KR20080085418A - Matured liqueur making method in oak bottle using leaching incubated wild ginseng root - Google Patents

Matured liqueur making method in oak bottle using leaching incubated wild ginseng root Download PDF

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KR20080085418A
KR20080085418A KR1020070026903A KR20070026903A KR20080085418A KR 20080085418 A KR20080085418 A KR 20080085418A KR 1020070026903 A KR1020070026903 A KR 1020070026903A KR 20070026903 A KR20070026903 A KR 20070026903A KR 20080085418 A KR20080085418 A KR 20080085418A
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wild ginseng
liqueur
root
matured
oak
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KR1020070026903A
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KR100864941B1 (en
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장덕수
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(주)충북소주
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/05Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides
    • C12G3/055Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides extracted from plants
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/08Preparation of other alcoholic beverages by methods for altering the composition of fermented solutions or alcoholic beverages not provided for in groups C12G3/02 - C12G3/07

Abstract

Liqueur containing cultured wild ginseng root, matured in oak bottle is provided to eat easily useful components of wild ginseng together with liqueur, remove alcohol smell from liqueur and alleviate toxic taste of liqueur, and serve distinct flavor of wild ginseng and oak bottle to the liqueur. A method for preparing liqueur containing cultured wild ginseng root, matured in oak bottle comprises the steps of: (a) adding the cultured wild ginseng roots into 42-48% distilled liquor(Soju) processed by a deodorization process and firstly maturing them for 1-3 months; (b) isolating the matured cultured wild ginseng roots and storing them; (c) secondly maturing the cultured wild ginseng roots-removed matured solution in an oak; (d) filtering the secondly matured wild ginseng root-matured solution, diluting the solution to 20-40% alcohol concentration and microfiltering the solution; and (e) introducing the stored cultured wild ginseng roots into the solution during bottling process, and sealing the bottle. Further, one or more selected from sugar, oligosaccharide, honey, citric acid and amino acid is mixed into the diluted secondly matured wild ginseng root-matured solution in the step (d).

Description

산삼배양근 침출 후 오크통 숙성 리큐르의 제조방법{Matured liqueur making method in oak bottle using leaching incubated wild ginseng root}Featured liqueur making method in oak bottle using leaching incubated wild ginseng root}

도 1은 본 발명의 제조 공정도이다.1 is a manufacturing process chart of the present invention.

본 발명은 산삼배양근 침출액을 오크통에서 숙성시키고 침출된 산삼 배양근을 병입과정에서 함유시키는 새로운 형태의 기능성 리큐르의 제조방법 및 그를 이용하여 제조되는 주류에 관한 것으로서, 산삼이 지니고 있는 유효한 약리적 성분을 주류를 통해 완전하게 이용하고 특유의 산삼이 지닌 향과 맛을 조화롭게 부여하기 위하여, 희석된 주정으로 산삼배양근을 침출시키고, 추출된 산삼 배양근은 따로 분리하여 저장하며, 산삼 배양근이 제거된 주정 침출액을 오크통에서 장기간 숙성하고 희석한 후 미리 분리하여 저장된 산삼 배양근을 추가로 첨가하여 병입 포장함을 특징으로 하는 기능성 리큐르의 제조방법 및 그를 이용한 주류에 관한 것이다. The present invention relates to a method for producing a new type of functional liqueur which contains aged ginseng cultured root leachate in oak barrels and contains the leached wild ginseng cultured root in the bottling process, and an effective pharmacological component of wild ginseng is used as a liquor. In order to fully utilize and harmonize the unique flavor and taste of wild ginseng, leaching wild ginseng cultured roots with diluted spirits, separate extracted wild ginseng roots and storing them, and extracting ethanol leachate from oak barrels. The present invention relates to a method for producing a functional liqueur, and to liquor using the same.

