KR20130022559A - Method of obtainging magnesiun and apparatus system for obtainging magnesiun - Google Patents

Method of obtainging magnesiun and apparatus system for obtainging magnesiun Download PDF

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Publication number
KR20130022559A
KR20130022559A KR1020110085185A KR20110085185A KR20130022559A KR 20130022559 A KR20130022559 A KR 20130022559A KR 1020110085185 A KR1020110085185 A KR 1020110085185A KR 20110085185 A KR20110085185 A KR 20110085185A KR 20130022559 A KR20130022559 A KR 20130022559A
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South Korea
Prior art keywords
magnesium
exterior
exhaust pipe
opening
discharged
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KR1020110085185A
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Korean (ko)
Inventor
김종충
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김종충
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Priority to KR1020110085185A priority Critical patent/KR20130022559A/en
Publication of KR20130022559A publication Critical patent/KR20130022559A/en

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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/20Obtaining alkaline earth metals or magnesium
    • C22B26/22Obtaining magnesium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00General methods of reducing to metals
    • C22B5/02Dry methods smelting of sulfides or formation of mattes
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D3/00Charging; Discharging; Manipulation of charge
    • F27D3/06Charging or discharging machines on travelling carriages
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D3/00Charging; Discharging; Manipulation of charge
    • F27D3/12Travelling or movable supports or containers for the charge
    • F27D2003/125Charging cars, lift trolleys
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • F27D2007/066Vacuum

Abstract

The present invention is provided with a cooling cylinder 110a-1 through which the inside penetrates up and down, and surrounds the circumferential surface on the outer surface of the upper end, and the cooling water is stored therein, and the inclined surface 110b-1 that slopes downward toward the center on the inner surface of the lower end. The formed appearance 110 and; A plurality of ribs 121 are formed radially on the outer surface, and are inserted into the interior of the exterior 110 so as to be lifted and mounted on the inclined surface 110b-1, and the ribs 121 are disposed on the inclined surface 110b-1. An inner tube 120 spaced apart from the inner surface; A cylindrical magnesium vapor deposition mechanism 130 disposed above the inner tube 120 and opened downwardly so that vaporized and rising magnesium vapor may be deposited on the inner surface thereof; Magnesium extraction furnace 100 having upper and lower covers 140 and 150 detachably installed at upper and lower ends, respectively, to seal the inside of the exterior 110: an opening 210 at a peripheral surface of the lower end of the magnesium extraction furnace 100. Support plate 200 is installed via: the body portion 311 and the inside is opened upward, the body portion 311 is provided with a wheel 311a driven through the drive means on the bottom surface, and communicates with the interior of the body portion 311 The exhaust pipe 312 and the body 311 provided inside the exhaust pipe 312 to provide a passage to be discharged through the opening 210 to be discharged through the opening 210 to be discharged to the outside and the appearance (110) Bogie 300 with a bogie body 310 provided with a collection box 313 for collecting slag falling through the lower portion of the bottom: having an inlet 410a in communication with the exhaust pipe 312, the exhaust pipe 312 Intake lines 410 for forcibly sucking the toxic gas, dust, high temperature heat discharged through the; It characterized in that it comprises a vacuum intake device 400 having an opening and closing device 420 for opening and closing the inlet portion (410a) of the intake line (410).
According to a preferred embodiment of the present invention, the magnesium extraction furnace is arranged on the bottom of the support plate vertically placed so that the upper surface of the bogie as close as possible, and connected so that the exhaust pipe extending from the bogie and the inlet of the vacuum intake apparatus are connected to each other. Under the condition, the strong suction force generated from the vacuum inhalation device is forced to suck the air between the support plate and the truck through the exhaust pipe through the exhaust pipe, and the hot air discharged together through the lower part of the magnesium extraction furnace together with the dust generated when the slag falls. By forcibly inhaling toxic gas through the vacuum intake device, it is possible not only to prevent the high temperature heat, toxic gas, dust, etc. from being diffused into the workplace and entering the respirator of the worker, but also the vacuum intake device. Strong suction force between the bottom of the support plate and the top of the bogie Since the outside air is continuously introduced through the gap, the gap between the bottom of the support plate and the top surface of the bogie can be easily sealed (sealing), so that high temperature heat, toxic gas, dust, etc. are naturally spread inside the workplace. There is an advantage to improve the working environment can be prevented.

Description

Method of Obtaining Magnesiun And Apparatus System For Obtaining Magnesiun

The present invention relates to a magnesium manufacturing method and a magnesium manufacturing system, and more specifically, to forcibly suck out dust, high temperature heat, toxic gas and the like discharged from the slag discharge from the magnesium extraction furnace through the bogie and vacuum intake apparatus The present invention relates to a magnesium production method and a magnesium production system that can prevent the diffusion of dust, high temperature heat, toxic gases, etc. into the workplace.

Magnesium is an element that is present in the earth's crust as well as in seawater.In 1808, British chemist H. Davie reduced magnesia (MgO) to metal potassium and extracted a small amount of metal for the first time. B. Reducing agent for titanium production and used as an alloy source of aluminum material. However, since 2000, it has light weight, high thermal conductivity, specific strength, heat dissipation, and has 2/3 of aluminum and 1/5 of iron. According to various material characteristics such as electromagnetic shielding, as the utilization is gradually expanded to transport equipment such as automobiles or IT industry materials, production is also rapidly increasing.

