KR20180001950A - Powder gel containing hinoki cypress extract and manufacturing method of the same - Google Patents

Abstract

The present invention relates to a powder gel containing a Chamaecyparis obtuse extract as an active ingredient and to a manufacturing method thereof, and specifically, to a powder gel containing a Chamaecyparis obtuse extract as an active ingredient and to a manufacturing method thereof, which comprises the following steps: a drying step of selecting, washing and drying Chamaecyparis obtuse; a crushing step of crushing the dried Chamaecyparis obtuse; an extracting step of extracting the crushed Chamaecyparis obtuse; a filtration step of filtering the Chamaecyparis obtuse extract; a concentration step of concentrating the filtered Chamaecyparis obtuse extract; and a mixing and stirring step of mixing cosmetic preparation components with the concentrated Chamaecyparis obtuse extract. It is an object of the present invention to provide the powder gel which is easy to use due to the absence of a blowing powder by using a gel-type powder instead of a powder-type powder.

Description

Technical Field [0001] The present invention relates to a powder gel containing an extract of Chamaecyparis obtusa as an active ingredient and a method for producing the powder gel.

The present invention relates to a powder gel containing an extract of Chamaecyparis obtusa as an active ingredient and a method for producing the same. More specifically, the present invention relates to a powder gel, A crushing step of crushing the dried white timber; An extracting step of extracting the crushed white wood; A filtration step of filtering the elderberry extract; Concentrating the filtered Clover wood extract; The present invention relates to a powder gel containing an extract of Chamaecyparis obtusa as an active ingredient and a process for producing the same.

When it comes to summer, the high temperature and humid environment in the children's skin causes an emergency. Newborn babies and infants who need to wear a diaper all the time because sweat glands are not fully functional and the amount of sweat on the surface of the skin is more than twice that of an adult, so it is easier to get ridges.

Our body releases the sweat to maintain proper body temperature, and the body temperature is lowered. When excessive amount of sweat is shed, the hole of the sweat pipe is clogged to cause a heat rash. The reason for the clogging of the sweatpipe is the high humidity and high humidity environment, the exposure to ultraviolet rays and the bacteria of the skin.

The heat rash usually occurs on the neck, armpits, groin, and inside of the elbow where the skin swells and the skin folds like forehead and back. When a heat rash occurs, small, transparent blisters are formed at first, and as time goes by, it spreads to the inside of the sweat glands and the skin appears red, and it is very itchy and sometimes feels hot.

In the case of newborn babies, diaper rashes may appear along with a sweaty bite. Especially when diarrhea occurs, it is difficult to change the diaper immediately in time, so that the hips become wet and the hips may become red. In severe cases, the skin becomes rough, and the pores get torn and the pus is caught.

It is desirable to prevent rashes and diaper rashes before they occur. To do this, it is important to dry the wet and sweaty areas with powder, and it is good to lower the heat feeling of the rash area. It is also desirable to use the ingredients of a natural material having an antibacterial function so as to improve the surface tension of the skin and to improve it without using the medicine if possible.

Representative natural materials that have antibacterial function include cottonwoods, which contain phytoncide (phytoncide). It is a term created in Russian by the combination of phyton (meaning "plant") and "cada" (meaning "killing"). It is composed of phenol compounds including alkaloids, alkaloids and glycosides, It is a natural material antibacterial agent with various effects such as strong antibacterial, antifungal action, stress relaxation, sedative effect of skin, induction of sleeping, improvement of allergic skin disease, and improvement of immune function.

The applicant of the present invention has also found that the present applicant has succeeded in producing a composition having a form such as a gel, a mist, or a cream containing a component of an antibacterial function of a natural white wool extract, using a porous powder of silica, I have devised eczema relief cosmetics.

Prior art relating to the present invention discloses a process for preparing a phytoncide atopic eczematous emollient composition in Korean Patent Registration No. 10-1280315.