일반적으로 술은 적당히 음용하면 스트레스를 해소하고 수면을 촉진하며 소화를 촉진하고 신진대사를 활성화하여 부차적으로 대인관계를 개선하는 등의 긍정 적인 면이 있으나, 과다 음용 시는 분해되지 못한 알코올이 체내 유해물질인 아세트알데히드(acetaldehyde)로 전환되어 두통과 속쓰림 등의 숙취현상을 나타나는 경우도 있다. 최근에 이러한 숙취현상을 완화시키려는 목적으로 다양한 특성을 지닌 즉 매실, 녹차, 복분자등의 첨가물을 함유한 기능성 주류가 상당히 개발되어 오고 있는데, 기능성 주류를 대표할 만한 것으로 리큐르(liqueur)가 있다. 리큐르는 옛날 연금술사들이 증류주에 식물 약제를 넣어 만든 술로 고대 그리스의 히포크라테스가 병자에게 힘을 주기 위하여 포도주에 약초를 넣어서 물약을 만들어 복용하게 하였다고 한 이후, 증류주에 약초, 향초, 과일, 종자류 등, 주로 식물성의 향미성분과 색을 가한 다음 설탕이나 벌꿀 등의 감미료를 첨가하여 제조하는 혼성주의 총칭으로서 아름다운 색, 짙은 향기, 약리성분을 갖는 술이다. In general, drinking alcohol has positive aspects such as relieving stress, promoting sleep, promoting digestion, and activating metabolism, thereby improving interpersonal relationships. It may be converted into acetaldehyde, which is a substance, causing hangovers such as headaches and heartburn. Recently, functional liquors having various properties, that is, additives such as plum, green tea, and bokbunja have been developed for the purpose of alleviating the hangover, and there is a liqueur that is representative of the functional liquor. Liqueurs were made by ancient alchemists who used herbal medicines in distilled liquor, and the ancient Greek Hippocrates told them to make potions by adding herbs to wine to power the sick. It is a general name of hybrid wine made by adding flavor and color of vegetable and then adding sweetener such as sugar and honey. It is liquor with beautiful color, dark fragrance and pharmacological ingredient.

산삼은 동의보감에서 "신초"라 불릴 만큼 희귀한 식물로서, 주요성분은 사포닌, 폴리아세틸렌 화합물, 폴리페놀 화합물, 산성 다당체, 기타 일반성분으로 이루어져, 항암작용, 항산화 활성, 콜레스테롤 저하효과, 암세포 증식 억제작용, 항혈소판작용(심장기능강화 및 혈행 개선), 항산화 활성, 노화억제, 면역기능의 증강, 허약체질개선, 항당뇨, 스트레스 해소, 미백활성 및 임상효과, 성기능 개선효과, 신경통, 갑상선, 불면증, 피부염치료 등의 광범위한 약리효과가 있는 것으로 알려져 있다. 최근의 생물공학적인 기법을 통해서 유효 생리활성 물질인 진세노사이드(ginsenosides)의 함량이 높은 산삼 배양근의 대량증식이 가능해졌다. 산삼을 이용하여 부정근 유도, 라인선발, 생물반응기 배양, 공장에서 대량배양, 수확, 건조 되어 대량생산에 의해 산삼배양근을 얻을 수 있게 되었다. Wild ginseng is rare enough to be called "sprout" in Dongbobogam, and its main ingredient consists of saponins, polyacetylene compounds, polyphenol compounds, acidic polysaccharides, and other common ingredients, and has anticancer activity, antioxidant activity, cholesterol lowering effect, and cancer cell proliferation. Action, antiplatelet action (enhancing heart function and improving blood circulation), antioxidant activity, anti-aging, enhancement of immune function, weakened constitution, antidiabetic, stress relief, whitening activity and clinical effect, sexual function improvement, neuralgia, thyroid, insomnia It is known to have a wide range of pharmacological effects such as dermatitis treatment. Recent biotechnological techniques enable the mass growth of wild ginseng cultured roots with high content of ginsenosides, an effective bioactive substance. Using wild ginseng, ginseng root induction, line selection, bioreactor cultivation, mass cultivation, harvesting, and drying in the plant were able to obtain wild ginseng roots by mass production.