In general, smelting of magnesium metal can be divided into electrolytic and metal thermal reduction. In the early days when magnesium was discovered, mass production has been carried out through magnesium electrolysis facilities built in countries such as Norway and Canada, where low-power electricity can be supplied through hydropower from seawater or magnesite.

Since then, the magnesium heat reduction method developed by Dr. Pigeon in Canada in 1941 has been transferred to China since the mid-1990s, with high-quality, rich dolomite minerals used as raw minerals, inexpensive human resources, and no environment. Due to the rapid quantitative growth of regulations, magnesium metal production by Western-based electrolysis was reduced to the loss of competitiveness, and magnesium production by China-based thermal reduction method rapidly increased, and as of the end of 2007, global production reached 810,000 tons. In China, more than 80% of these are produced by thermal reduction in China.

Magnesium is not naturally produced in the free state, but it is widely and largely present on earth as carbonates and silicates, and the amount in the crust is the eighth place after sodium and potassium. Major mineral resources are magnesite, canalite, dolomite, talc, serpentine, etc.Magnesite, dolomite, and canrite are mainly used as magnesium raw materials for electrolysis, and dolomite is used for thermal reduction. .

Magnesium smelting Pigeon heat reduction method developed in Canada, but developed in China, mainly used anthracite coal as a fuel and used it as a heat source for calcination of dolomite and heat reduction furnace. Sox, NOx and CO As a source of environmental pollution, it is generally recognized as an energy-consuming environmental pollution facility.

In addition, the horizontal retort of the Pigeon heat-reduction furnace is a magnesium manufacturing process through external heating, which is an intermittent operation facility requiring about 8 hours of reduction and 3 hours of cooling time. On the other hand, the production of opposing magnesium has a limitation in productivity, and the operation is performed by manual labor by a large amount of manpower under poor environmental conditions.

The existing Pigeon heat reduction method is basically a horizontal heat reduction reaction tube whose shape is closed at one end, and charges the raw material for manufacturing magnesium depending on manual labor and installs a condenser with a cooling jacket at the entrance of the reaction tube. While producing a magnesium crown by heat reduction while making the inside of the furnace (vacuum) into a vacuum, the loading of the raw material and the discharge of the product had a problem that is dependent on the manpower.

In addition, the heat reduction reaction tube is also mounted horizontally in a high-temperature atmosphere furnace, and has a limitation in multi-stage installation. The heat reduction reaction tube is limited to two installations in commercial facilities, and the limitation of the installation of the heat reduction reaction tube per unit volume is limited. Furnace has a limitation in productivity, and therefore has a limitation in mass production.

In addition, in the conventional heat reduction process, anthracite coal has been mainly used as a predetermined source or energy source of the heat reduction furnace, and as a result, many environments such as SOx, NOx, and CO are generated due to dust generation and combustion of anthracite coal. Emission of pollutants is inevitable.

Therefore, this also needs to be improved.

In order to improve the intermittent operation of the Pigeon thermal reduction method, charge magnesium oxide raw material continuously calcined ore into the upper part of the furnace body, and melt it at about 1500 ~ 1600 ℃ by using a high-temperature melting furnace, and melt the silicon metal in the molten state. The Magnesite method of reducing magnesium to produce magnesium was commercially developed and commercialized in France earlier, but after the operation of the heat reduction smelting facility in the Pecheney region of France, which was commercialized for the first time due to technical limitations due to the use of electricity, This was not done, and the facility also shut down in the early 1970s.

In South Africa in the early 2000s, a similar magnesium heat reduction and smelting plant was developed up to the scale of a pilot plant.In contrast, unlike the magnesite process in which the heat reduction reaction proceeds under vacuum conditions, Mintech (Metal Tech) is developed to dissolve and smelt under high temperature conditions.

As an application using the heat reduction reaction as described above, Korean Patent Application Publication No. 10-2010-0073266 (Magnesium Production Apparatus and Magnesium Production Method Using the Same) has been disclosed.

However, the Korean Patent Application Publication No. 10-2010-0073266 (magnesium production apparatus and magnesium manufacturing method using the same) as shown in the accompanying drawings, 1, the heat reduction furnace in the state of simply placing the collection in the lower portion of the heat reduction furnace Since the reduced residue discharged from the waste is collected, the workers operating in the workplace are always exposed to the risk of safety accidents because hot and toxic gases are diffused into the workplace together with the dust of the reduced residue generated during the fall. .

The present invention has been made in order to solve the above problems, by forcibly inhaling dust, high temperature heat, toxic gas, etc. discharged during the slag discharge from the magnesium extraction furnace through the trolley and vacuum intake apparatus to dust into the workplace It is an object of the present invention to provide a magnesium production method and a magnesium production system capable of preventing the spread of hot air, toxic gases, and the like at the source.

Still another object of the present invention is to cool the hot slag discharged from the magnesium extraction furnace through a vacuum intake device to protect the worker from dangers such as burns.