According to claim 1, there is provided a method for producing a phytogenic atopic eczulation relieving composition comprising 35 parts by weight of a pine cone extract, 25 parts by weight of a Pleurotus cornus extract, 5-10 parts by weight of green tea leaf extract, and 5-10 parts by weight of phytoncite- The wood was separated and placed in 1 to 15 times water of pine wood and white wood for 24 to 36 hours, then dried and dried for one day. Then, the wood was first pulverized to 8 to 10 mm using an all- The resulting pine wood and the crushed wood crushed material were put into a 325-mesh mesh and squeezed with a hydraulic compression press (2HP) to separate the liquid phase. The resultant liquid was separated for 24 hours to obtain a supernatant liquid and a precipitate slurry , Filtering the precipitate slurry to obtain a liquid extract by taking only the supernatant, firstly aging the extract at 13-15 ° C for 36 hours, Is aged at 13-15 캜 for 36 hours in a pottery reactor which is ground and pulverized and air is permeated and the liquid component is not permeated to obtain a liquid extract of the first aged green tea leaves, Wherein the phytoncide-generated ionized water is mixed with 40 to 50 parts by weight of leek, 30 to 40 parts by weight of pine needles, and 10 to 20 parts by weight of green tea leaves, and the mixture is passed through a pottery A step of introducing the mixture into a reactor of a material and allowing it to stand at room temperature for 5 to 6 days to ferment and then using a material obtained by filtering a liquid material generated by fermentation; Lt; 0 > C for 72 hours.

However, the above-mentioned prior art shows a process for producing the extract of Clostridium perfringens. The process for using the Clostridium perfringens extract thus prepared in the production of lotions, creams, ointments and the like is not specified, I did not. In particular, the specific manufacturing process of the powder gel to be developed by the present applicant is not described.

In addition, in the process of preparing the extract of Cryptomeria japonica, the time of washing and drying the Cryptomeria japonica is short and the complete drying can not be performed, so that the water contained in the Cryptomeria japonica can dilute the Cryptomeria japonica extract.

Another technique relates to a powder containing a silica component, and Japanese Patent Publication No. 10-1566293 discloses a method for producing rice baby powder which improves skin feel and hygroscopicity.

According to claim 1, there is provided a method for producing a white rice, comprising the steps of: (a) pulverizing an aged white rice; (b) coating said pulverized material with an essential oil; And (c) mixing silica with the pulverized product coated with the essential oil.

The prior art is a baby powder in which rice is pulverized and mixed with silica and has a powder form. However, if you spray baby powder in the form of powder to a newborn or infant child, you may inhale the powder dispersed in the air, which can cause problems with the bronchial tubes. In addition, it does not meet the purpose of the present applicant, because it does not contain the extract of Cryptomeria japonica, which helps strengthen the antibacterial activity and the surface tension.

Therefore, we want to develop a powder gel containing silica extract which helps antibacterial activity and strengthening of cotton surface, silica functioning as a powder, and ingredients for lowering heat and filling water.

Registered Patent Publication No. 10-1280315 (Announcement of Jan. 2013, 2013) Patent Registration No. 10-1566293 (issued November 5, 2015)

It is an object of the present invention to prevent or alleviate skin rash or heat rash by using antler leaf extract, silica and an additional ingredient to make antimicrobial function, to enhance moisture retention, to reduce heat sensation and to finish skin smoothly.

It is an object of the present invention to provide a powder gel which is easy to use due to the absence of dusting by using gel-type powder instead of powder type powder.

The present invention relates to a powder gel containing an extract of Chamaecyparis obtusa as an active ingredient and a method for producing the same. More specifically, the present invention relates to a powder gel, A crushing step of crushing the dried white timber; An extracting step of extracting the crushed white wood; A filtration step of filtering the elderberry extract; Concentrating the filtered Clover wood extract; And a mixing and stirring step of mixing the concentrated unilamellar vinegar extract and a cosmetic preparation component. The present invention provides a powder gel containing an extract of Chenopodium albuma as an active ingredient and a process for producing the same. do.

The present invention has antimicrobial function by using the extract of Cryptomeria japonica, silica and an additional ingredient, and has the effect of enhancing the moisturizing power, lowering the heat sensation, finishing the skin smoothly, and preventing and alleviating skin rash or heat rash.

