KR20150033896A - The extraction method of pure sulfur after removing toxic from a sulfur-containing mineral and how to take advantage of it. - Google Patents

The extraction method of pure sulfur after removing toxic from a sulfur-containing mineral and how to take advantage of it. Download PDF

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KR20150033896A
KR20150033896A KR20130113734A KR20130113734A KR20150033896A KR 20150033896 A KR20150033896 A KR 20150033896A KR 20130113734 A KR20130113734 A KR 20130113734A KR 20130113734 A KR20130113734 A KR 20130113734A KR 20150033896 A KR20150033896 A KR 20150033896A
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South Korea
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sulfur
distilled water
mineral
water
pure
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KR20130113734A
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Korean (ko)
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김영국
김진호
정상화
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김영국
정상화
김진호
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Publication of KR20150033896A publication Critical patent/KR20150033896A/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03BSEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
    • B03B5/00Washing granular, powdered or lumpy materials; Wet separating
    • B03B5/28Washing granular, powdered or lumpy materials; Wet separating by sink-float separation
    • B03B5/30Washing granular, powdered or lumpy materials; Wet separating by sink-float separation using heavy liquids or suspensions
    • B03B5/32Washing granular, powdered or lumpy materials; Wet separating by sink-float separation using heavy liquids or suspensions using centrifugal force
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/02Preparation of sulfur; Purification
    • C01B17/0232Purification, e.g. degassing

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)

Abstract

A very small amount of toxic substances included in mineral sulfur (S) can be classified as arsenic (As-Arsenic), cadmium (Cd-Cadmium), mercury (Hg-Mercury), lead (Pb-Lead), chrome (Cr-Chroma), and nickel (Ni-Nikel). The present invention relates to a method for extracting pure sulfur with a purity of 99.99% by removing a toxic substance. According to the present invention, 20% of mineral sulfur and 80% of distilled water are put together in an extractor in vacuum at high-temperatures (200 to 300°C) and pressures (2 to 3 atmospheres), and the mineral sulfur and the distilled water are heated for one hour. Since mineral sulfur is well dissolved in water at a temperature equal to or more than 117°C, gas having a light specific gravity (pure O2) is evaporated, when the distilled water heating-dissolved by a concentrating process passes through a super cooler, thereby collecting only the distilled water having a dissolved sulfur. Sulfurous water is manufactured through a process (a filtering step) of precipitating the reactant and filtering out the sludge of the precipitated reactant, wherein the sulfurous water contains 5 to 30 parts by weight % of sulfur component as an active component, the sulfur component is included in a form of sulfur particles, sulfur compounds, ions of the sulfur compounds, or sulfur solution. The small amount of toxic included in the sulfur distilled water, which is the arsenic, chrome, lead, mercury, etc., are removed in the following high-speed centrifugal separation process depending on a specific gravity of the materials, and pure sulfur is extracted. The purified sulfur is extracted from the sulfur containing ion in the distilled water so as to to be formed in nanoparticles. The purified sulfur from which a toxic substance is removed can be safely utilized as a replacement component of a vegetable sulfur (MSM) in various fields.

Description

A method of extracting pure sulfur from toxic substances in mineral sulfur, and a method of utilizing the same. {The extraction method of sulfur is a sulfur-containing mineral and how to take advantage of it.

Sulfur (S): The melting point is 120 and the specific gravity is 1.92. It is a yellowish, odorless, crisp crystal at room temperature. It forms a sulfide by combining with almost all metals and hydrogen except gold and platinum at high temperatures. When ignited, a blue flame is formed. It is used for raw materials for gunpowder and matches, and for making medicinal pesticide pulp.

The toxicities contained in mineral sulfur (S) are classified as arsenic (As-Arsenic). Cadmium (Cd-Cadmium). Mercury (Hg-Mercury). Lead (Pb-Lead). Chromium (Cr-Chroma). Nickel (Ni-Nickel).

This is an invention that removes toxicity based on a technical process and extracts sulfur with a purity of 99.99%.

Sulfur is an ore substance consisting of flour corresponding to atomic number 16, period 6 group (group) period of element, which is used to chemically neutralize acidic soil and to eliminate the red tide phenomenon of seawater. This is because of the freshness of sulfur, that is, sulfur is an element of the Periodic Table of Elements such as oxygen, oxygen and sulfur without animals, plants and can not survive the life of sulfur, oxygen and biological breathing, assimilation, metabolism is indispensable It is the most important substance.

There are 14 kinds of biological elements that constitute the human body including hydrogen (H), oxygen (O), nitrogen (N), sulfur (S), sodium (Na) These elements are subjective elements that account for 99.99% of the total elements constituting the human body, of which sulfur is the eighth largest in our body.