According to an aspect of the present invention,

Removing the lower cover fixed at the bottom of the exterior of the magnesium extraction furnace:

An exhaust pipe is provided which has an inside opening upward and communicates with the inside, and a bogie with a collection box is disposed under the exterior of the lower cover separated, and the exhaust pipe is opened with the opening and closing device closing the inlet of the intake line. Arranging adjacent to the inlet portion so as to communicate with each other, and then sucking air into the trolley through the exhaust pipe through the suction force acting on the intake line:

Separating the upper cover fixed to the top of the exterior of the magnesium extraction furnace so that the outside air flows through the top of the exterior to be discharged through the exhaust pipe of the bogie:

Drawing a magnesium vapor deposition apparatus having magnesium metal deposited on the inner surface from the inside of the exterior to the outside, and elevating the inner tube inserted in the exterior to a predetermined height to discharge hot slag through the lower portion of the exterior:

Injecting the dolomite through the upper end of the exterior while lowering the elevated inner tube to close the inside of the lower end of the exterior, and inserting the magnesium deposition apparatus into the interior of the exterior when the input is completed:

Reinstall the top cover at the top of the facade, move the trolley to the next magnesium extraction furnace, and close the inlet of the open intake line via the switchgear:

It characterized in that it comprises the step of reinstalling the lower cover at the bottom of the appearance.

Further, according to the present invention,

An interior penetrating up and down, the outer surface of which surrounds a circumferential surface and is provided with a cooling tube for storing the cooling water therein, and an inclined surface inclined downward toward the center on an inner surface of the lower portion; An inner tube having a plurality of ribs formed radially on an outer surface thereof, the inner tube being inserted on the inclined surface so as to be liftable into the interior of the exterior, and spaced apart from the inner surface of the exterior via the ribs; A cylindrical magnesium vapor deposition mechanism disposed above the inner tube and opened downwardly so that vaporized and rising magnesium vapor can be deposited on the inner surface; Magnesium extraction furnace with top and bottom covers detachably installed at the top and bottom respectively to seal the inside of the exterior:

Support plate installed at the lower end of the magnesium extraction furnace having an opening communicating with the lower end of the magnesium extraction furnace:

The body is opened upward and the body part is provided with a wheel driven through the driving means at the bottom, and the toxic gas, dust, and hot heat discharged through the opening are installed to communicate with the inside of the body part and discharged to the outside. A bogie body with an exhaust pipe providing an aisle so as to be provided, and a collection bin installed inside the body part to collect slag falling through the lower part of the exterior:

An intake line having an inlet portion communicating with the exhaust pipe and forcibly inhaling toxic gas, dust, and hot heat discharged through the exhaust pipe; It characterized in that it comprises a vacuum intake device having a cover for opening and closing the inlet of the intake line.

According to a preferred embodiment of the present invention, the magnesium extraction furnace is arranged on the bottom of the support plate vertically placed so that the upper surface of the bogie as close as possible, and connected so that the exhaust pipe extending from the bogie and the inlet of the vacuum intake apparatus are connected to each other. Under the condition, the strong suction force generated from the vacuum inhalation device is forced to suck the air between the support plate and the truck through the exhaust pipe through the exhaust pipe, and the hot air discharged together through the lower part of the magnesium extraction furnace together with the dust generated when the slag falls. By forcibly inhaling toxic gas through the vacuum intake device, it is possible not only to prevent the high temperature heat, toxic gas, dust, etc. from being diffused into the workplace and entering the respirator of the worker, but also the vacuum intake device. Strong suction force between the bottom of the support plate and the top of the bogie Since the outside air is continuously introduced through the gap, the gap between the bottom of the support plate and the top surface of the bogie can be easily sealed (sealing), so that high temperature heat, toxic gas, dust, etc. are naturally spread inside the workplace. There is an advantage to improve the working environment can be prevented.

In addition, the hot slag discharged from the magnesium extraction furnace is collected through a trolley, and the hot heat emitted from the collected hot slag can be quickly cooled through a vacuum intake device to protect the worker from dangers such as burns. There is an advantage to this.

In addition, by further strengthening the lower cover opening and closing device to the movable main body to allow the lower cover to be automatically separated and coupled via this, in the process of separating the lower cover manually by the operator in the past, Toxic gas, dust, etc. due to the respiratory disease, there is an advantage that can protect the worker safely.

1 to 3 is a front view, a side view and a plan view of a magnesium manufacturing system according to the present invention.
4 to 6 is a side view, a plan view and a front view showing a partial cross-sectional view separately from the balance in the magnesium production system according to the present invention.
7a and 7b is a side view and a plan view showing a partial cross-sectional view of the lower opening and closing device separately in the bogie of the magnesium manufacturing system according to the present invention.
8a to 8f are flowcharts sequentially showing a method of manufacturing magnesium according to the present invention.

Hereinafter, the present invention will be described in detail with reference to the accompanying drawings.

In describing the present invention, when it is determined that a detailed description of a related known function or configuration may unnecessarily obscure the gist of the present invention, the detailed description thereof will be omitted.

1 to 3, the magnesium manufacturing system according to the present invention includes a magnesium extraction furnace 100, a support plate 200, a trolley 300, and a vacuum intake device 400.

The magnesium extraction furnace 100 is composed of an exterior 110, an inner tube 120, a magnesium deposition mechanism 130, and upper and lower covers 140 and 150, and an opening 210 of the support plate 220 to be described later. It is disposed in the) to function to extract magnesium metal from the dolomite (Dolomite) introduced between the exterior 110 and the inner tube 120 through the heat reduction reaction.

The exterior 110 is a tube through which the inside penetrates up and down, the upper portion of which is a cooling unit 110a in which a circumferential surface is cooled by a coolant, and the lower portion is a heating unit in which a circumferential surface is heated by high temperature heat ( 110b).

In particular, the cooling unit 110a is provided with a cooling cylinder 110a-1 through which coolant is introduced and discharged, and an inclined surface 110b-1 inclined downward toward the center is formed on the inner circumferential surface of the lower end of the heating unit 110b. . Here, the inclined surface (110b-1) is introduced between the exterior 110 and the inner tube 120 serves to guide the slag converted by the heat reduction reaction can be easily discharged through the lower end of the exterior (110). .

