가 없으며, 실리카-산소 결합을 갖고 있어 전자 주게(electron donor)가 아니다. 이러한 물리적 성질은 벽개면이 물과의 수소결합을 이루지 못하는 이유로 인해 소수성의 특성을 갖고 있으며, 따라서 물에는 분산이 어렵다는 특성이 있다. 그렇기 때문에 반죽상의 경도를 조절하고 분산을 용이하게 하기 위해서는 분체와 물의 친화력이 중요하다.The makeup cosmetic composition of the firing formulation is generally prepared by mixing Powder Powder with water or an O / W emulsion to prepare a kneaded powder, molding it using an extruder and drying it. At this time, when the hardness of the dough is too high, the moldability is lowered. Therefore, in order to lower the hardness of the dough, the content of water is controlled. If the dough contains more than a certain amount of water, the product shrinks after drying, so that it can not contain water over a certain amount. Talc, which is an extender pigment of cosmetics, is a plate-like inorganic oxide having an Mg 3 Si 4 O 10 (OH) 2 formula as an oxide of magnesium and silica. The cleavage surfaces of this material are free of hydroxy (-OH) functionalities and have silica-oxygen bonds and are not electron donors. These physical properties are characterized by hydrophobicity due to the fact that the cleavage plane does not form a hydrogen bonding with water, and therefore, it is difficult to disperse in water. Therefore, the affinity between the powder and water is important for controlling the hardness of the dough and for facilitating the dispersion.
종래에 상기와 같은 문제점을 해결하기 위하여 분체를 수용성 물질로 코팅을 하여 소성제형의 메이크업 화장료 조성물을 제조하였는데, 이 경우에는 코팅된 분체와 물과의 반발력이 너무 낮아 반죽상태의 경도가 낮아지게 되어 압출이 용이하지 않을 뿐만 아니라 분체 표면이 수용성으로 되어 있어 땀과 같은 성분에 잘 지워져 화장의 지속성이 떨어지게 되는 문제점이 있다. 이와 반대로 분체를 오일로 코팅하는 경우에는 화장의 지속성은 높아지나 코팅된 분체와 물과의 반발력이 높아 성형이 어렵다는 문제점이 발생하게 된다. Conventionally, in order to solve the above problems, powder is coated with a water-soluble substance to prepare a makeup cosmetic composition of a firing formulation. In this case, the repulsive force between the coated powder and water is too low, Extrusion is not easy, and the surface of the powder is water-soluble, so that the powder is easily removed from components such as sweat, and the persistence of make-up is deteriorated. On the contrary, when the powder is coated with oil, persistence of make-up is high, but there is a problem that it is difficult to form because of high repulsive force between the coated powder and water.
이에, 본 발명자들은 상기 종래기술들의 문제점들을 극복하기 위하여 예의 연구노력한 결과, 정제수, 오일, 및 분체로 구성된 소성타입의 화장료 조성물에 있어서, 분체를 계면활성제로 코팅하는 경우, 계면활성제로 코팅된 분체와 용매인 물과의 친화력을 높여 반발력을 줄임으로써, 성형 안정성 및 제품 사용감을 높여줄 수 있음을 확인하고, 본 발명을 완성하게 되었다.The inventors of the present invention have conducted intensive researches to overcome the problems of the prior art. As a result, it has been found that when a powder is coated with a surfactant in a plasticized cosmetic composition composed of purified water, oil, and powder, By increasing the affinity between water and a solvent and reducing the repulsive force, it is possible to increase the molding stability and feel of use of the product.
따라서, 본 발명의 주된 목적은 계면활성제로 코팅된 분체와 용매인 물과의 친화력을 높여 반발력을 줄임으로써, 성형 안정성 및 제품 사용감을 높여줄 수 있는 소성타입의 메이크업 화장료 조성물을 제공하는 데 있다.Accordingly, it is a main object of the present invention to provide a makeup cosmetic composition of a plastic type which can increase the affinity between a powder coated with a surfactant and water as a solvent to reduce the repulsive force, thereby improving the molding stability and feeling of product use.