The present invention uses a gel-type powder rather than a powder-type powder, and has an efficacy that is easy to use due to no flaking.

FIG. 1 is a diagram illustrating a manufacturing process of a powder gel according to the present invention.
Fig. 2 is a diagram showing the sensory evaluation according to the presence or absence of the hen egg extract.
3 is a diagram showing sensory evaluation according to the amount of the thickening agent.

The terms and words used in the present specification and claims should not be construed as limited to ordinary or dictionary terms and applicants may properly define the concept of a term in order to best describe its invention It should be construed as meaning and concept consistent with the technical idea of the present invention.

Therefore, the embodiments described in the present specification and the configurations shown in the drawings are merely the most preferred embodiments of the present invention and do not represent all the technical ideas of the present invention, so that various equivalents It should be understood that variations can be made.

Before describing the present invention with reference to the accompanying drawings, it should be noted that the present invention is not described or specifically described with respect to a known configuration that can be easily added by a person skilled in the art, Let the sound be revealed.

Example  1. Preparation of Powder Gel Containing Cottonwood Extract

1) drying step

It is a step of selecting, preparing and washing the unicorn tree leaves. It is preferable to use leaves having a large amount of functional ingredients among them.

Cut the leaves of silkworm in 3 ~ 5cm size and wash and dry. Drying may be carried out by various drying methods such as natural drying, hot air drying, cold air drying, far infrared drying, electric drying, freeze drying or microwave drying, but a cold air drying method may be used.

Drying through cold air drying can prevent the components contained in the perilla leaf from being easily volatilized at high temperatures, and the extraction efficiency of the perilla leaf is increased.

Cold air drying can be carried out at 10 to 40 ° C for 1 to 5 days and can be controlled according to the moisture content of the perilla leaf. If the moisture of the leaves of the unicorn tree is not completely dried, the moisture of the unicorn tree can be diluted in the process of producing the extract, and it is preferable to dry completely.

2) Grinding step

And drying the dried unshiu tree leaves through the above steps.

The crushing method may be a rotary crusher, a jaw crusher, a roll crusher, a cone crusher, a hammer crusher, an impact crusher, a hammer mill A ball mill, a Hammer mill, a rod mill, a ball mill, a Raymond mill, a super mill, a roll mill, a pin mill, a jet mill, And may be performed using a ball mill or a vibration mill.

At this time, the size of the unshiu leaf can be crushed to 1 ~ 5mm, and it can be variously set according to the design conditions, and it can be applied by repeating the crushing step twice or more according to the design conditions.

The smaller the size to be crushed, the greater the extraction efficiency in the following extraction step, but less than 1 mm may be inefficient in the filtration step after the extraction.

3) Extraction step

After drying, it is a step of extracting the crushed softwood leaves.

Various extraction methods such as a supercritical fluid extraction method, a steam distillation method, a vacuum extraction method, a vacuum extraction method, a microwave process extraction method, and a percolation extraction method may be used as the extraction method. Preferably, .

Steam distillation is the process of distilling the white flakes through water vapor to collect the functional ingredients of the white flakes. First, the white flakes are fed with steam and compressed air.

The pressure range of the steam supplied to obtain the curd extract containing a large amount of functional ingredient in the steam and compressed air supply can be adjusted to 2.0 ~ 4.0 k parts by weight f / cm ² , and the pressure range of the compressed air supplied is 1.0 ~ 3.0 atm. ≪ / RTI >

Steam and compressed air distils the flock, so that various functional ingredients, which are contained in a large amount in the flock, flow out together with water vapor, and condensed water is condensed by condensing the outflow steam together with various functional ingredients of the flock.

From the condensed water resulting from the condensation of water vapor, centrifugal separation is performed to extract the untranslated water and the untranslated oil separated into layers.

The extracted unmixed water and the unshallowed oil can be used both in the following mixing and stirring stages.