Our bodies are made of water and fire, and when the water and the fire are in harmony with each other, the healthy body and the best energy are maintained. Water and fire are antagonistic, but when the pole reaches the top, it is the nature of Ichiyo providence to reconcile with mutual life.

Sulfur plays a role in supplementing the essentials of this most basic life activity. If the 20th century was vitamins, the emperor of nutrients, the 21st century will be the era of sulfur. This is because there is a mysterious detoxifying action that adversely attacks heavy metals, harmful substances, and chemical poisons, which are the biggest enemies of modern people's health routes, than sulfur elements.

It is time for the modern people to desperately need sulfur. Therefore, the legal sulfur is a century-old forbidden to revive people (hereinafter referred to as "sulfur" for convenience). At the present American alternative medicine hospital, sulfur capsules are used as anticancer, antidote, muscle pain, pain reliever, , An inflammation treatment agent, a skin external agent, and the like. Especially, sulfur cosmetics such as collagen, nutrition cream, cleaner, skin, body lotion, shampoo which are developed mainly with sulfur are popular.

Sulfur highlighted as new and nutrient

Adult plasma contains about 4 mg of sulfur. The sulfur amino acids methionine and cysthine also contain a small amount of sulfur. The effect of sulfur in the body has been specifically demonstrated since the animal studies conducted by Virginia Richmond in 1966 at the Seattle Pacific Northwest Research Altar were published in the Life Science magazine. Furthermore, sulfur is a new nutrient that began to emerge from the latter half of the 20th century. Let's summarize in a few ways how sulfur is applied in the human body to what kind of physiological function it has.

First, sulfur has strong pain relief.

Second, sulfur has a strong effect of cooling the inflammation.

Third, sulfur has a strong property of transporting substances, and penetrates deeply into the skin of the human body, and exerts malignancy.

Fourth, sulfur restores antioxidant and intestinal interactions, and quickly restores constipation.

Fifth, sulfur reduces the scar tissue rapidly by changing the cross-linking process of collagen, the constituent of the settlement tissue.

Sulfur as a vital essential ingredient

- The eighth essential element in human body, sulfur

There are 14 kinds of biological elements that constitute the human body including hydrogen (H), oxygen (O), nitrogen (N), sulfur (S), sodium (Na) These elements are subjective elements accounting for 99.99% of total elements constituting the human body. Among them, sulfur is the eighth highest percentage in our body.

- Sulfur existing abundantly in bones, skin, hair of human body

In human tissues, sulfur is most commonly distributed in bones, skin, and hair. These phenomena, where the hair is not glossy, the skin is wrinkled, and the nails and toenails are keratinized, are all due to a considerable deficiency of sulfur. This is evidence that sulfur is deeply involved in hair, bone and skin tissue.

The effect of sulfur on skin tissue

Sulfur is deeply involved in the osseointegration of the skin tissue (wrinkle elasticity).

First, let's look at the skin tissue to see how the sulfur acts on the skin tissue. Skin tissue is divided into epidermis (epidermis) and dermis (dermis).

The epidermis is composed of keratin protein and it prevents the loss of water. The dermal layer is made up of elastin and collagen proteins and functions to maintain elasticity.

Sulfur that detoxifies harmful substances deposited in skin tissue (caratine)

Since ancient times, mineral sulfur has been used frequently as a treatment for skin diseases. This sulfur has been closely related to the skin. Skin is a pathway connecting the external and internal tissues of the human body and is sensitive to natural environmental conditions. Therefore, it is a prerequisite for skin health to detoxify poisonous poison and toxic substances accumulating in the skin tissue in the everyday deepening environmental pollution. It is a sulfur cosmetic which is mainly composed of sulfur amino acid, which is a main component of the keratin protein structure, which further improves the keratin function of skin tissue and cleans and decodes accumulated harmful substances on the skin.

Sulfur to maintain elasticity of skin tissue (collagen)

The sign of youth is the elasticity of the skin. Going further, the skin loses its elasticity and becomes squashed. Is the skin elastic? Whether or not this is the function of collagen, the dermal layer. Therefore, the most expensive cosmetic products among them are collagen functional cosmetics. Let's look at the relationship between collagen and sulfur, which gives elasticity to skin tissue. Collagen molecules are the most abundant proteins in the human body. They have a triple helix structure and maintain high stability.

There is an enzyme called collagenase that is directly involved in this collagen molecule. It is sulfur to make several amino acid chains that make up Echolacantha now like glue. Again, sulfur acts as an adhesive to aggregate the tissues and tissues of the skin. Thus, the collagen functional action keeps the skin elastic. Thus, sulfur cosmetics combine tissues and tissues to maintain excellent elasticity on the skin.