The inner tube 120 is a cylinder with both ends blocked with a plurality of ribs 121 formed radially on the outer surface, is inserted into the inside of the exterior 110 is placed on the inclined surface (110b-1), the exterior 110 Functions to open and close the inner bottom of the. More specifically, the slag converted by the dolomite and the heat reduction reaction introduced between the exterior 110 and the inner tube 120 serves to prevent the slag from falling through the lower end of the exterior 110. Here, the plurality of ribs 121 serves to maintain the gap between the appearance 110 and the inner tube (120).

The magnesium vapor deposition mechanism 130, the inside is a downwardly open tube, is inserted into the inside of the exterior 110 is disposed on the upper portion of the inner tube 120, and functions to capture the vaporized and rising magnesium vapor. In the present embodiment, the vaporized and vaporized magnesium vapor is rapidly cooled by the cooling water stored in the cooling tube 110a-1, and is deposited on the inner surface while condensation occurs inside the magnesium deposition apparatus 130. ).

For reference, protrusions (not shown) are formed on upper surfaces of the inner tube 120 and the magnesium deposition apparatus 130 so as to be easily lifted or inserted and drawn out through a separate lifting device (not shown).

Although not specifically illustrated in the present embodiment, an explosion prevention plate is installed between the inner tube 120 and the magnesium deposition apparatus 130 to prevent the explosion phenomenon from occurring inside the exterior 110 due to the temperature difference.

The upper and lower covers 140 and 150 are detachably installed at upper and lower ends so that the inside of the exterior 110 is hermetically sealed. The cross body cover bodies 141 and 151 and the disk-shaped sealing plates 142 and 152 and the cover body are installed. It is composed of the pressing bolts (143, 153) are fastened to (141, 151) to connect the sealing plates (142, 152) to the cover body (141, 151).

According to the present exemplary embodiment, the upper and lower covers 140 and 150 are disposed at the upper and lower ends of the exterior 110, and the inside of the exterior 110 is sealed while the cover bodies 141 and 151 are rotated about the vertical axis to be coupled. Tighten the pressure bolts (143, 153) as much as possible to be completely sealed by the plates (142, 152).

The structure and sealing principle of the upper and lower covers 140 and 150 as described above may be similar to the lid opening and closing principle of the hatch or pressure cooker of the submarine.

The support plate 200 is a well-known plate in which the opening 210 is formed, and in the present embodiment, the support plate 200 is installed on the peripheral surface of the lower end of the magnesium extraction furnace 100 via the opening 210 to space the magnesium extraction furnace 100. Function to adjust.

4 to 6, the trolley 300 includes a trolley body 310 having a body portion 311, an exhaust pipe 312, and a collection box 313, and the magnesium extraction furnace 100 has a predetermined interval. It is installed to be movable between the support plate 200 and the bottom surface installed to serve to collect the slag discharged from the magnesium extraction furnace (100).

The body portion 311 is a well-known cylinder having a wheel 311 a which is opened upward and has a lower surface driven through a driving means (servo motor). It is made of, and moves along the rail installed on the floor.

Although the shape of the body portion 311 is manufactured in the form of a box in the present embodiment, this is only one embodiment to the last and may be manufactured in various known forms as necessary.

In addition, in the present embodiment, the body portion 311 is shown and described as being moved along the rail installed on the floor surface via the wheel 311a, but this is only one embodiment to the last, various known as needed Since the technique of may be applied, it is not preferable to interpret the limitation.

The upper surface of the body portion 311 is arranged to be as close as possible to the bottom of the support plate 200 so that when the slag is discharged from the magnesium extraction furnace 100, dust, high temperature heat, toxic gas discharged together with the support plate ( It is preferable to minimize the leakage between the bottom surface of the 200 and the upper surface of the body portion 311.

The exhaust pipe 312 is a well-known pipe installed to communicate with the inside of the body part 311, and is connected to the inlet part 410a of the intake line 410, which will be described later, in the case of the present embodiment, and opens 210. Toxic gas, dust, and hot air discharged through the function to provide a passage for the discharge to the outside.

The collection box 313 is a well-known cylinder for collecting slag falling through the lower portion of the exterior 110 is installed in the body portion 311.

On the other hand, the body portion 311 is provided with a door (not shown) on one surface so that the inside of the collection box 313 can be easily withdrawn to the outside when the inside of the collection box 313 is filled with slag.

On the other hand, the trolley 300 is provided on one side of the trolley body 310 is further provided with a lower cover opening and closing device 320 for separating and coupling the lower cover 150 from the exterior (110).

The lower cover opening and closing device 320 is preferably installed in the direction that the cart 300 proceeds.

Referring to FIGS. 7A and 7B, the lower cover opening and closing device 320 includes a horizontal conveying part 321, a first lifting part 322, a second lifting part 323, a fixing mechanism 324, and a turn. Consists of the eastern portion 325 and the rotation cylinder 326, as mentioned above, the operation is controlled by a separate control controller (not shown) to separate and combine the lower cover 150 from the exterior 110 To perform.

The horizontal conveying unit 321 is a horizontal rail 331a that is installed side by side on the upper surface of the installation plate 314 installed on the balance body 310, and a horizontal rail guide (movable to the horizontal rail 331a) 321b and a plate-shaped base 321c fixed to the upper surface of the horizontal rail guide 321b. Here, the horizontal transfer unit 321 is the first lifting unit 322, the second lifting unit 323, the fixing mechanism 324, the rotating unit 325, the rotating cylinder 326 to be described later in the horizontal direction It functions to transfer.

