KR20150141096A - thermal performance testing method of radiating film - Google Patents

thermal performance testing method of radiating film Download PDF

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Publication number
KR20150141096A
KR20150141096A KR1020140069703A KR20140069703A KR20150141096A KR 20150141096 A KR20150141096 A KR 20150141096A KR 1020140069703 A KR1020140069703 A KR 1020140069703A KR 20140069703 A KR20140069703 A KR 20140069703A KR 20150141096 A KR20150141096 A KR 20150141096A
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South Korea
Prior art keywords
heat
film
thermal performance
temperature
heating
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KR1020140069703A
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Korean (ko)
Inventor
김덕종
김재현
이학주
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한국기계연구원
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Priority to KR1020140069703A priority Critical patent/KR20150141096A/en
Publication of KR20150141096A publication Critical patent/KR20150141096A/en

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J3/00Spectrometry; Spectrophotometry; Monochromators; Measuring colours
    • G01J3/28Investigating the spectrum
    • G01J3/44Raman spectrometry; Scattering spectrometry ; Fluorescence spectrometry
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00Radiation pyrometry, e.g. infrared or optical thermometry
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/18Investigating or analyzing materials by the use of thermal means by investigating thermal conductivity

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  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • General Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)

Abstract

Disclosed is a method for evaluating the thermal performance of a heat dissipation film that heats a local region of a heat dissipation film, measures a temperature at which convergence progresses while a temperature change in a heated local region increases, and evaluates a thermal performance of the heat dissipation film.
The present invention relates to a method of manufacturing a heat dissipation film, comprising: a heating step of heating a local region of a heat dissipation film; a measurement step of measuring a temperature change of a local region of the heat dissipation film heated through the heating step; And judging the thermal performance.

Description

TECHNICAL FIELD [0001] The present invention relates to a thermal performance testing method of radiating film,

More particularly, the present invention relates to a method of evaluating thermal performance of a heat-radiating film, and more particularly, to a method of evaluating thermal performance of a heat-radiating film by heating a local region of the heat- The present invention relates to a thermal performance evaluation method of a heat dissipation film.

Generally, a method of installing a heat sink or a fan is used as a method of discharging or cooling the heat generated from various electronic parts to the outside of an electronic product. In the case of a heat sink, The heat dissipation efficiency is very low due to the small amount of heat that the heat sink can emit. In addition, the heat dissipating fan generates noise and vibration. In addition, since the PDP, the notebook computer, There is a problem that it can not be applied to a product which is required to be heated. Therefore, it is common to use a heat-radiating film on a sheet or film for electronic products which are required to be lightweight and slim.

The process of evaluating the thermal performance by measuring the thermal conductivity of the heat-radiating film during development of the heat-radiating film is very important.

When the developed heat-radiating film has a thickness of 100 μm or more, it is usually measured by a laser flash method.

However, if the thickness is less than that, 'Time-domain thermoreflectance' or '3 Omega' method can be used, but it is difficult to obtain a reliable measurement value. Furthermore, the thermal conductivity measuring equipment is very expensive and the charge is expensive, so that the usual cost is inconvenient. For a related industry that usually develops heat-radiating films by optimizing a variety of materials and process conditions, it would be a better approach to be able to resolve relative comparisons at a lower cost than absolute value measurements of thermal conductivity.

Patent Document 1: JP-A-10-22008-0113631

SUMMARY OF THE INVENTION It is an object of the present invention to solve the above problems and to provide a heat dissipating film which is superior in thermal performance to heat dissipating films, And a method of evaluating the thermal performance of the heat dissipation film.

According to another aspect of the present invention, there is provided a method of evaluating a thermal performance of a heat radiating film, the method comprising: heating a local region of the heat radiating film; measuring a temperature change of a local region of the heat radiating film heated through the heating step; And a determination step of determining a thermal performance by comparing the temperature measured when the temperature measured in the measuring step increases and the temperature measured by the measuring step.

The heating step is characterized by irradiating a laser to a local site of the heat radiation film.

The measuring step is characterized by being made in a non-contact manner using an infrared thermometer.

And the heating step and the measuring step are performed simultaneously.

Wherein the heating step is performed by irradiating a laser to a local region of the heat dissipation film through a laser generator included in a Raman spectrometer, The method of claim 1, wherein the determining step comprises a step of comparing the degree to which the peak of the Raman spectrum is redshifted in the measuring step, To determine the thermal performance.

As described above, in the thermal performance evaluation method of the heat radiation film according to the present invention, the thermal performance of the heat radiation film can be evaluated by a relative comparison method.