4) Filtration step

And filtering the filtrate to remove impurities remaining in the untranslated water and the untransparent oil extracted through the extraction step. The filtering screen has a mesh size of about 10 to 30 um.

The hair size of ordinary people is 100um, and the mesh size of the sieve used in the above is a size that can be filtered into a clear beverage.

Filtration can be carried out by various methods such as chromatography (chromato weight part), suction filtration, atmospheric filtration, vacuum filtration, pressure filtration, ultrafiltration, microfiltration and reverse osmosis.

The filtration time, temperature, and the number of times may also be varied depending on the design conditions. Filtration can be performed using a method other than the filtration method described above, or using two or more methods.

5) Concentration step

And the step of concentrating each of the filtered water extract and the whitening oil, respectively.

Concentration of the washing water may be carried out by methods such as evaporation concentration, freezing concentration, drying concentration, membrane concentration, vacuum concentration, and concentration under reduced pressure. It may also be concentrated using more than one method.

Preferably, the vacuum concentration method used typically for concentrating the extract can be used and can be carried out for 2 to 5 hours.

It is most desirable that the maturing oil is kept at a low temperature and at a constant temperature in a space free from light to keep it fresh.

6) Mixing and Stirring step

The step of concentrating the leaching extract, the leaching water and the leaven oil, the thickener, the neutralizing agent, the aloe powder, the resulting extract, the pepper extract and the honey are mixed.

1 to 3 parts by weight of the resulting extract, 1 to 3 parts by weight of the peppermint extract, 0.5 to 1 part by weight of the thickening agent, 0.25 to 0.5 part by weight of the neutralizing agent, 0.5 to 1 part by weight of the aloe powder 5 to 10 parts by weight of glycerin, 1 to 5 parts by weight of monoaxial oil, 0.25 to 0.5 parts by weight of honey and 15 to 25 parts by weight of silica, wherein aloe powder is used as a soothing agent It can be changed to powder of other ingredients.

The creation here refers to the root fruit of a perennial herb, belonging to the Asteraceae family, which excellently removes wastes from the skin and regenerates skin, and functions as a natural preservative. However, due to the spicy components of its creation, it should be used in small quantities at an optimal rate.

When used in cosmetics, peppermint provides a refreshing sensation to the skin, thereby relieving the heat and helping to eliminate the activity of foreign substances harmful to the skin. It also helps to heal damaged skin, and it can act as a skin conditioning and turn it into a vitality skin. However, mushrooms should also be used in small quantities at an optimum rate due to the unique spicy ingredients.

The ingredients in honey have the effect of preventing aging and reducing inflammation, and it acts as a good moisturizer that draws moisture from the air to keep the skin soft and moist. When a small amount of honey is contained, it is possible to naturally sweat the sweat while filling the moisture.

Increasing agents should be used in combination with neutralizing agents to increase the viscosity of the manufactured cosmetics. Carbomer is the most commonly used ingredient. It is a water-soluble thickening agent and has almost no irritation to the skin. Its viscosity can be controlled easily with a wide increase range. It is most commonly used. In addition to its increasing role, it helps stabilize emulsions and is widely used in creams, essences, emulsions and packs.

The pH of the carbomer should be adjusted to pH 5 ~ 6, which is the acidity of healthy skin, by mixing the neutralizing agent at a pH of about 4. The most commonly used neutralizing agent is L-arginine, which is added to food, so it can be used by children in infancy.

If a large viscosity is required according to the design conditions, the ratio of the thickening agent and the neutralizing agent may be increased, and if the viscosity is required, the proportion of the whiteing agent and the aloe powder may be increased.

In addition, it is preferable to add a small amount of glycerin and linseed oil to enhance the moisturizing power because the water can not be retained in the white water and the incremental water because it absorbs moisture inherent in the conventional baby powders and other moisture absorbers It is difficult for children with dry skin to go there.

The mixing method is as follows.

First, add aloe powder, glycerin, and neutralizing agent to the sample water, completely dissolve it, add silica and thickener, and stir with a blender for 5 to 10 minutes until all the mixture is mixed. Since the agitated powder gel contains a large amount of bubbles, it is preferable to undergo a defoaming process of stirring at a slow speed for 3 to 5 minutes.