The first lifting unit 322 includes a plurality of pinion gear boxes 322a installed in a quadrangular shape on an upper surface of the base 321c, and a rack 322b installed to be liftable in each pinion gear box 322a. And a plurality of shafts 322c installed between the pinion gear box 322a and transmitting power to the pinion gear box 322a, and installed in any one of the plurality of shafts 322c to rotate the shaft 322c. It is comprised from the 1st motor 322d and the upper board 322e which opened the center provided in the upper surface of the rack 322b. For reference, the first lifting unit 322 is a known power base. Here, the first lifting unit 322 has a function of raising and lowering the second lifting unit 323, the fixing mechanism 324, the rotating unit 325, and the rotation cylinder 326 which will be described later.

The second elevating part 323 has a guide part 323a-1 extending downward in the bottom direction and disposed to face each other, and is rotatably rotated through the bearing B1 on the bottom of the upper plate 322e. The lower plate 323a is installed between the upper plate 323a, the lower plate 323b installed to be elevated on the guide portion 323a-1 of the upper plate 323a, and the lower plate 323a and the lower plate 323b. It consists of the cylinder 323c which raises and lowers 323b. Here, the second lifting unit 323 serves to raise and lower the rotating unit 325 to be described later.

The fixing mechanism 324 is installed on the upper plate 323a of the second lifting unit 323 and detachably installed on the cover body 151 of the lower cover 150. For reference, the fixing mechanism 324 is a known air chuck (Air Chuck).

The rotating part 325, the second motor 325a is installed on the bottom surface of the lower plate 323b of the second lifting unit 323 and the head coupler 325b-1 detachably coupled to the pressure bolt 153. ) Is rotated in the forward or reverse direction by the second motor 325a, and constitutes a drive shaft 325b for tightening or releasing the pressure bolt 153.

The rotating cylinder 326 is a known hydraulic / pneumatic cylinder, one end of which is installed on the upper plate 322e of the first lifting unit 322, and the other end of the rotation cylinder 326 of the upper plate 323c of the second lifting unit 323. The second lifting unit 323 is installed and the fixing mechanism 324 is installed to rotate in a forward or reverse direction about a vertical axis.

The vacuum intake device 400 is composed of an intake line 410 and the opening and closing device 420 to forcibly sucks toxic gas, dust, and high temperature heat introduced through the exhaust pipe 312.

The intake line 410 has an inlet 410a communicating with the exhaust pipe 312 and is installed along the traveling direction of the trolley 300.

The opening and closing device 420 is a means for opening and closing the inlet 410a. In the present embodiment, the opening and closing device 420 opens or blocks the inlet 410a through a rotation means (motor).

In the present embodiment, the opening and closing device 420 is operated by a rotating means (motor) to open and block the inlet 410a, but it is shown and described, but this is only one embodiment to the last, and various Known techniques can be applied and practiced.

Although not specifically illustrated, a dust collector (not shown) may be installed at the end of the intake line 410.

Although not specifically illustrated, the magnesium extraction furnace 100, the bogie 300, and the vacuum intake device 400 constituting the magnesium production system according to the present invention are controlled by a central controller, that is, a controller.

Referring to the operation of the lower cover opening and closing device 320 in detail as follows.

First, the trolley 300 having the lower cover opening and closing device 320 is disposed on the bottom of the magnesium extraction furnace 100 so that the lower cover opening and closing device 320 and the lower cover 150 of the magnesium extraction furnace 100 are the same. The horizontal transfer unit 321 is controlled through a horizontal rail guide 321b that is transferred along the horizontal rail 321a to form a vertical line.

Next, when the pinion gear box 322a is operated by operating the first motor 322d of the first lifting unit 322 via the shaft 322c, the rack 322b inserted into the lifting unit 322 is lowered. Ascending and descending toward the cover 150, and finally the fixing mechanism 324 installed on the upper plate 322e of the first lifting unit 322 is reached.

As described above, in the state in which the fixing mechanism 324 reaches the lower cover 150, the cover body 151 is fixed by the fixing mechanism 324, and the second lifting unit 323 is elevated to raise and lower the head. The groove 325b-1 is inserted into the head of the pressure bolt 153, and then the driving shaft 325b is rotated through the second motor 325a of the rotating part 325 to seal the sealing plate 152. Loosen to release the pressurized state of the pressurizing bolt 153 is pressurized.

As described above, after the sealing state of the sealing plate 152 held in the pressurized state by the pressurizing bolt 153 is released by the rotating part 325, one end of the upper plate of the first lifting unit 322 ( 322e) and the other end is operated to control the rotation cylinder 326 installed on the upper plate 323c of the second lifting unit 323, the second lifting unit through the stretching movement of the rotation cylinder 326 323 is rotated about the vertical axis via the bearing (B1), which causes the fixing mechanism 324 that was fixing the cover body 151 rotates together and was fixed to the fixing mechanism 324 at the same time. The lower cover 150 also rotates together to release the coupled state.

Therefore, after releasing the fixed state of the lower cover 150, when the first lifting unit 322 is lowered vertically, the lower cover 150 is naturally separated from the appearance 110.

On the other hand, when the separated lower cover 150 is to be coupled to the lower end of the exterior 110, the lower cover 150 is coupled to the lower end of the exterior 110 by operating control in the reverse order of the above-mentioned order. .