본 발명의 한 양태에 따르면, 본 발명은 정제수, 오일, 및 분체로 구성된 소성타입의 화장료 조성물에 있어서, 분체를 계면활성제로 코팅하는 것을 특징으로 하는 소성타입의 화장료 조성물을 제공한다.According to one aspect of the present invention, there is provided a calcined cosmetic composition comprising purified water, oil, and powder, wherein the powder is coated with a surfactant.
종래에 소성 타입의 메이크업 화장료 조성물을 제조하는데 있어서, 분체와 물과의 반발력을 줄이기 위해 분체를 수용성 물질로 코팅하는 경우, 조성물의 반죽상태의 경도가 높아져 압출이 용이하지 않을 뿐만 아니라 화장의 지속성이 떨어진다는 문제점이 있었으며, 이러한 지속성을 높이기 위해 분체를 오일로 코팅하는 경우 지속성은 높으나 물과의 반발력이 높아져 성형성이 낮아지는 문제가 발생하였다. 이에, 본 발명자들은 분체와 물과의 친화력을 높이기 위하여 분체를 계면활성제로 코팅할 경우, 코팅된 분체와 용매인 물과의 친화력을 높여 반발력을 줄임으로써 성형 안정성 및 제품 사용감을 높여줄 수 있음을 확인하고, 본 발명을 완성하게 되었다.Conventionally, in the production of a makeup cosmetic composition of a firing type, when the powder is coated with a water-soluble substance in order to reduce the repulsive force between the powder and the water, the hardness of the kneaded state of the composition is increased so that the extrusion is not easy, In order to improve the durability, when the powder is coated with oil, persistence is high, but the repulsive force with water is increased and the formability is lowered. The present inventors have found that when the powder is coated with a surfactant to increase the affinity between the powder and water, the affinity between the coated powder and the solvent, water, is increased to reduce the repulsive force, And the present invention was completed.
본 발명에 있어서, 상기 분체를 코팅하는 계면활성제는 비이온 계면활성제인 것을 특징으로 한다. 본 발명에서는 계면활성제 가운데 피부 자극이 가장 적고 피부에 대한 안정성이 높은 비이온 계면활성제를 사용하였으나, 이에 한정되지 않는다.In the present invention, the surfactant for coating the powder is characterized by being a nonionic surfactant. In the present invention, non-ionic surfactants having the least skin irritation and high skin stability among surfactants are used, but the present invention is not limited thereto.
본 발명에 있어서, 상기 비이온 계면활성제는 피이지(PEG)화된 실리콘 유화제 (PEGylated silicone emulsifier)인 것을 특징으로 하며, 구체적으로는 PEG-11 Methyl Ether Dimethicone, PEG-9 Dimethicone, PEG-32 Methyl Ether Dimethicone, PEG-10 Dimethicone, PEG-8 Dimethicone 또는 PEG 12 Dimethicone인 것을 특징으로 한다. 본 발명의 실시예에서는 PEG 12 Dimethicone를 사용하였으나, 이에 한정되지 않는다.In the present invention, the nonionic surfactant is a PEGylated silicone emulsifier. Examples of the nonionic surfactant include PEG-11 Methyl Ether Dimethicone, PEG-9 Dimethicone, PEG-32 Methyl Ether Dimethicone, PEG-10 dimethicone, PEG-8 dimethicone or PEG 12 dimethicone. In the examples of the present invention, PEG 12 dimethicone was used, but the present invention is not limited thereto.