Accordingly, there is an advantage in that a heat radiation film excellent in thermal performance can be selected simply and inexpensively as compared with the method of measuring the absolute value of the thermal performance.

In addition, when a heat-radiating film with high thermal conductivity is verified, it is possible to prevent the overheating of the local heat source when the heat-radiating film is applied to the actual product, and the heat generated from the heat source effectively spreads over a large area, Lt; / RTI >

1 is a flowchart of a method for evaluating a thermal performance of a heat radiation film according to an embodiment of the present invention,
2 is a perspective view showing a state in which a heat radiation film is heated using a laser,
3 is a perspective view showing a state where the temperature of the heat radiation film is measured using an infrared thermometer,
FIG. 4 is a perspective view showing a state in which heating and temperature measurement of the heat radiation film proceed simultaneously;
5 is a view showing a state in which the thermal performance of a heat radiation film is evaluated using a Raman spectrometer,
6 is a graph showing the temperature change of the heat-radiating film measured using an infrared thermometer.

Hereinafter, a method of evaluating the thermal performance of the heat radiating film according to the present invention having the above-described structure will be described in detail with reference to the accompanying drawings.

2 is a perspective view illustrating a method of heating a heat radiating film using a laser, and FIG. 3 is a perspective view illustrating a heat radiating film using an infrared thermometer, In which the temperature is measured.

A thermal performance evaluation method of a heat radiation film according to the present invention includes a heating step of heating a local region of a heat radiation film 10 and a measurement step of measuring a temperature change of a local region of the heat radiation film 10 heated through the heating step And a determining step of determining a thermal performance by comparing the temperature measured while the temperature measured in the measuring step increases.

The heating step is a step of heating the local region of the heat dissipating film 10, and various embodiments may occur within a range where heat energy can be transmitted to the heat dissipating film 10.

The heating step may be performed by a contact method or a non-contact method, and the local area is heated to judge whether heat radiation and heat radiation of the heat radiation film 10 are reliably performed.

According to another embodiment of the present invention, the heating step is performed by irradiating a local portion of the heat dissipation film 10 with a laser (L).

The laser generator 2 is required to irradiate the laser beam L to the heat radiating film 10 as described above and the thermal energy can be transmitted to the heat radiating film 10 in a non-contact manner using the laser generator 2. When the thermal energy is supplied to the heat-radiating film 10 in a noncontact manner as described above, there is no element to be in contact with the heat-radiating film 10 as compared with the contact type heating, It is possible to accurately determine how much heat is applied and how much heat is dissipated.

The measuring step is a step of measuring the temperature of the local region of the heat-radiating film 10 heated through the heating step. The local temperature of the heat-radiating film 10, which has been heated, As the heat begins to dissipate, the increase in temperature starts to converge.

According to another embodiment of the present invention, the measuring step is performed in a non-contact manner using an infrared thermometer (3).

When the surface temperature of the heat-radiating film 10 is measured in the non-contact manner as described above, there is no element to be in contact with the heat-radiating film 10 as compared with the contact-type temperature measurement. 10) can be measured. Furthermore, it is possible to accurately determine how much heat is applied to the heat radiating film 10 and how heat is dissipated.

4 is a perspective view showing a state in which heating of the heat radiation film and temperature measurement are progressed at the same time.

According to an embodiment of the present invention, the heating step and the measuring step may be performed simultaneously. That is, the local region of the heat-radiating film 10 is heated in contact or non-contact manner, and the temperature of the local region of the heat-radiating film 10 is measured in real time. Therefore, the time required to evaluate the thermal performance of the heat radiation film can be reduced, and the temperature change due to heating of the local region can be more accurately measured.

The determination step evaluates the thermal performance of the heat radiation film 10 based on the temperature at which the temperature change of the heat radiation film 10 measured in the measurement step is less than the temperature change. More specifically, in the determination step, it is determined that heat transfer and heat dissipation are performed better as the temperature of the heat dissipation film 10 increases while the temperature at which the heat dissipation film 10 converges is lower.

6 is a graph showing the temperature change of the heat-radiating film measured using an infrared thermometer.

If it is assumed that the thermal performance of the two heat dissipation films 10 is evaluated, since the heat dissipation film having a high temperature (T2) at which the surface temperature increases as described above is not properly heat-transferred and heat-dissipated, It is judged that the thermal performance is excellent because the heat radiation film having a low temperature (T1) at which the surface temperature is increased and the temperature is converged is properly heat-transferred and heat-dissipated.

According to an embodiment of the present invention, thermal performance of a plurality of heat-radiating films manufactured by different methods can be evaluated at the same time.

In this case, each of the heat radiating films 10 should have the same size and thickness, and the heating temperature and the heating time should be heated under the same conditions, and the temperature should be measured in the same manner.