In the present embodiment, as one of the preferred embodiments, the lower cover opening and closing device 320 is shown and described as more reinforcement provided in the trolley 300, but this is only one embodiment, for example, the lower cover opening and closing A device that performs the same function as the device 320 is installed directly on the lower cover 150 of the magnesium extraction furnace 100 so that when the bogie 300 is located in the magnesium extraction furnace 100, the lower cover 150 Since modifications may be made to be automatically separated or combined, the modified embodiment may be changed at any time.

8A to 8F, a method of manufacturing magnesium using the magnesium production system according to the present invention will be described.

(1) Lower cover removal step ( S1 )

Referring to FIGS. 8A and 8B, first, only the lower cover 150 of the upper cover 140 and the lower cover 150 which respectively seal the upper and lower ends of the exterior 110 of the magnesium extraction furnace 100 may be external ( 110) from the bottom.

When the separation process of the lower cover 150 will be described in more detail, the pressure bolt 153 is gradually released by pressing the sealing plate 152 to release the pressure state, and then the cover body 151 is centered on the vertical axis. The lower cover 150 is separated from the exterior 110 by rotating clockwise or counterclockwise.

(2) Balance placement and air intake step ( S2 )

Referring to FIG. 8C, an exhaust pipe 312 having an interior opening upward and communicating with the inside is provided at a lower portion of the exterior 110 in which the lower cover 150 is separated as described above, and a collection 313 is provided therein. The trolley | bogie 300 is arrange | positioned adjacently.

In particular, the gap between the upper surface of the trolley 300 and the bottom of the support plate 200 is arranged as close as possible, so that dust, toxic gas, high temperature through the upper surface of the trolley 300 and the bottom of the support plate 200. It is desirable to minimize the heat discharge to the outside.

In addition, the exhaust pipe 312 and the inlet 410a are disposed adjacent to each other so as to communicate with each other after the opening and closing device 420 closing the inlet 410a of the intake line 410 is opened. Air is sucked into the exhaust pipe 312 through the suction force acting on the 410.

In the present embodiment, the opening and closing device 420 is shown as being rotated by the rotation means (not shown) to open and close the inlet portion 410a, but this is only one embodiment, and various known technologies are applied. Can be.

(3) Removing the top cover S3 )

As described above, the upper cover 140 fixed to the upper end of the exterior 110 of the magnesium extraction furnace 100 in the state that arranged the trolley 300 is separated.

When the upper cover 140 is separated from the upper end of the exterior 110, external air is sucked in by the strong suction force of the vacuum intake device 400, and the external air passes through the interior of the exterior 110. It is introduced into the trolley 300 and discharged through the exhaust pipe 312 of the trolley 300.

(4) magnesium Vapor deposition apparatus  Withdrawal steps and Slag  Ejection stage ( S4 )

Referring to FIGS. 8D and 8E, when the upper cover 140 is separated, the magnesium deposition apparatus 130 having magnesium (Mg) metal deposited on the inner surface of the magnesium vapor deposition apparatus 130 may be separated by an external lifting device (not shown). Withdraw from the inside of the 110.

Next, as shown in FIG. 8E, after the magnesium deposition apparatus 130 is drawn out, it is inserted into the exterior 110 of the magnesium extraction furnace 100 and seated on the inclined surface 110b-1. The inner pipe 120 is lifted to a predetermined height through a separate lifting device (not shown).

As described above, when the inner tube 120 is lifted up, the slag disposed between the exterior 110 and the inner tube 120 is inclined surface 110b-while the interior of the exterior 110 that is closed by the inner tube 120 is opened. The free fall along 1) is introduced into the collection box 313 of the trolley 300 through the opening 210 of the support plate 200.

In particular, when hot slag falls into the collection box 313 of the trolley 300, hot heat and toxic gas are discharged together, and dust is generated by the slag dropped into the collection box 313. The hot air, the toxic gas, and the dust are forced into the intake line 410 through the inlet 410a by being forced in by the exhaust pipe 312 which is in communication with the inlet 410a of the intake line 410. Since the external air is continuously introduced through the gap between the bottom of the support plate 200 and the top of the trolley 300 by the strong suction force of the vacuum intake device 400, the bottom and the bogie 300 of the support plate 200. The gap between the upper surfaces of the) can be completely sealed (sealing) to prevent the spread of high temperature heat, toxic gas, dust, etc. into the workplace.

In addition, in the case of the hot slag collected by the collection box 313 of the trolley 300, the hot heat discharged from the hot slag is first discharged to the outside through the exhaust pipe 312, and the appearance 110 Since secondary cooling by the external air flowing into the inside of the vehicle 300 through the upper end of the), it is possible to quickly cool the hot slag.

(5) dolomite supply and magnesium Vapor deposition apparatus  Insertion step ( S5 )

Referring to FIG. 8F, the inner tube 120 that is elevated to a predetermined height is lowered again via a lifting device (not shown), and seated on the inclined surface 110b-1 of the exterior 110 to close the inside of the lower end. .

Then, dolomite containing magnesium (Mg) is introduced through the upper end of the exterior 110 to be disposed between the exterior 110 and the inner tube 120.

After dolomite is introduced between the exterior 110 and the inner tube 120 as described above, a new magnesium deposition apparatus 130 in which magnesium metal (Mg) is removed from the inner surface is lifted through a lifting device (not shown). Inserted through the upper end of the exterior 110 is placed on top of the inner tube (120).