본 발명의 실험예에 따르면, 비이온 계면활성제 중 피이지(PEG)화된 실리콘 유화제 (PEGylated silicone emulsifier), 특히 PEG 12 Dimethicone로 분체를 코팅하여 제조한 실시예 1의 경우, 그렇지 않은 비교예 1 내지 3보다 반죽상태의 경도는 낮아 압출 성형이 용이하게 할 수 있었고, 성형 후의 경도는 높아 성형 안정성이 우수할 뿐만 아니라 낙하 안정성 또한 매우 우수한 것을 확인하였다. 또한, 사용성 평가에서도 우수하다는 결과를 확인할 수 있었다. 이에 반면에 분체를 지용성인 디메치콘으로 코팅한 비교예 2의 경우, 반발력이 높아져 반죽상태에서의 경도가 가장 높아 압출에 용이하지 않았으며, 분체를 수용성인 실리카로 코팅한 비교예 3의 경우, 반발력이 낮아져 소성 과정 후의 경도가 낮아 낙하 안정성에서도 좋지 못한 평가를 얻었다. 뿐만아니라 비교예 2 및 3 모두 사용성 평가에서도 우수하지 못한 결과를 얻었다. 이러한 결과로 볼 때, 분체를 계면활성제로 코팅한 본원발명 조성물은 소성타입의 메이크업 화장료 조성물로서 적합하다는 것을 알 수 있다.According to the experimental example of the present invention, in the case of Example 1 prepared by coating a powder with a PEGylated silicone emulsifier, particularly PEG 12 Dimethicone, of nonionic surfactants, 3, the hardness of the kneaded state was low, so that extrusion molding could be facilitated, and the hardness after molding was high, and it was confirmed that not only the molding stability but also the falling stability was also excellent. In addition, it was confirmed that the usability test was also excellent. On the other hand, in the case of Comparative Example 2 in which the powder was coated with the liposoluble dimethicone, in Comparative Example 3 in which the repulsive force was increased and the hardness in the kneaded state was the highest, The repulsive force was low and the hardness after the firing process was low, so that the drop stability was not good. In addition, both Comparative Examples 2 and 3 were not excellent in usability evaluation. From these results, it can be seen that the composition of the present invention, in which the powder is coated with a surfactant, is suitable as a makeup cosmetic composition of the burning type.
본 발명에 있어서, 상기 분체의 코팅은 계면활성제 외에 이소프로필알코올 및 탈크를 이용하는 것을 특징으로 한다.In the present invention, the coating of the powder is characterized by using isopropyl alcohol and talc in addition to the surfactant.
본 발명에 있어서, 상기 화장료 조성물은 투웨이케익, 팩트, 파우더 또는 아이섀도우로 구성된 군에서 선택된 하나 이상의 제형을 갖는 것을 특징으로 한다.In the present invention, the cosmetic composition is characterized by having at least one formulation selected from the group consisting of two-way cakes, facts, powders or eye shadows.
이상 설명한 바와 같이, 정제수, 오일, 및 분체로 구성된 소성타입의 화장료 조성물에 있어서, 분체를 계면활성제로 코팅한 소성타입의 화장료 조성물의 경우, 계면활성제로 코팅된 분체와 용매인 물과의 친화력을 높여 반발력을 줄임으로써, 성형 안정성 및 제품 사용감을 높여줄 수 있다.As described above, in the case of a calcined type cosmetic composition in which the powder is coated with a surfactant, the affinity between the powder coated with the surfactant and water serving as the solvent in the calcined type cosmetic composition composed of purified water, oil and powder By lowering the repulsive force, it is possible to enhance the molding stability and the feeling of use of the product.
이하, 실시예를 통하여 본 발명을 더욱 상세히 설명하기로 한다. 이들 실시예는 단지 본 발명을 예시하기 위한 것이므로, 본 발명의 범위가 이들 실시예에 의해 제한되는 것으로 해석되지는 않는다.Hereinafter, the present invention will be described in more detail with reference to Examples. These embodiments are only for illustrating the present invention, and thus the scope of the present invention is not construed as being limited by these embodiments.
