CN106821847B - Natural organic cosmetic and preparation method thereof - Google Patents

Natural organic cosmetic and preparation method thereof Download PDF

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Publication number
CN106821847B
CN106821847B CN201710067009.8A CN201710067009A CN106821847B CN 106821847 B CN106821847 B CN 106821847B CN 201710067009 A CN201710067009 A CN 201710067009A CN 106821847 B CN106821847 B CN 106821847B
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skin
extract
natural organic
xanthan gum
stirring
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CN106821847A (en
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何晓燕
冯婷婷
张云雷
朱亚真
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Nord traceability (Guangzhou) Biotechnology Co.,Ltd.
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Northwest Normal University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a natural organic cosmetic with the functions of moisturizing, whitening and resisting wrinkles, which is prepared by taking the pure dew of the bitter rose and the extract of the medlar as active ingredients according to the conventional auxiliary materials and the process for producing the cosmetic. The fructus Lycii water extract as active material contains vitamins, polysaccharides, flavonoids, polyphenols and 5-hydroxytryptamine, has effects of resisting oxidation and scavenging free radicals, can improve skin immunity and delay aging, and has effects of keeping moisture, whitening skin, and enhancing skin elasticity; the pure water rose dew has stable performance, is rich in various nutrient components such as vitamins, amino acids, flavone and the like, and has obvious effects on nourishing and moisturizing human skin, promoting skin metabolism, softening skin, inhibiting pigment precipitation and resisting aging. The invention combines the aqua ku rose hydrosol and the medlar extract, leads the efficacies of the two to be synergistic, and has more remarkable efficacies of moisturizing, whitening, delaying skin aging, enhancing skin elasticity and resisting wrinkles.

