CN1316266A - Process for extracting natural medicine for pine, cypress and fir - Google Patents
Process for extracting natural medicine for pine, cypress and fir Download PDFInfo
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- CN1316266A CN1316266A CN 01107786 CN01107786A CN1316266A CN 1316266 A CN1316266 A CN 1316266A CN 01107786 CN01107786 CN 01107786 CN 01107786 A CN01107786 A CN 01107786A CN 1316266 A CN1316266 A CN 1316266A
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Abstract
A process for extracting natural medicine from the bark, root, stalk, twig, leaf, kernel and shell of pine, cypress, fir, Chinese scholartree, birch, willow and poplar includes such steps as removing impurities, cutting or crushing, drying, heating in retort to generate vapoar, condensing to obtain liquid mixture, conventional distilling, separation, cleaning, chemical analysis and dispensing.
Description
The present invention relates to from pine, cypress, fir, extract the manufacturing technology field of natural drug.
Afforestation rate in the world accounts for the long-pending 30-40% of earth surface, and the seeds in the forest, pine, cypress, China fir, birch, willow, poplar, Chinese scholartree account for 60% of whole forest.The source of timber is mostly from pine, cypress, fir, these towering trees, and well established and vigorously developing, vitality is extremely strong, no matter be in the temperate zone or the frigid zone, it is all very luxuriant to grow.Annual all have large quantities of pines, cypress, China fir after felling, transports the usefulness of each big city, its building life of hinterland to.After every tree felling, its branch, root, leaf are all abandoned in forest.Timber per ton will go out 1.5 tons of branches, root, leaf, calculates like this, and annual waste digital surprising of these timber wastes if these garbages are effectively developed, extracted natural medicinal component wherein, makes new drug, and its market prospect is very wide.The utilization of waste and old resource also is one of focus of 21st century research and development.
Chinese medicine and pharmacy is the rarity of the Chinese nation, and the successive dynasties, the medicine scholar carried out extensive studies to natural plants.According to the Compendium of Material Medica record, the purposes of pinaster is as follows:
Lignum Pini Nodi: bitter in the mouth, warm in nature, nontoxic.Evil six wind of the face that cures mainly, wind void, foot numbness pain.As: wine brewing cures mainly flaccidity of the lower limbs, joint wind.Parching to brown cures mainly disease between muscles and bones, and is wet in the dry blood of energy.Fry in shallow oil the water rinsing the mouth, it is painful to control the wind decayed tooth, or wipes effectively ashing day.
Folium Pini: bitter in the mouth, warm in nature, nontoxic.Cure mainly the rheumatism skin ulcer, piliation, settling five organs.In keeping, not hungry prolonging life.Chop up, with water and face clothes or smash ball clothes to pieces, the paddy and control foul disease of can breaking, treating chilblain wind skin ulcer effect is good, goes wind pain foot numbness, kills cadelle.Take Folium Pini, Folium Pini fritters to be ground into powder, and wine is transferred two money down before the every day food, but also liquor is made the medicated porridge food, and just clothes are difficult, then at one's convenience for a long time, make us not old, the QI invigorating of making light of one's life by commiting suicide, for a long time clothes endlessly, exhausted paddy is not hungry not thirsty.Peaceful holy benevolent prescription, day row pestilence, Folium Pini number piece, wine clothes heart.Seven takings medicine three times daily can be warded off 5 years pestilences (the typhoid fever class is wanted).Folium Pini is through concocting, and to apoplexy, wind saves, the wind pain, and the beriberi migratory arthralgia, the wind tooth swells and ache, and strong wind is disliked pain, and the scrotum pruritus due to damp pathogen is effective.
Cortex Pini: cure mainly carbuncle, ulcerous nonunion.Promoting regeneration of the tissue and arresting bleeding, control white bald, flogging injury, sore due to scald and burn, discharging fresh blood stool, incised wound flogging injury, children's's head sore.
The purposes of Cupressaceae is as follows:
Cypress is real: sweet in the mouth, property is flat, and is nontoxic.Cure mainly the palpitation with fear QI invigorating, remove rheumatism, settling five organs.Clothes make skin moist for a long time, make the people clear-headed and clear-sighted, and are not hungry not old, make light of one's life by commiting suicide and prolong life.Dimly treat, deficient suction is inhaled, heavy pain in the waist, and beneficial blood hidroschesis is controlled wind syndrome of head, and is cold in the waist kidney, the cold pus retained water of bladder, Xing Yangdao, the hundred evil ghosts and goblins that lengthen one's life, Fructus Alpiniae Oxyphyllae is allayed excitement.Burn the drop Zetou and send out, control scabies, yellow fluid eczema, old man's constipation etc.