This powder gel helps to keep the sweaty areas dry and comfortable, and it can lower the skin heat by the cooling unique cooling sensation of soothing gel.

Manufacturing example  1. Powder Mist  Produce

Powder mist can be produced using the powder gel according to the first embodiment.

Fill the container to be mixed with 10 ~ 20% of powder gel, add purified water or cotton wool water so that the total amount becomes 100%, and shake well to make a powder mist.

Manufacturing example  2. Manufacture of Powder Cream

Powder cream can be prepared using the powder gel according to Example 1.

10 to 15 parts by weight of the powder gel, 10 to 15 parts by weight of maleic anhydride, 10 to 15 parts by weight of a whitening oil, and 3 parts by weight of an olive oil wax are mixed with each other. It can be mixed with or changed with the product.

The preparation method is to dissolve the olive oil wax in a weak fire, and then add milky oil to thoroughly mix. Mixed olive oil wax and whitening oil are cooled, and the powdered cream is prepared by mixing the gelatinized water and the powder gel.

Reference Example  1. Sensory evaluation of soothing effect with or without the extract

1-1. Assessment Process

The sensory evaluation in Reference Example 1 is carried out by selecting 30 parents who have children from infants to infants, applying the manufacturing conditions to the different experimental groups, and then calming the effect of the rash and the general preference items in a manner of query response.

The powder gel was prepared and evaluated based on Example 1.

The evaluation method was based on the 5 - point scale method.

The test group used in Reference Example 1 was used by changing the presence or absence of the whitening extract in the powder gel of Example 1, and specifically, see FIG. 2 below.

1-2. Evaluation results

As shown in FIG. 2, the mixing ratio of all the ingredients was fixed, and the products were subjected to the above-described evaluation process by comparing the products using the untreated water and the unbleached oil with the products using the purified water and glycerin.

As a result, it was confirmed that the products produced by using the simplex and monofilament oil were higher in the sedative effect and overall acceptability of the rashes evaluated by the panel according to Reference Example 1. [

The use of powdered gels made only with purified water and glycerin, without the extract of cotton wool, had little sedative effect on the rash, and the recovery rate was slow, and the odor of glycerin was felt because of the absence of special fragrance ingredients There were many.

When 50 parts by weight of maleic anhydride, 50 parts by weight of purified water, and a powder gel made of glycerin were used, the sedative effect of the rash was partially expressed but still little, and the scent of the whitening was fine.

It was confirmed that the sedative effect of the rash was maximized and the fragrance of the whiteness was kept by the fragrance of the other ingredients.

Therefore, it was confirmed that a powder gel composed of only a flat water channel and containing a simple white oil is most preferable.

Reference example  2. Sensory evaluation according to mixing ratio of incrementer

1-1. Assessment Process

The evaluation process is carried out in the same manner as in Reference Example 1, except that the viscosity, the spreading, and the general preference items are inquired and responded to in the test group having different manufacturing conditions.

The powder gel was prepared and evaluated based on Example 1.

The mixing ratio of aloe powder, glycerin, linseed oil and silica was fixed as described in Example 1, and the mixing ratio of the neutralizing agent was Fix at a rate of half of the incremental agent. Specifically, reference is made to Fig. 3 below.

1-2. Evaluation results

As shown in FIG. 3, the increment ratio of the powder gel in Example 1 was changed to three, and the panels were subjected to the evaluation process.

At this time, the ratio of the thickener to the neutralizer was 1: 0.5 and the mixing ratio of the remaining components was fixed.

As a result, it was confirmed that the powder gel having a mixing ratio of 0.5 to 1 part by weight in the overall preference of the panels according to Reference Example 2 was the highest.

The objective of this evaluation was to identify the change in preference of silica according to the ratio of incremental agent, and found an optimal ratio with appropriate viscosity and softness.