For reference, although not specifically illustrated, an explosion prevention plate may be installed between the inner tube 120 and the magnesium deposition apparatus 130 to prevent an explosion caused by an internal temperature difference (hot and cold air). Steps may be further included.

(6) bogie moving and vacuum inhalation stage S6 )

After inserting the magnesium deposition mechanism 130 into the inside of the exterior 110 as described above, by reinstalling the upper cover 140 that was separated from the upper end of the exterior 110 to seal the upper end of the exterior 110. .

After the upper cover 140 is reinstalled as described above, the trolley 300 disposed below the exterior 110 is moved to the next (second order) magnesium extraction furnace 100.

Then, the vacuum intake device 400 is stopped, and then the inlet portion 410a of the open intake line 410 is closed by the opening and closing device 420.

As mentioned above, the opening and closing device 420 is rotated by a rotation means (not shown) to close the inlet 410a.

(7) Reinstall the bottom cover S7 )

After the trolley 300 is moved to the next (second order) magnesium extraction furnace 100, the inside of the exterior 110 is completely completed through the lower cover 150 which was separated at the bottom of the exterior 110. Seal it.

As described above, in the state in which the inside of the exterior 110 of the magnesium extraction furnace 100 is completely sealed through the upper and lower covers 140 and 150, the exterior is filled with dolomite so that magnesium vapor may be formed from the dolomite ( The outer circumferential surface of the lower end of the 110, that is, the heating unit 110b is heated to a high temperature through a burner (not shown), and the appearance of the vapor so that vaporized magnesium vapor can be condensed and deposited on the inner surface of the magnesium deposition apparatus 130. Cooling water is supplied to the circumferential surface of the upper end of the c), that is, the cooling cylinder 110a-1 formed in the cooling unit 110a.

According to a preferred embodiment of the present invention, the upper surface of the trolley 300 is disposed as close as possible to the bottom of the support plate 200 vertically placed in the magnesium extraction furnace 100, the exhaust pipe extending from the trolley 300 The support plate 200 and the support plate 200 through the exhaust pipe 312 via the strong suction force generated from the vacuum intake device 400 in a state in which the connection 312 and the inlet portion 401a of the vacuum intake device 400 are connected to each other. By allowing the air between the trolley 300 to be forcibly sucked, the hot air, toxic gas, etc., which are discharged together through the lower end of the magnesium extraction furnace 100 together with the dust generated when the slag falls, are mediated through the vacuum intake device 400. By forcibly inhaling the gas, it is possible not only to prevent the high temperature heat, toxic gas, dust, etc. from being diffused into the worker's respiratory system, but also to strongly inhale the vacuum inhaler 400. Since the external air is continuously introduced through the gap between the bottom of the support plate 200 and the upper surface of the trolley 300, the gap between the bottom of the support plate 200 and the upper surface of the trolley easily sealed (sealing) Since it can prevent the spread of high temperature heat, toxic gas, dust, etc. into the workplace, there is an advantage to improve the working environment.

In addition, by additionally reinforcing the lower cover opening and closing device 320 to the movable main body 310 to be separated and coupled to the lower cover 150 through this as a medium, the operator manually in the prior art The separation process has the advantage of protecting workers from respiratory diseases and burns due to high temperature heat, toxic gas, dust and the like.

It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the present invention as defined by the appended claims.

100: magnesium extraction furnace 110: appearance 110a: cooling unit
110b: heating part 120: inner tube 130: magnesium vapor deposition mechanism
140: upper cover 150: lower cover 200: support plate
210: opening 300: trolley 310: trolley body
311 body 312 exhaust pipe 313 collection container
320: lower cover opening and closing device 321: horizontal transfer unit 322: first lifting unit
323: second lifting unit 324: fixing mechanism 325: rotating unit
400: vacuum intake device 410: intake line 420: cover

Claims (4)