Cacumen Platycladi (Cacumen Biotae): bitter in the mouth, tepor, nontoxic.Cure mainly haematemesis, red white in the dysentery metrorrhagia, the QI invigorating of making light of one's life by commiting suicide is made us cold-resistant summer-heat, the numbness of drying, granulation promoting.Refrigeration wind face joint pain is ended hematuria, specially controls scalds and burns, and what scar clothes were gone out in pain relieving treats legendary venomous insect dysentery, makes the soup informal dress, the five internal organs worm extremely, beneficial people.
Ramulus Biotae: the liquor wine brewing, go migratory arthralgia, severe and migratory arthralgia.Burning is got fatty oil, treats the disease scabies.Oils and fats cures mainly body surface wart order, grinds well with Colophonium and is coated with it, and a few days is from losing.
The cypress root bark: bitter in the mouth, property is flat, and is nontoxic.Treat the bright mashed skin ulcer of fire, hair growth promoting etc.
The purposes of Cunninghamia lanceolata (Lamb.) Hook. is as follows:
Lignum seu Ramulus Cunninghamiae Lanceolatae: acrid in the mouth, tepor, nontoxic.Cure mainly various skin infection, boil soup and wash it, heal invariably, to boil water soaking smoothed out with the fingers the beriberi generalized edema with distention of the chest and abdomen, and the trusted subordinate that controls of clothes goes up painful, and removes bad odor, controls the pathogenic wind toxic renal mass, gas on the cholera, and fry in shallow oil the soup clothes.
Cortex Cunninghamiae Lanceolatae: cure mainly incised wound blood and go out, and scalds and burns, get the bark from old tress charred medicinal herb with its property retained, grind clothes into powder, or add Ovum Gallus domesticus album and transfer day depositedly, promptly healed in 1st.
Semen Cunninghamiae Lanceolatae: cure mainly colicky, one-year-old one, burning is ground wine and is obeyed it.
Successive dynasties, the medicine scholar all had extensive studies and argumentation to branch, leaf, skin, root, the kind medical value of pine, cypress, fir.But owing to be subjected to the restriction of technical conditions at that time, have no idea pine, cypress, the contained composition of fir are extracted, be used for the treatment of disease more easily.Traditional Chinese medicine extraction method is difficult to form scale, and intensification is produced.Only pluck by some folk remedies, use amount is very little.So up to now, various places forest department does not have any good method to effective periodical aspect of the branch of pine, cypress, China fir, leaf, root, kind, shell, causes a large amount of branches, root, leaf, kind, shell to be discarded in the forest, wastes.Only utilized doing of pine, cypress, fir, through investigation, each forestry bureau will fell 3-5 ten thousand stere timber every year, branch, leaf, kind, shell, root the like waste that every cubic metre of timber output is 1.5 cubic metres, and the so annual garbage that just has the 4.5-7.5 ten thousand stere is lost.Research experiment result according to us shows, in the garbage per ton, can produce 30% thick product with manufacture method of the present invention, and a province is calculated by 10 forestry bureaus, and so Mei Nian garbage just can extract ten thousand tons of thick products of 13.5-22.5.These thick products are behind extraction-separation-purification-chemical analysis, and according to the character of its contained composition, the synthetic preparation of performance can be made into multiple natural drug.These natural drugs can be used for industries such as medicine, sterilization, health care, beauty treatment, food antiseptic.
According to our exquisite and calculating at present, its depleted branch of every cubic metre of timber (counting roughly 1 ton), leaf, root, kind, shell are exactly 1.5 tons, 1.5 the ton garbage can extract the 450kg medicinal liquid with this method, go on the market at present 30,000 yuan of lowest prices of medicinal liquid per ton, the 450kg medicinal liquid is just sold 1.35 ten thousand yuan so, and a big tree do 1 cube of timber, the most expensively on this cube lumber market sell 800 yuan, the garbage development product is 16.9 times of high-quality timber price.If utilize the present invention earlier, branch, leaf, the kind of big tree developed and utilized destruction that will the few virgin forest of alkali; both protected ecological environment; make the enterprise of forest department avoid closing down because of resource exhaustion again, bankruptcy has opened up new employment channel also for vast forestry laid-off worker.