Sulfur used as a skin external agent

In Korea, sulfur has been mainly used as a dermatitis prescription. It has been reported that Chinese intention is to mix sulfur, alum, garlic, zeolite, zinc oxide, vinegar, etc. at an appropriate ratio and apply it to the affected area.

Biochemically, sulfuric acid acts on organic matter to form pentatitanic acid (HO-SO2-S3-SO2-OH). This substance dissolves the keratin of the skin, causing insecticidal and bactericidal action. Therefore, sulfur is a nontoxic and odorless sulfur element, which helps to cool the inflammation and has a strong sterilizing power. When the patient is taking the medicine, the pain is alleviated and the surgical streak is not overwhelmed.

Thus, medical health functions in each field. It is possible to extract and safely utilize sulfur which is essentially used in pharmaceuticals without toxicity.

It is true that sulfur is good for Koreans, but it is true that it is misunderstood to exist only as mineral sulfur. Nevertheless, there are so many cases that our ancestors used in clinical practice.

- Applying loess earth wall under thatch roof (loess is called loess because it contains sulfur)

- I planted loess on top of the fields.

- Used yellow pottery in pottery, pottery and earthenware pots

- I ate pepper and miso in boiled rice.

- When bamboo salt was made, bamboo was covered with yellow clay, and pine trees were lit (bamboo shoots were sulfur components)

- When the sea breeze is heavy, it is sprayed with loess to stop the red tide (two oxygen molecules are combined with one sulfur molecule)

- Even the pigs who helped digest the loess would have to know the amazing fact that our ancestors were really close to the sulfur. It is because the pine bark, the pine bark, the pine tree powder and the pine bark were the only ones that did not lose their health even when they were dying from the pine bark when they lived in the past.

Among the pines, it is known that sea grass grown by sea breeze, especially dietary sulfur, which is the best quality in seafood is extracted, and it is found that it is contained in a large amount in algae (plankton, seaweed, sea tangle).

There are three main types of sulfur present in nature: mineral sulfur, vegetable sulfur, and animal sulfur.

- Mineral Sulfur: Sulfur (light yellow) that is exposed in the ground like a volcano, earthquake or sulfur hot spring.

- Animal volcano: Bull of the bear commonly referred to as ugum (the same as that of a pig's gall), bovine bile of the main component of Woo Hwang Chim-hwan, musk collected from the belly of a musk deer

- Vegetable Sulfur: The number can not be counted, but typical examples are saponins in ginseng, vegetables and herbs with unique orientations. Recently, it has been found that many sulfur amino acids are contained in the mulberry trees such as garlic, onion, mugwort, mugwort, agaricus, and kale, and this sulfur amino acid has been introduced as an excellent substance for treating cancer. In addition, the bamboo used in the process of manufacturing bamboo is a sulphurous amino acid mass, filling the salt, blocking the entrance with ocher, and burning the pine tree to make bamboo salt. The cloud is also a volcanic lump of sulfur rising up to the sky with water as the plankton of the sea dies.

So, we need to use the sulfur that is fed to plants around us, but now we are producing the food by covering the house, and the sulfur present in the plants is consuming all the toxins such as fertilizer and antibiotics. We are eating plants that have become so that the sulfur shortage has reached a serious situation.

Sulfur used in cosmetics and pharmaceuticals in the whole world is imported from the United States to import pharmaceuticals sulfur (MSM) through clinical trials in the United States. This is because there is no safe way to remove the toxicity contained in mineral sulfur.

The present invention is to enable the safe use of vegetable sulfur which is dependent on import by removing 100% of the toxicity of mineral sulfur, as mineral sulfur.

We have developed a toxic removal process technology in sulfur (S).

At present, mineral sulfur is toxic and it is used in small quantities by legislating by fertilizer or doctor's prescription. Of course, sulfur from the desulfurization treatment at the oil refinery facilities is also the same level.

The present invention is characterized in that mineral oil is heated to a vacuum high temperature (200 to 300 ° C) pressure (2 atm to 3 atm) extractor, distilled water is added to mineral sulfur 20% and distilled water 80% When the distilled water heated by the next process, that is, the concentration process, is passed through the water cooler, the gas (pure-O 2) having a low specific gravity is evaporated and only the distilled water in which sulfur is dissolved is collected. Wherein the sulfur water contains 5 to 30% by weight of a sulfur component as an effective ingredient, and the sulfur component is at least one selected from the group consisting of sulfur particles, sulfur compounds, Is contained in the form of an ionic or sulfuric solution of the sulfur compound, and the trace amount of toxicity contained in the sulfur distilled water, that is, arsenic. chrome. lead. Mercury and so on, depending on the weight of each substance in the next ultra-high speed centrifugation process. Only pure sulfur is extracted.