Meanwhile, the heat radiation film 10 may be heated and measured while being mounted on the substrate 1.

At this time, the substrate 1 should be formed to have the same material and thickness. In addition, the material of the substrate 1 should be selected to correspond to the situation in which the heat radiation film 10 is actually applied.

As described above, according to the method of evaluating the thermal performance of the heat radiating film according to the present invention, it is possible to evaluate the thermal performance of the heat radiating film by a relative comparison method. Therefore, compared with the method of measuring the absolute value of the thermal performance, There is an advantage that an excellent heat-radiating film can be selected.

5 is a view showing a thermal performance evaluation of a heat radiation film using a Raman spectrometer.

According to another embodiment of the present invention, the heating step is performed by irradiating a laser L to a local region of the heat dissipation film through a laser generator 4 included in a Raman spectrometer. At this time, the heat-radiating film 10 may include crystalline particles.

Raman spectroscopy refers to a spectroscopic method for obtaining the frequency of a molecule in the Raman effect, which is a phenomenon in which scattered light having a frequency corresponding to a frequency of a molecule is generated when a strong monochromatic excitation light such as a laser beam is irradiated. Thus, in general, a Raman spectrometer includes a light source, and in particular, a laser light source. Raman spectra are recorded by a Raman spectrometer.

The measuring step measures the tendency of a peak of the Raman spectrum generated in the heat radiating film 10 to be redshift. For this, a photodetector 5 included in a Raman spectrometer can be used.

For example, when the peak of the Raman spectrum has a lot of redshift, it can be seen that the peak of the raman spectrum has increased significantly. Redshifts are less likely to be observed as temperature rises.

The determining step determines the thermal performance by comparing the degree of the redshift of the peak of the Raman spectrum in the measuring step. For example, when the peak of the Raman spectrum has a lot of redshifts, it is determined that the heat radiation performance is poor. On the contrary, when the Raman spectrum has a raman spectrum, It can be judged that the heat radiation performance is excellent because the temperature is lowered when the peak progresses with less redshift.

When the thermal performance of the heat-radiating film is evaluated by the above-described method, it is possible to develop a heat-radiating film having a high thermal conductivity, which is verified with respect to thermal performance. When a heat-radiating film is applied to an actual product, overheating of a local heat source can be prevented, The heat generated in the heat dissipating unit can be effectively spread over a large area and heat dissipation can be achieved.

While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it will be understood by those skilled in the art that various changes and modifications may be made without departing from the scope of the invention.

Accordingly, the true scope of protection of the present invention should be determined only by the appended claims.

1: substrate
2,4: Laser generator
3: Infrared thermometer
5: Photodetector
10: heat-radiating film

Claims (5)

A method of evaluating a thermal performance of a heat radiation film,
A heating step of heating a local region of the heat radiation film,
A measuring step of measuring a temperature change of a local region of the heat-radiating film heated through the heating step;
And determining a thermal performance by comparing the temperature measured by the measuring step with the temperature at which the measured temperature is increased.
The method according to claim 1,
Wherein the heating step comprises irradiating a laser to a local portion of the heat radiation film.
The method according to claim 1,
Wherein the measurement step is performed in a non-contact manner using an infrared thermometer.
The method according to claim 1,
Wherein the heating step and the measuring step are performed at the same time.
The method according to claim 1,
Wherein the heating step is performed by irradiating a laser to a local region of the heat dissipating film through a laser generator included in a Raman spectrometer, The method of claim 1, wherein the determining step comprises a step of comparing the degree to which the peak of the Raman spectrum is redshifted in the measuring step, And determining the thermal performance of the heat radiation film.
KR1020140069703A 2014-06-09 2014-06-09 thermal performance testing method of radiating film KR20150141096A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20180093867A (en) 2015-12-17 2018-08-22 니폰 덴키 가라스 가부시키가이샤 Manufacturing method of glass plate
CN115062462A (en) * 2022-06-08 2022-09-16 南京贝迪新材料科技股份有限公司 Intelligent heat transfer performance evaluation method and system for ultrathin heat dissipation film

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20180093867A (en) 2015-12-17 2018-08-22 니폰 덴키 가라스 가부시키가이샤 Manufacturing method of glass plate
CN115062462A (en) * 2022-06-08 2022-09-16 南京贝迪新材料科技股份有限公司 Intelligent heat transfer performance evaluation method and system for ultrathin heat dissipation film
CN115062462B (en) * 2022-06-08 2024-05-03 南京贝迪新材料科技股份有限公司 Intelligent assessment method and system for heat transfer performance of ultrathin heat dissipation film

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