Separating the lower cover 150 fixed to the bottom of the appearance 110 of the magnesium extraction furnace 100 (S1):
An exhaust pipe 312 having an interior opening upward and communicating with the interior is disposed, and a trolley 300 having a collection box 313 therein is disposed below the exterior 110 in which the lower cover 150 is separated, and intake is performed. With the opening and closing device 420 closing the inlet 410a of the line 410 open, the exhaust pipe 312 and the inlet 410a are disposed adjacent to each other, and then in the intake line 410. Step of inhaling air into the trolley 300 through the exhaust pipe 312 via the suction force acting (S2):
The upper cover 140 fixed to the top of the exterior 110 of the magnesium extraction furnace 100 so that the outside air flows into the interior through the top of the exterior 110 to be discharged through the exhaust pipe 312 of the bogie 300. Step of separating (S3):
The magnesium deposition apparatus 130 having magnesium metal deposited on the inner surface thereof is drawn out from the inside of the exterior 110, and the inner tube 120 inserted into the exterior 110 is lifted up to a predetermined height to make the exterior 110. Discharging the hot slag through the lower portion of (S4):
The dolomite is introduced through the upper end of the exterior 110 in a state in which the lower inner tube 120 is lowered to close the inside of the exterior 110, and when the input is completed, the magnesium deposition mechanism 130 is applied to the exterior 110. Insert into the inside of (S5):
The upper cover 140 is reinstalled on the top of the exterior 110, the trolley 300 is moved to the next magnesium extraction furnace 100, and the opening and closing device 410a of the intake line 410 is opened. Closing via 420 (S6):
Magnesium manufacturing method comprising the step (S7) of reinstalling the lower cover 150 at the bottom of the appearance (110).
The inside penetrates up and down, and surrounds the circumferential surface on the outer surface of the upper end is provided with a cooling cylinder (110a-1) for storing the coolant therein, the outer surface formed with an inclined surface (110b-1) inclined downward toward the center ( 110); A plurality of ribs 121 are formed radially on the outer surface, and are inserted into the interior of the exterior 110 so as to be lifted and mounted on the inclined surface 110b-1, and the ribs 121 are disposed on the inclined surface 110b-1. An inner tube 120 spaced apart from the inner surface; A cylindrical magnesium vapor deposition mechanism 130 disposed above the inner tube 120 and opened downwardly so that vaporized and rising magnesium vapor may be deposited on the inner surface thereof; Magnesium extraction furnace 100 having upper and lower covers 140 and 150 detachably installed at upper and lower ends so that the interior of the exterior 110 is sealed:
A support plate 200 having an opening 210 which is in communication with the lower end of the magnesium extraction furnace 100, is installed at the lower end of the magnesium extraction furnace 100:
A body 311 having an inside opening upward and a wheel 311a driven through a driving means on the bottom surface thereof is installed to be in communication with the inside of the body 311 and is discharged through the opening 210. Toxic gas, dust, and the hot air that is to be discharged to the outside exhaust pipe 312 to provide a passage and the body portion 311 is installed inside the body 110 to collect the slag falling through the lower portion of the exterior 110 Balance 300 with balance body 310 provided with collection box 313:
An intake line 410 having an inlet 410a communicating with the exhaust pipe 312 and forcibly sucking toxic gas, dust, and hot air discharged through the exhaust pipe 312; Magnesium manufacturing system, characterized in that it comprises a vacuum intake device 400 having an opening and closing device (420) for opening and closing the inlet (410a) of the intake line (410).
The method of claim 2,
The trolley 300, magnesium manufacturing system, characterized in that further provided with a lower cover opening and closing device 320 is installed on the balance body 310 to separate and combine the lower cover 150 from the exterior (110).
The method of claim 3,
The lower cover opening and closing device 320,
Horizontal rails 331a installed side by side on the upper surface of the mounting plate 314 installed on the trolley main body 310, horizontal rail guides 321b movably installed on the horizontal rails 331a, and horizontal rail guides 321b. A horizontal conveying part 321 composed of a plate-shaped base 321c fixed to an upper surface of the upper and lower surfaces thereof;
Between the plurality of pinion gear boxes 322a installed in a rectangular shape on the upper surface of the base 321c, the rack 322b installed to be liftable on each pinion gear box 322a, and the pinion gear box 322a. A plurality of shafts 322c installed and transmitting power to the pinion gear box 322a, a first motor 322d installed on any one of the plurality of shafts 322c, and rotating the shaft 322c, and a rack ( A first elevating portion 322 composed of an upper plate 322e having an open center at an upper surface of the 322b;
An upper plate 323a extending downward in the bottom direction and disposed to face each other, the upper plate 323a being rotatably installed on the bottom of the upper plate 322e via a bearing B1; A lower plate 323b installed on the guide portion 323a-1 of the plate 323a to be elevated, and a cylinder installed between the upper plate 323a and the lower plate 323b to raise and lower the lower plate 323b ( A second lifting unit 323 composed of 323c;
A fixing mechanism 324 installed on the upper plate 323a of the second lifting unit 323 and detachably installed on the cover body 151 of the lower cover 150;
The second motor is provided with a second motor 325a installed on the bottom of the lower plate 323b of the second lifting unit 323 and a head coupler 325b-1 detachably coupled to the pressure bolt 153. A rotating part 325 which is rotated in the forward or reverse direction by the 325a and composed of a drive shaft 325b for tightening or releasing the pressure bolt 153;
The second lifting unit 323, one end of which is installed on the upper plate 322e of the first lifting unit 322, and the other end is installed on the upper plate 323c of the second lifting unit 323, and the fixing mechanism 324 is installed. Magnesium manufacturing system characterized in that it has a rotation cylinder (326) to rotate in a forward or reverse direction about a vertical axis.
KR1020110085185A 2011-08-25 2011-08-25 Method of obtainging magnesiun and apparatus system for obtainging magnesiun KR20130022559A (en)

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KR1020110085185A KR20130022559A (en) 2011-08-25 2011-08-25 Method of obtainging magnesiun and apparatus system for obtainging magnesiun

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101528073B1 (en) * 2013-12-24 2015-06-10 주식회사 포스코 Apparatus and method of monitoring operation data in magnesium extracting process
KR101536739B1 (en) * 2013-12-24 2015-07-14 주식회사 포스코 Device for precentig retort sticking
KR101536738B1 (en) * 2013-12-24 2015-07-14 주식회사 포스코 Device for magnesium thermal reduction
KR101536735B1 (en) * 2013-12-26 2015-07-16 재단법인 포항산업과학연구원 Manufacturing method of magnesium with radiation tube

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101528073B1 (en) * 2013-12-24 2015-06-10 주식회사 포스코 Apparatus and method of monitoring operation data in magnesium extracting process
KR101536739B1 (en) * 2013-12-24 2015-07-14 주식회사 포스코 Device for precentig retort sticking
KR101536738B1 (en) * 2013-12-24 2015-07-14 주식회사 포스코 Device for magnesium thermal reduction
KR101536735B1 (en) * 2013-12-26 2015-07-16 재단법인 포항산업과학연구원 Manufacturing method of magnesium with radiation tube

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