Refined sulfur can be said to be nanoparticles because sulfur extracted from ionized water is extracted in distilled water. This toxic refined sulfur is as safe as vegetable sulfur (MSM) and can be utilized as a substitute for vegetable sulfur in each field.

In principle, the sulfur used in the present invention should be excluded from the sulfur extracted from the desulfurization equipment and used pure mineral sulfur. It is a method of collecting the pure sulfur in which the mineral sulfur is removed by the following process. 1. Add mineral sulfur 20% and distilled water 80% to the mineral sulfur extractor. 2. Heat the extractor at 200 ° C to 300 ° C, 2 atmospheric pressure and 3 atmospheric pressure for 1 hour. 3. When the high-temperature sulfur distilled water dissolved in the distilled water is passed through a cooler (-30 ° C to -20 ° C), the gas (O 2) evaporates and only the dissolved sulfur distilled water remains. 4. Sulfur is dissolved in distilled water and sulfuric water is added to the high-temperature centrifuge (high-speed centrifuge - 25,000 revolutions per second).

Only pure sulfur by specific gravity is collected. Of course, it captures only the pure sulfur except the toxic substances contained in it.

Custom ordering of plant based on process chart (Standard and extractor have standard equipment according to the specifications are owned by domestic plant manufacturers. Extractor, cooler, ultra-high speed centrifuge can be installed according to the daily production.

For the present invention, it was confirmed that the pure sulfur removed from the toxic solution was collected by the separation process by the water process rather than the continuous process in each device.

1: process drawing

1. Complete elimination of toxic substances in mineral sulfur.

2. Botanical (MSM) Sulfur-dependent medical and cosmetics that can be dealt with in each field opens a cage.

3. It is possible to use each field at low price by eliminating the toxic effect of mineral sulfur.

4. The safety of sulfur produced by other feeds and fertilizers has always been problematic, and there is no management method. This method has been systematized and proven as an invention and has been applied to various fields. It is also helpful to solve red tide.

Process chart

One of the domestic production sites of mineral sulfur is the sulfuric acid protruding to the upper part of Sangdong-myeon, Sangdong-myeon, Youngwol-gun, Gangwon-do. The previous application is the tungsten mining and floodlighting method. .

When this mineral sulfur is used as the present invention, the domestic resources can be efficiently utilized, and the alternative profit is also increased, thereby making the present invention. Mineral sulfur mass was extracted and 80% of distilled water was added to the extractor at a rate of 20% of the sulfur mass in the extractor and the temperature was changed from 200 to 300 ° C. for 1 hour. When the valve is opened after pressurizing with 2-3 atmospheric pressure, the sulfur is dissolved in the distilled water in the extractor by the pressurization and the high temperature, and the sulfuric water concentrated at high temperature is sprayed. The sulfur water through the pipe is discharged to the cooler (20-30 ° C) When passing through a line that can stay for a second, pure water (O2) is evaporated into the atmosphere and the sulfur-containing sulfur water is collected according to the specific gravity. This sulfur water is put into a ultra-high speed centrifuge (25000 rpm), and it is possible to separate and collect by the specific gravity of each angle element. Of course, since it is separated from distilled sulfur water, pure sulfur can be collected more than 99.99% pure, so that toxic of mineral sulfur can be removed.

O2: Oxygen

Claims (4)

A method of using mineral sulfur as a catalyst. Mineral sulfur 20% in distiller: 80% of distilled water 200 ° -300 ° C for 1 hour to 2-3 atm. A method of collecting only distilled sulfur water dissolved in an extractor by using a cooler. A method of separating and collecting the angular and angular elements contained in the distilled sulfur water by using a high speed centrifuge.
KR20130113734A 2013-09-25 2013-09-25 The extraction method of pure sulfur after removing toxic from a sulfur-containing mineral and how to take advantage of it. KR20150033896A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20190050492A (en) * 2017-11-03 2019-05-13 주식회사 파이브네이쳐스 Method of manufacturing mineral detoxified fine particle sulfur dispersion, method of manufacturing functional animal feed additive using the same, and method of breeding livestock using the same
KR20230134167A (en) 2022-03-14 2023-09-21 김현동 Manufacturing methods of solid powdery water soluble sulfuric compounds

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20190050492A (en) * 2017-11-03 2019-05-13 주식회사 파이브네이쳐스 Method of manufacturing mineral detoxified fine particle sulfur dispersion, method of manufacturing functional animal feed additive using the same, and method of breeding livestock using the same
KR20230134167A (en) 2022-03-14 2023-09-21 김현동 Manufacturing methods of solid powdery water soluble sulfuric compounds

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