When the mixing ratio of the thickening agent is set to 0.1 to 0.5 part by weight, the viscosity is low, so that the spreadability of the powder gel when applied is soft, but it has a problem that it easily flows down. Also, since the viscosity of the powder was low, the powder gel was separated, resulting in irregular mixing ratio of silica contained in the single use.

When the mixing ratio of the thickener was 0.5 to 1.0 part by weight, the viscosity was not diluted and the spreadability was smooth and smooth, and the mixing ratio of silica contained in the mixture was constant.

However, when the mixing ratio of the thickening agent was set to 0.8 to 1.3 parts by weight, the viscosity was so high that it was difficult to use, and thus the wettability and acceptability were decreased.

Therefore, it was confirmed that the mixing ratio of the thickener was most preferably 0.5 to 1.0 part by weight in the preparation of the powder gel.

Reference Example  3. Sensory Evaluation according to Mixing Ratio of Mint Extract and Creation Extract

1-1. Assessment Process

The evaluation process is carried out in the same manner as in Reference Example 1, except that the degree of dissipation of heat and the general preference items are subjected to a question and answer process after applying the manufacturing conditions to different test groups.

The powder gel was prepared and evaluated based on Example 1.

The experimental group used in Reference Example 3 was used by changing the mixing ratio of the peppermint extract and the resulting extract to that of Example 1, and the mixing ratio of the remaining components was fixed as described in Example 1. Specifically, see FIG. 4 below.

1-2. Evaluation results

As shown in FIG. 4, the mixture ratio of the peppermint extract and the extractive extract of the powdered gel of Example 1 was changed to three, and the panels were then subjected to the evaluation procedure.

As a result, it was confirmed that the powder gel having the mixing ratio of the peppermint extract and the resulting extract was 1 to 3 parts by weight in the overall preference of the panel according to Reference Example 3.

The purpose of this evaluation was to determine the degree and preference of skin heat relief according to the mixing ratio of peppermint extract and the resulting extract to find the optimal ratio to eliminate the spicy component and lower the heat sensation.

Peppermint Extract and Creation When the extract was not contained, the skin temperature was raised and the effect of lowering the elevated heat was not effective.

When 1 to 3 parts by weight of the extract of peppermint and the extract of the peppermint was contained, the feeling of cooling sensation was felt due to the function of dissolving the mint and the feeling of creation, and the skin temperature was lowered.

However, when the mixing ratio of the peppermint extract and the resulting extract was set to 3 to 5 parts by weight or more, a large amount of the powdery gel was contained, and it was felt that it was cool immediately after the application.

Thus, it was confirmed that the mixing ratio of the peppermint extract and the resulting extract was 1 to 3 parts by weight most preferably in the production of the powder gel.

Claims (4)

A drying step of selectively washing and then drying the white wood;
A crushing step of crushing the dried white timber;
An extracting step of extracting the crushed white wood;
A filtration step of filtering the elderberry extract;
Concentrating the filtered Clover wood extract; And
Wherein the extract is prepared by mixing and agitating the mixture of the concentrated cottonseed extract and the cosmetic preparation component.
The method according to claim 1,
In the mixing and stirring step,
Wherein the extract is selected from the group consisting of cottonseed oil and cottonseed oil,
The method for producing a powder gel according to any one of claims 1 to 7, wherein the cosmetic preparation component comprises an ascorbic acid extract as an active ingredient, characterized in that it consists of a thickening agent, a neutralizing agent, glycerin, aloe powder, silica,
The method of claim 2,
Wherein the mixing and stirring step comprises:
1 to 3 parts by weight of the resulting extract, 1 to 3 parts by weight of a peppermint extract, 0.5 to 1 part by weight of an incremental agent, 0.25 to 0.5 part by weight of the neutralizing agent, 5 to 10 parts by weight of glycerin, 1 to 5 parts by weight of an oil, 0.5 to 1 part by weight of an aloe powder, 0.25 to 0.5 part by weight of honey, and 15 to 25 parts by weight of silica.
A powder gel containing an extract of Prunus mume extract obtained by the production method according to any one of claims 1 to 3 as an active ingredient.

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