Description

Natural organic cosmetic and preparation method thereof
Technical Field
The invention relates to a natural organic cosmetic, in particular to a natural organic cosmetic taking medlar extract and bitter rose hydrosol as biological activity and a preparation method thereof, belonging to the field of fine chemical industry and articles for daily use.
Background
With the rapid development of economy and the remarkable improvement of the living standard of people, people tend to have natural, organic and safe requirements on cosmetics. Therefore, raw materials for producing cosmetics gradually tend to natural organic raw materials.
In the production raw materials of organic cosmetics in the market at present, roses are concerned. Gansu Yongden bitter rose is a representative of the strong aromatic rose, and the research of cosmetics cited at present is less. The bitter rose is also a good medicinal material, can play a role in reducing fat and losing weight, and also has good effects of moistening skin and beautifying, resisting human body aging, resisting wrinkles and the like. Researches show that the bitter rose contains multiple nutritional ingredients including polyphenol, flavone, amino acid and vitamins, and has the effects of scavenging free radicals and resisting oxidation. In addition, the bitter rose has the functions of dispelling wind, relieving pain, detoxifying and reducing swelling, and is beneficial to clearing away acnes and pimples on the face.
The Chinese wolfberry is a general name of the species under the lycium genus such as commercial Chinese wolfberry, plant Ningxia wolfberry, Chinese wolfberry and the like. The wolfberry fruits which are edible and medicinal in daily life are mostly the fruits of Ningxia wolfberry fruit, and Ningxia wolfberry fruit is the only one loaded in Chinese pharmacopoeia 2010 edition and is called as the traditional Chinese medicine four-treasure together with Qiongzhen glossy ganoderma, Changbai mountain ginseng and Dong' donkey-hide gelatin. The Ningxia wolfberry fruit is a good medicine for strengthening body resistance, consolidating constitution, producing essence, replenishing marrow, nourishing Yin, tonifying kidney, benefiting vital energy, soothing the nerves, strengthening body and delaying senility, is a top grade product for nourishing, strengthening and nourishing human from old times, effectively enhances various visceral functions, can improve brain functions and resist free radicals, and has obvious effect of delaying senility. At present, the cosmetics containing the extract of the rosa rugosa and the cosmetics containing the extract of the lycium barbarum are respectively researched, but no attention is paid to the cosmetics containing the components of the rosa rugosa and the lycium barbarum.
Disclosure of Invention
The invention aims to provide a natural organic cosmetic with the functions of moisturizing, whitening and resisting wrinkles;
another object of the present invention is to provide a method for preparing the above natural organic cosmetic.
The natural organic cosmetic is prepared by taking the pure rose aqua and the Chinese wolfberry extract as active ingredients according to conventional auxiliary materials and processes for producing the cosmetic.
The auxiliary materials are xanthan gum, citric acid, magnesium aluminum silicate, sodium alginate and glycerol.
The active ingredients and the auxiliary materials are mixed in the following ratio: in percent by weight
20-30% of bitter rose hydrosol, 30-40% of medlar extract, 0-1.1% of xanthan gum, 0-1.2% of citric acid, 1-1.2% of aluminum magnesium silicate, 0-1.2% of sodium alginate, 2-3% of glycerol and the balance of deionized water.
The bitter rose hydrosol is water left in the distillation and extraction process of essential oil, is a byproduct of the essential oil, is 100% saturated hydrosol separated in the essential oil extraction process, is natural and pure in components, and has light and pleasant fragrance.
Preparing a medlar extract: mixing the wolfberry fruit with water according to the mass-volume ratio of 1: 8-1: 10 (g/ml), heating in a water bath kettle at 75-85 ℃ for 2-2.5 hours, cooling, and filtering to obtain a liquid, namely a wolfberry fruit extract.
The xanthan gum, sodium alginate, magnesium aluminum silicate, citric acid, glycerol and other reagents are all pure products.
Preparation of organic cosmetics: firstly, adding xanthan gum into deionized water while stirring, and cooling to room temperature after completely dissolving to obtain a xanthan gum dissolving solution; and respectively adding the active ingredients and the auxiliary materials into the dissolved solution, and uniformly stirring to obtain the product.
And when the auxiliary materials contain sodium alginate, slowly adding the sodium alginate under magnetic stirring, and stirring for 20-25 minutes after adding to obtain the product.
The product prepared by the invention is uniform liquid and free of impurities, and various performance indexes of the product are shown in table 1.
TABLE 1 Performance index of inventive samples
Item The result of the detection
Appearance of the product Uniform color and no impurities
Smell(s) Mixed fragrance of bitter rose and wolfberry fruit
Total active (%) 20-24
pH(25℃) 4.8-5.7
Arsenic (As)/(mg/kg) Is free of
Heavy metals (in Pd) Is free of
Mercury (in Hg)/(mg/kg) Is free of
Because the fructus Lycii water extract used as active material contains vitamins, polysaccharides, flavonoids, polyphenols and 5-hydroxytryptamine, etc., has effects of resisting oxidation and scavenging free radicals, can improve skin immunity and delay aging, and has effects of keeping moisture, whitening skin, and enhancing skin elasticity; the pure water rose dew has stable performance, is rich in various nutrient components such as vitamins, amino acids, flavone and the like, and has obvious effects on nourishing and moisturizing human skin, promoting skin metabolism, softening skin, inhibiting pigment precipitation and resisting aging. The invention combines the aqua ku rose hydrosol and the medlar extract, leads the efficacies of the two to be synergistic, and has more remarkable efficacies of moisturizing, whitening, delaying skin aging, enhancing skin elasticity and resisting wrinkles.
In order to prove the effects of moisturizing, whitening, delaying skin aging and resisting wrinkles of the product, the following comparative tests are carried out: 30 subjects are selected, the neck and the right hand of the subject are cleaned firstly, then the skin care product is smeared on the skin care product, the left hand and the face of the subject continuously use the skin care product, the skin care product is used once in the morning and at night every day, after one month, the neck and the right hand of the subject are found to be obviously white and soft, and the elasticity and the vitality of the skin are obviously increased. The product of the invention has obvious effects of moisturizing, whitening, delaying skin aging and resisting wrinkles.
Detailed Description
The formulation and preparation of the cosmetic of the present invention are further illustrated by the following specific examples.
Example 1
The raw material ratio is as follows: in percent by weight
30% of bitter rose hydrosol, 30% of medlar extract, 1% of xanthan gum, 1% of magnesium aluminum silicate, 1% of citric acid, 2% of glycerol and the balance of deionized water.
The preparation process comprises the following steps: firstly, adding xanthan gum into deionized water while stirring, and cooling to room temperature after completely dissolving to obtain a xanthan gum dissolving solution; adding the pure water rose dew, the Chinese wolfberry extract, magnesium aluminum silicate, citric acid and glycerol into the dissolved solution respectively, and stirring uniformly to obtain the product.
Example 2
The raw material ratio is as follows: in percent by weight
20% of bitter rose hydrosol, 30% of medlar extract, 1.1% of xanthan gum, 1% of magnesium aluminum silicate, 1% of citric acid, 3% of glycerol and the balance of deionized water.
The preparation process comprises the following steps: the same as in example 1.
Example 3
The raw material ratio is as follows: in percent by weight
30% of bitter rose hydrosol, 40% of medlar extract, 1% of xanthan gum, 1.2% of magnesium aluminum silicate, 1% of citric acid, 2% of glycerol and the balance of deionized water.
The preparation process comprises the following steps: the same as in example 1.
Example 4
The raw material ratio is as follows: in percent by weight
30% of bitter rose hydrosol, 35% of medlar extract, 1% of xanthan gum, 1% of magnesium aluminum silicate, 1.2% of citric acid, 3% of glycerol and the balance of deionized water.
The preparation process comprises the following steps: the same as in example 1.
Example 5
The raw material ratio is as follows: in percent by weight
30% of bitter rose hydrosol, 35% of medlar extract, 1% of xanthan gum, 1% of sodium alginate, 1% of magnesium aluminum silicate, 1% of citric acid, 3% of glycerol and the balance of deionized water.
The preparation process comprises the following steps: firstly, adding xanthan gum into deionized water while stirring, and cooling to room temperature after completely dissolving to obtain a xanthan gum dissolving solution; adding the pure water rose dew, the Chinese wolfberry extract, magnesium aluminum silicate, citric acid and glycerol into the dissolved solution respectively, and stirring uniformly; and finally, slowly adding sodium alginate under magnetic stirring, and stirring for 20 minutes after the sodium alginate is added, thus obtaining the product.
Example 6
The raw material ratio is as follows: in percent by weight
30% of bitter rose hydrosol, 30% of medlar extract, 1% of xanthan gum, 1% of sodium alginate, 1.2% of magnesium aluminum silicate, 3% of glycerol and the balance of deionized water.
The preparation process comprises the following steps: firstly, adding xanthan gum into deionized water while stirring, and cooling to room temperature after completely dissolving to obtain a xanthan gum dissolving solution; adding the pure water rose dew, the Chinese wolfberry extract, the magnesium aluminum silicate and the glycerol into the dissolved solution respectively, and stirring uniformly; and finally, slowly adding sodium alginate under magnetic stirring, and stirring for 20 minutes after the sodium alginate is added, thus obtaining the product.
Example 7
The raw material ratio is as follows: in percent by weight
20% of bitter rose hydrosol, 40% of medlar extract, 1% of xanthan gum, 1% of sodium alginate, 1% of magnesium aluminum silicate, 2% of glycerol and the balance of deionized water.
The preparation process comprises the following steps: firstly, adding xanthan gum into deionized water while stirring, and cooling to room temperature after completely dissolving to obtain a xanthan gum dissolving solution; adding the pure water rose dew, the Chinese wolfberry extract, the magnesium aluminum silicate and the glycerol into the dissolved solution respectively, and stirring uniformly; and finally, slowly adding sodium alginate under magnetic stirring, and stirring for 20 minutes after the sodium alginate is added, thus obtaining the product.
In the above embodiments, the aqua-bitter rose hydrosol is 100% saturated hydrosol separated in the process of refining essential oil.
Preparing a Chinese wolfberry extract: mixing fructus Lycii with water at a ratio of 1:10 (g/ml), heating in water bath at about 80 deg.C for 2 hr, cooling, and filtering.
The auxiliary materials are pure xanthan gum, sodium alginate, magnesium aluminum silicate, citric acid, glycerol and other reagents.