위와 같은 산삼배양근의 다양한 생리적 기능과 효과를 주류에 적용하기 위하여, 본 발명자는 한국등록특허 제0686888호를 통해 산삼 배양근을 함유한 최적의 약주류 제조방법에 대하여 공개한바 있으며, 한국특허출원 제2006-81547호를 통해 산삼배양근 추출액과 산삼배양근을 함유한 리큐르의 제조방법에 대하여 출원한바 있다. 본 발명은 이 출원에 대한 보완적 연구결과를 통해 얻어진 것으로, 산삼 배양근을 이용하여 리큐르를 제조하는 방법에 있어서, 산삼 배양근의 약리 효과를 충분히 얻고 산삼배양근 특유의 향취와 맛이 주정의 이취를 더욱 효율적으로 마스킹하고 조화를 이룰 수 있도록, 오크(oak)통 숙성을 통하여 산삼배양근 침출액의 기호도를 높일 수 있는 산삼 배양근 성분이 함유된 최적의 리큐르 제조 공정 및 이를 이용한 각종 주류 개발을 위하여 실시되었다.In order to apply various physiological functions and effects of wild ginseng culture roots to the liquor, the present inventors have disclosed an optimal method for producing alcoholic liquor containing wild ginseng culture root through Korean Patent No. 0686888, Korean Patent Application No. 2006 No. -81547 filed for the preparation of liqueurs containing wild ginseng cultured root extract and wild ginseng cultured root. The present invention has been obtained through the complementary research results for this application, in the method of producing a liqueur using wild ginseng culture root, the pharmacological effect of wild ginseng culture root is sufficiently obtained and the smell and taste peculiar to the wild ginseng culture root more smell In order to effectively mask and harmonize, an optimal liqueur manufacturing process containing wild ginseng culture root components that can increase the acceptability of wild ginseng culture root leachate through oak barrel aging was conducted for the development of various liquors using the same.

따라서 본 발명은 오랫동안 인간에게 널리 알려진 산삼의 유용한 약리성분을 리큐르에 접목하여 알코올과 함께 섭취할 수 있도록 산삼배양근을 주정에 침출하여 리큐르 제품을 제조하는 과정에서 나타날 수 있는 주정취와 마실 때 거부감을 주는 독한 맛을 해소하기 위해, 산삼배양근을 침출시키고 오크통 숙성과정을 거쳐 음용 시에 주정취가 제거되고 산삼배양근 특유의 향미와 오크통 숙성의 효과가 조화롭게 결합되어 산삼 특유의 향미와 마시기에 부드러운 기능성 리큐르를 개발하는 것을 목적으로 한다. Therefore, the present invention is a rejection when drinking and drinking alcohol that may appear in the process of manufacturing a liqueur product by leaching wild ginseng cultured root to alcohol so that it can be ingested with alcohol by incorporating useful pharmacological ingredients of wild ginseng known to humans for a long time In order to relieve its strong taste, the wild ginseng cultured roots are removed, the oak barrels are aged, and alcoholic beverages are removed during drinking. The purpose is to develop a.

상기 목적을 달성하기 위하여 본 발명은 (a) 산삼 배양근을 탈취 과정을 거친 주정에서 침출 및 숙성시키는 단계, (b) 추출된 산삼 배양근을 분리하여 따로 저장하는 단계, (c) 산삼 배양근이 제거된 주정 침출액을 오크통에 저장하여 숙성하는 단계, (d) 숙성된 산삼배양근 주정 침출액을 희석하고 여과하는 단계, 및 (e) 상기 (b)단계에서 분리하여 저장된 산삼배양근을 병입 과정에서 다시 투입하여 포장하는 단계를 포함하는 산삼배양근을 함유하여 오크통 숙성 리큐르의 제조방법에 관한 것이다.In order to achieve the above object, the present invention comprises the steps of (a) leaching and ripening wild ginseng cultured roots in a deodorized alcoholic beverage, (b) separating and storing the extracted wild ginseng cultured roots, and (c) removing the wild ginseng cultured roots. Storing the alcoholic leachate in oak barrels for aging, (d) diluting the aged wild ginseng cultured ethanol leachate and filtering, and (e) storing the wild ginseng cultured in step (b) again in the bottling process. It relates to a method for producing oak barrel aging liqueur containing wild ginseng cultured root comprising the step of.