제조예Manufacturing example 1 내지 3: 코팅 1 to 3: Coating 분체의Powdery 제조 Produce
5L의 유리비커에 탈이온수 5.0 kg을 부가하고, 피복조성물로서 이소프로필알코올 300g 및 피이지-12 디메치콘(실소프트 870, 모멘티브사제, 코팅물질) 90g을 별도의 용기에 혼합하여 피복 조성물의 혼합액 만든 후, 상기 탈이온수를 1 Hp 디졸바로 1,000 rpm에서 교반하면서 상기 피복 조성물의 혼합액을 10분간에 걸쳐 부가하고 같은 교반 조건에서 20분간 더 혼합하였다. 이어서, 탈크(Talc JA 46R, 아사다밀사제, 안료)를 2.910 kg을 30분간에 걸쳐 천천히 첨가한 후 30분간 분산액을 만들고, 피이지-12 디메치콘 피복 티타니아 입자를 얻었다. 5.0 kg of deionized water was added to 5 L of a glass beaker, and 300 g of isopropyl alcohol and 90 g of phage-12 dimethicone (Silsoft 870, manufactured by Momentive Co., Ltd., coating material) After the mixture solution was prepared, the deionized water was added to the coating composition solution for 10 minutes while stirring the mixture at 1,000 rpm immediately after the 1 Hp dissolve, and further mixed for 20 minutes under the same stirring conditions. Subsequently, 2.910 kg of talc (Talc JA 46R, manufactured by Asada Silicone Co., Ltd., pigment) was slowly added over 30 minutes, and a dispersion was made for 30 minutes to obtain a pigment-12 dimethicone-coated titania particles.
상기 반응종료 후, 수세, 여과, 탈수, 건조 및 분쇄를 거쳐 본 발명에 따른 피이지-12 디메치콘 피복 탈크 분체(제조예 3)를 수득하였다.After the completion of the reaction, water, filtration, dehydration, drying and pulverization were carried out to obtain a paper-12 dimethicone-coated talc powder (Preparation Example 3) according to the present invention.
하기 표 1의 안료 및 코팅물질을 이용하여 비교예 1 및 2의 코팅분체를 상기와 같은 동일한 방법으로 제조하였다.The coating powders of Comparative Examples 1 and 2 were prepared by the same method as above using the pigment and coating material of Table 1 below.
실시예Example 1 및 1 and 비교예Comparative Example 1 내지 2: 소성 타입의 메이크업 1 to 2: firing type make-up 화장료Cosmetics 조성물의 제조 Preparation of composition
하기 표 2의 성분을 조합하여 화장료 조성물을 제조하였다. 구체적으로는 표 2의 상 A에서 수득한 분체 혼합물과 상B를 60:40의 중량비로 만능 혼합기 안에서 120rpm으로 5분간 혼합하였다. 알맞은 점도로 제조된 반죽을 압출기를 이용하여 일정 두께의 내용물을 얻고, 유압타정기로 일정모양으로 성형하였다. 이 성형물을 65℃ 오븐에서 8시간 동안 건조하였다.The ingredients of Table 2 below were combined to prepare a cosmetic composition. Specifically, the powder mixture obtained in the phase A of Table 2 and the phase B were mixed in a universal mixer at a weight ratio of 60:40 at 120 rpm for 5 minutes. The kneaded dough with appropriate viscosity was extruded to obtain a certain thickness of the dough and molded into a certain shape with a hydraulic tablet machine. The molded product was dried in an oven at 65 DEG C for 8 hours.
실험예Experimental Example 1: 경도 평가 1: Hardness evaluation
상기 실시예 및 비교예1-3의 반죽상태 일 때와 성형 후 소성과정을 거친 상태일 때 경도를 비교하기 위하여 경도계(기기명: Sun Rheo-Meter (CR-500DX-L))를 이용해 경도를 측정하였다. 반죽상태일 때의 경도는 표 3에 나타내었고, 성형 후 소성 과정 후 경도는 표 4에 나타내었다.Hardness was measured using a hardness meter (equipment name: Sun Rheo-Meter (CR-500DX-L)) to compare the hardness of the kneaded state of the above Examples and Comparative Examples 1-3, Respectively. The hardness in the kneaded state is shown in Table 3, and the hardness after the post-molding firing process is shown in Table 4. [
그 결과, 상기 표 3에서 알 수 있듯이, 본 발명의 실시예 1이 비교예 1 ~3 조성물보다 반죽상 경도는 낮은 경도를 갖고 있는 것으로 평가되었으며, 압출 공정 시 보다 용이하게 압출이 가능함이 확인 되었다. As a result, as shown in Table 3, it was evaluated that the Example 1 of the present invention had a hardness comparatively lower than that of the compositions of Comparative Examples 1 to 3, and it was confirmed that extrusion can be performed more easily in the extrusion process .