Claims (4)

1. A natural organic cosmetic is prepared from the following raw materials by the following process:
the raw material ratio is as follows: by weight percentage, 20-30% of bitter rose hydrosol, 30-40% of medlar extract, 1-1.1% of xanthan gum, 0-1.2% of citric acid, 1-1.2% of aluminum magnesium silicate, 0-1.2% of sodium alginate, 2-3% of glycerol and the balance of deionized water;
the preparation method comprises the steps of adding the xanthan gum into deionized water under stirring, completely dissolving, and cooling to room temperature to obtain a xanthan gum dissolving solution; respectively adding active ingredients and adjuvants into the solution, and stirring.
2. A natural organic cosmetic according to claim 1, wherein: the active component of the balsam pear hydrosol is 100 percent saturated hydrosol separated in the process of refining essential oil.
3. A natural organic cosmetic according to claim 1, wherein: the preparation of the Chinese wolfberry extract comprises the following steps: mixing the wolfberry fruit with water according to the ratio of 1: 8-1: 10 g/ml, heating in a water bath kettle at the temperature of 75-85 ℃ for 2-2.5 hours, cooling, and filtering to obtain liquid, namely the wolfberry fruit extract.
4. The natural organic cosmetic according to claim 1, wherein: and finally, adding the sodium alginate under magnetic stirring, and stirring for 20-25 minutes after the sodium alginate is added, thus obtaining the product.
CN201710067009.8A 2017-02-07 2017-02-07 Natural organic cosmetic and preparation method thereof Active CN106821847B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101721337B (en) * 2009-11-20 2012-07-04 甘肃农业大学 Cosmetic containing Rosa setate X R. rugosa extract
CN103655372A (en) * 2013-12-23 2014-03-26 青岛安信医疗器械有限公司 Method for preparing rose hydrolat
CN105213261A (en) * 2015-10-28 2016-01-06 青海尤尼克生物技术有限公司 A kind of black fruit matrimony vine oxidation resistant skin care item

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