The protection of virgin forest vegetation more and more is subject to people's attention, and former people's indiscriminate felling of trees causes a large amount of alkali of forest cover few, causes disruption of ecological balance; severe water and soil erosion; the extraodinary flood in 98 years, sandstorm weather in recent years is exactly the punishment that the Nature is given us.If not disafforestation is only repaired the branch, leaf, kind, nuclear, the shell that get off to big tree and combined the platform utilization, utilize the technology of the present invention to extract natural drug; open the New Development product, so both protected forest environment, benefited the mankind again; created enormous wealth, this wouldn't be to achieve many things at one stroke.
Traditional makes use of local resources, and eats woods by woods, sits idle at home eating away a fortune as big as a mountain often, and forest is fewer and feweri.And use the present invention, and only the new branch and leaf of the big tree growth of annual forest are repaired, make big tree more luxuriant.The branch and leaf that shear off make full use of, and year after year, forest constantly enlarges, when we when utilizing existing timber waste resource, new resource also increases in continuous growth, thereby inexhaustible, make ecological environment step into benign cycle, be merit now, sharp add the offspring now.The fundamental state policy of I figure " the waste and old resource of stripping increases new resources " that this has also accorded with platform.
Purpose of the present invention and method.
The purpose of this invention is to provide a kind of novel method of from trees such as pine, cypress, China fir, birch, poplar, willow, Chinese scholartree, extracting the natural drug active ingredient.
The present invention is achieved in that
1, raw materials such as individual event or the multinomial stem of choosing tree such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree, leaf, nuclear, shell, branch, kind, removal impurity fritters or pulverizes, and dries or dries, in the pyroreaction of packing into the still.Igniting or send electricity heating, treat that temperature rises to 1000 ℃ from room temperature gradually, along with the continuous rising of temperature, material converts the smoke-like gas in the still, and this gas is under the pressure of self, enter first-stage condenser along connecting pipe, become liquid through cooling segment, uncooled for the gas of liquid continues to move ahead, enter two, three grades of condensers, (this cooling procedure is a multi-stage condensing) is up to whole gases are condensed into liquid.Promptly get the crude product of contained natural drug in setting such as loose, cypress, China fir, birch, willow, poplar, Chinese scholartree after condensed fluids at different levels are collected.
2, the present invention also can match various reagent combinations according to pharmacology, performance, reinstalls to carry out dry distilling in the reactor, gets the medicine crude product.
3, crude products such as distilled pine, cypress, China fir, birch, willow, poplar, Chinese scholartree, putting into conventional distillating still carries out multistage distillation, and distills-extract-separate-purify according to the physical characteristic of contained composition.Oxious component is separated, useful composition collect medicine in the middle of product.
4, natural drug crude product, through multistage extraction-separation, the requirement that reaches quality standards basically, the reuse active carbon adsorbs, the impurity of natural drug, abnormal flavour, color are adsorbed to fall, just can obtain the elaboration of the natural drug of trees such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree.
5, the natural drug elaboration of trees such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree is carried out chemical analysis, carry out formulated in combination, synthetic Chinese patent medicine according to analysis result.
6, carry out formulated in combination according to the performance of the Natural Medicine Chemistry analysis of components of trees such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree, but the synthesis of natural disinfectant, natural biocide.
7, according to the performance of the Natural Medicine Chemistry analysis of components of tree such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree, natural drug through the preparation platform of organizing a performance becomes can be used for pharmaceuticals industry, health products trade, also can be used as dermopathic medicine for external use and oral medicine, and the prevention of various diseases and treatment.
8, according to the performance of the Natural Medicine Chemistry analysis of components of tree such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree, synthetic through preparing with the natural drug that this invention is extracted, can be used for cosmetic industry, make natural medicated cosmetics.
9, according to the performance of the Natural Medicine Chemistry analysis of components of tree such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree, with the natural drug that this invention is made, can be for food service industry as natural food-preservative.
10, according to the performance of the Natural Medicine Chemistry analysis of components of tree such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree, the natural drug made from this invention synthesizes with surfactant, can make the natural drug paint scrubber.