또한, 표 4에서 확인할 수 있듯이, 소성과정 후 경도는 실시예 1이 제일 높았으며 이는 최종적으로 우수한 성형 안정성을 얻을 수 있었다. As can be seen from Table 4, the hardness after the firing process was the highest in Example 1, which resulted in excellent molding stability at the end.
실험예Experimental Example 2: 낙하 안정성 평가 2: Evaluation of falling stability
낙하 안정성의 측정은 50 cm 높이에서 성형 제조품을 3 mm 고무판에 3회 수평 낙하시켜 측정하였다. 그 결과를 하기 표 5에 나타내었다(나쁨 1 - 2 - 3 -4 - 5 좋음).The drop stability was measured by dropping the molded article horizontally three times onto a 3 mm rubber plate at a height of 50 cm. The results are shown in Table 5 (poor 1 - 2 - 3 - 4 - 5).
그 결과, 상기 표 5에 나타나는 바와 같이. 본원발명의 실시예 1의 조성물의 낙하 안정성이 매우 우수한 것을 확인하였다.As a result, as shown in Table 5 above. It was confirmed that the drop stability of the composition of Example 1 of the present invention was extremely excellent.
실험예Experimental Example 3: 3: 사용감Feeling 평가 evaluation
사용감 측정은 25 명의 panel을 선정하여 아래의 시료를 각각 제공하고, 눈두덩이 주위에 사용 후 5점을 만점으로 기준한 후 그 수치의 평균을 나타내었다.The sensory evaluation was carried out by selecting 25 panels from each of the following samples, and the average of the values after the use of 5 points after the use around the eyes were evaluated.
그 결과를 하기 표 6에 나타내었다(나쁨 1 - 2 - 3 - 4 - 5 좋음).The results are shown in Table 6 below (poor 1 - 2 - 3 - 4 - 5 is good).
그 결과, 상기 표 5에 나타나는 바와 같이. 본원발명의 실시예 1의 조성물의 사용감(발색력, 밀착력 및 지속성)이 모두 우수한 것을 확인하였다.As a result, as shown in Table 5 above. It was confirmed that the feeling of use (color development, adhesion and persistence) of the composition of Example 1 of the present invention was excellent.
Claims (5)
A cosmetic composition of a calcined type comprising purified water, oil, and powder, wherein the powder is coated with a surfactant.
A cosmetic composition of a calcined type comprising purified water, oil, and powder, wherein the powder is coated with a surfactant.
The cosmetic composition of claim 2, wherein the nonionic surfactant is a PEGylated silicone emulsifier.
The cosmetic composition of claim 1, wherein the powder is coated with isopropyl alcohol and talc in addition to a surfactant.
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| CN111000736A (en) * | 2019-12-24 | 2020-04-14 | 张士飞 | Preparation method of eyebrow pencil lead |
| WO2022102875A1 (en) * | 2020-11-16 | 2022-05-19 | 코스맥스 주식회사 | Baked makeup cosmetic composition and method for producing same |
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| CN111000736A (en) * | 2019-12-24 | 2020-04-14 | 张士飞 | Preparation method of eyebrow pencil lead |
| WO2022102875A1 (en) * | 2020-11-16 | 2022-05-19 | 코스맥스 주식회사 | Baked makeup cosmetic composition and method for producing same |
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