11, according to the performance of the Natural Medicine Chemistry composition of tree such as pine, cypress, China fir, birch, willow, poplar, Chinese scholartree, the waste liquid of the natural drug made from this invention can be made " environment friendly agricultural ", is used for the control of agricultural pest.
12, waste residue, particularly nuclear, shell, the kind of producing the natural drug of pine, cypress, birch, willow, poplar, Chinese scholartree, fir is to make the raw material of active carbon, needs only activatedly again can produce senior active carbon, and thus much one with regard to recoverable cost.
The natural drug that from pine, cypress, fir, extracts, as follows through the epidemic prevention station test basis GB15981-1995 of Jinan City " evaluation methodology and the standard of sterilization and sterilization effect " survey report: as all to reach 99.96%, 5 minute sterilizing rate and all can reach 100% to colibacillus (ATCC25922), staphylococcus aureus (ATCC6538), 2 minutes sterilizing rates of Candida albicans (ATCC1023 1) effect.The on-site disinfection test result: 5,15 minutes action time, average kill ratio was 99.96%, 100%.
The stability test result: disinfectant stock solution is after accelerated test, to colibacillus (ATCC25922) sterilization result: 2,5,10 minutes action time, average bactericidal rate is respectively 99.85%, 99.99%, 100%.
Check conclusion: meet GB15981-1995 " evaluation methodology and the standard of sterilization and sterilization effect "
Through Jinan City health and epidemic prevention station according to health ministry " disinfection technology standard " 8.3.1; Acute oral toxicity test 8.3.3; The skin irritation test, its conclusion is:
1, according to the analytical standard of acute oral toxicity test, the censorship medicine belongs to innocuous substance.
2, according to the analytical standard of skin irritation test, the censorship medicine is to White Rabbit skin nonirritant
Sense environmental conditions: 23 ℃ of relative humiditys of temperature, 34% air pressure 101.3KPa
The main test instrument and equipment:
| Numbering | Title | Model |
| ????1 | Irritate the stomach pin | ????2ml |
| ????2 | White mice | ????18-22g |
| ????3 | White Rabbit | ????2-3kg |
Claims (10)
1, from pine, cypress, China fir, birch, poplar, willow, extract the method for natural drug in the tree such as Chinese scholartree, its basic feature is: single plant or multiplely choose pine, cypress, China fir, birch, poplar, willow, the skin of tree such as Chinese scholartree, root, stem, leaf, branch, kind, nuclear, the garbage that shell and traditional handicraft can't be processed, oven dry or dry in the sun, after shearing or the coarse pulverization, in the pyroreaction of packing into the still, reacting by heating still then, make temperature in the kettle rise to 1000 ℃, time is general through 6-8 hour, in the meantime, generate the smoke-like gas in the reactor, pipeline by the reactor upper end enters condenser, through multi-stage condensing, the condensed fluid of collecting at last is pine, cypress, China fir, birch, poplar, the crude product of the natural drug of tree such as Liu Huai.
2, according to the described method of from trees such as pine, cypress, China fir, birch, poplar, willow, Chinese scholartree, extracting natural drug of claim (1), its basic feature is: the single kind or multiple root, skin, stem, leaf, branch, kind, shell, the nuclear of choosing pine, cypress, fir, pack in the reactor, carry out the crude product that high-temperature retorting gets natural drug.
3, according to the described method of from trees such as pine, cypress, China fir, birch, poplar, willow, Chinese scholartree, extracting natural drug of claim (1), it is characterized in that: can be various prescriptions, according to pharmacology, after performance prepares, reinstall and carry out the crude product that dry distilling obtains natural drug in the pyroreaction still.
4, the method for from trees such as pine, cypress, China fir, birch, poplar, willow, Chinese scholartree, extracting natural drug that is connected according to claim (1) (2) (3), it is characterized in that: the crude product that high-temperature retorting goes out, after filtration, precipitation reinstalls and carries out multistage distillation in the conventional distillating still, according to the physical characteristic of the contained chemical analysis of distillation, extract-separate, remove deleterious composition and impurity, useful composition is collected, obtain the elaboration of natural drug.
5, according to the described method of from trees such as pine, cypress, China fir, birch, poplar, willow, Chinese scholartree, extracting natural drug of claim (1) (2) (3) (4), it is characterized in that: this elaboration liquid is put into active carbon, through activated carbon adsorption, microgranule in the elaboration, impurity, abnormal flavour, color are removed, promptly got purified natural drug.
6, according to claim described in the natural drug that obtains of (1) (2) (3) (4) (5), can be used for medical treatment, medicine, health, health products trade.
7, according to claim described in the product that obtains of (1) (2) (3) (4) (5) can be used as the antibacterial of pure natural, disinfectant.
8, according to claim described in the product that obtains of (1) (2) (3) (4) (5) be the good additive of cosmetic industry and food service industry, antiseptic both can crease-resistantly be improved looks, skin care, defying age again can be anticorrosion, mildew-resistant helps improving the effect of cosmetics and the long preservation of food.
9, according to claim described in (1) (2) (3) (4) the product waste liquid, through the allotment, can synthesize " environment friendly agricultural ", be widely used in the control of the disease and pest of agriculture aspect.
10, according to the waste residue of the resulting product of claim (1) (2), be the good raw material of producing active carbon, activated again, can produce senior active carbon.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN 01107786 CN1316266A (en) | 2001-02-12 | 2001-02-12 | Process for extracting natural medicine for pine, cypress and fir |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 01107786 CN1316266A (en) | 2001-02-12 | 2001-02-12 | Process for extracting natural medicine for pine, cypress and fir |
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| CN 01107786 Pending CN1316266A (en) | 2001-02-12 | 2001-02-12 | Process for extracting natural medicine for pine, cypress and fir |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102105130A (en) * | 2008-06-24 | 2011-06-22 | 株式会社爱茉莉太平洋 | Composition for external skin application containing pine knot extract and method for preparation of the same |
| CN102125062A (en) * | 2011-03-28 | 2011-07-20 | 山东大学威海分校 | Compound lightyellow sophora root preparation and application thereof |
| CN102197832A (en) * | 2011-03-28 | 2011-09-28 | 山东大学威海分校 | Compound salix leaf preparation and application thereof |
| CN101695295B (en) * | 2009-10-19 | 2012-12-26 | 深圳诺普信农化股份有限公司 | Plant source green and environment-friendly solvent and preparation thereof |
| CN105686728A (en) * | 2016-03-14 | 2016-06-22 | 廖舟 | Mouldproof towel |
| CN106418536A (en) * | 2016-09-23 | 2017-02-22 | 河源市兴睿食品科技开发有限公司 | Selenium-enriched extract and manufacture method thereof |
| CN109463401A (en) * | 2018-11-22 | 2019-03-15 | 河南农业大学 | A kind of wooden essential oil and preparation method thereof |
| CN109893550A (en) * | 2019-03-15 | 2019-06-18 | 吴江平 | A kind of natural herb pine birch compound fluid and its application |
-
2001
- 2001-02-12 CN CN 01107786 patent/CN1316266A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102105130A (en) * | 2008-06-24 | 2011-06-22 | 株式会社爱茉莉太平洋 | Composition for external skin application containing pine knot extract and method for preparation of the same |
| CN101695295B (en) * | 2009-10-19 | 2012-12-26 | 深圳诺普信农化股份有限公司 | Plant source green and environment-friendly solvent and preparation thereof |
| CN102125062A (en) * | 2011-03-28 | 2011-07-20 | 山东大学威海分校 | Compound lightyellow sophora root preparation and application thereof |
| CN102197832A (en) * | 2011-03-28 | 2011-09-28 | 山东大学威海分校 | Compound salix leaf preparation and application thereof |
| CN102125062B (en) * | 2011-03-28 | 2013-06-05 | 山东大学威海分校 | Compound lightyellow sophora root preparation and application thereof |
| CN102197832B (en) * | 2011-03-28 | 2013-06-12 | 山东大学威海分校 | Compound salix leaf preparation and application thereof |
| CN105686728A (en) * | 2016-03-14 | 2016-06-22 | 廖舟 | Mouldproof towel |
| CN106418536A (en) * | 2016-09-23 | 2017-02-22 | 河源市兴睿食品科技开发有限公司 | Selenium-enriched extract and manufacture method thereof |
| CN109463401A (en) * | 2018-11-22 | 2019-03-15 | 河南农业大学 | A kind of wooden essential oil and preparation method thereof |
| CN109893550A (en) * | 2019-03-15 | 2019-06-18 | 吴江平 | A kind of natural herb pine birch compound fluid and its application |
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