바람직하게는, (a) 산삼배양근을 탈취 과정을 거친 42~48% 증류식 주정에 투입하여 1~3개월간 침출 및 1차숙성시키는 단계, (b) 추출된 산삼배양근을 분리하여 따로 저장하는 단계, (c) 산삼배양근이 제거된 주정 침출액을 오크통에 저장하여 2차숙성하는 단계, (d) 2차숙성된 산삼배양근 주정 침출액을 여과하고 20~40% 알코올 농도로 희석한 후 정밀 여과하는 단계, 및 (e) 상기 (b)단계에서 분리하여 저장된 추출된 산삼배양근을 병입 과정에서 다시 투입하여 밀봉 포장하는 단계를 포함하는 산삼배양근을 함유한 오크통 숙성 리큐르의 제조방법을 제공한다.Preferably, (a) leaching the wild ginseng culture root in 42 ~ 48% distilled spirits undergoing deodorization and leaching and primary maturation for 1 to 3 months, (b) separating and storing the extracted wild ginseng culture root separately (c) storing the alcoholic liquor from which the wild ginseng culture root was removed in an oak barrel for secondary maturation, and (d) filtering the second matured wild ginseng cultured alcohol leach liquor after diluting to 20-40% alcohol concentration followed by fine filtration. , And (e) provides a method for producing an aged oak barrel liqueur containing wild ginseng cultured root, which comprises the step of sealing and packaging the extracted wild ginseng cultured root separated and stored in step (b).

더욱 바람직하게는, 통상적인 리큐르 형태의 제품을 제조하기 위하여, 상기 (d)단계에서 희석된 산삼배양근 주정 침출액에 설탕, 올리고당, 벌꿀, 구연산 및 아미노산 등의 첨가제가 추가로 배합되는 것을 특징으로 하며, 이와 같이 제조된 리큐르를 이용하여 다양한 형태의 주류 제품으로 응용될 수 있다.More preferably, in order to manufacture a conventional liqueur form of the product, an additive such as sugar, oligosaccharide, honey, citric acid and amino acid is further added to the wild ginseng root alcohol leachate diluted in step (d). By using the liqueur prepared in this way, it can be applied to various types of liquor products.

이하, 본 발명의 산삼 배양근이 함유된 리큐르 제조방법을 도면과 연관하여 상세히 설명하면 다음과 같다.Hereinafter, the liqueur manufacturing method containing the wild ginseng culture root of the present invention will be described in detail with reference to the accompanying drawings.

상기의 목적을 달성하기 위해 본 발명은 주류에 산삼 배양근의 추출과 주정비율을 이용한 기능성 리큐르의 개발에 관한 것으로, 리큐르 제조방법에 있어서 주정을 희석하여 활성탄 및 백토로 정제한 후, 산삼 배양근(110년근 산삼 → 세포조직 핵분열 → 우량 배양근 선발 → 배양근 성장 → 대량 배양 → 수확 → 건조과정을 통해 생산된 제품)을 구입하여 정제된 주정(증류식 소주)에 첨가하여 침출하고 산삼 배양근을 분리하여 다시 오크통에서 숙성시킨 침출원액을 희석하여 기타 첨가물을 배합한 후 분리 저장된 산삼 배양근을 재투입하여 병입하는 제조과정을 특징으로 한다.In order to achieve the above object, the present invention relates to the extraction of wild ginseng culture root in liquor and the development of functional liqueurs using a brewing ratio, distilled spirits in a liqueur manufacturing method, purified by activated carbon and clay, and then ginseng culture root (110). Annual root ginseng → cell nuclear fission → selection of fine culture roots → growth of culture roots → mass culture → harvesting → product produced through drying process, added to purified spirits (distilled soju), and leached. It is characterized by the manufacturing process of diluting the leaching leachate aged in the mix to mix the other additives and then re-introduced and stored wild ginseng culture root.

우선 산삼배양근 침출액을 얻기 위하여, 원주정(R1)에 지하 250미터의 천연 지하암반수를 이용하여, 30~60%, 바람직하게는 42-48% 정도로 희석한다. 적당하게는 45% 정도가 추출효과가 큰 것으로 본 발명자의 실험에 의하여 입증되었다. 희석한 주정(R2)을 탈취공정(R3) 즉 탈취효과가 뛰어난 활성탄 및 백토(고령토)로 정제한 후 건조된 산삼배양근을 희석된 주정을 기준으로 1~10중량%, 바람직하게는 3-5중량%, 적당하게는 5중량%정도를 투입(R2)한다.First, in order to obtain a wild ginseng culture root leachate, dilute to 30-60%, preferably 42-48%, using 250 m of underground underground rock water in Wonju (R1). Suitably about 45% of the extraction effect was proved by the inventors' experiment. The diluted alcohol (R2) is purified by deodorization process (R3), that is, activated carbon and white clay (kaolin) with excellent deodorizing effect, and then dried ginseng cultured root is 1 to 10% by weight based on the diluted alcohol, preferably 3-5 Wt%, suitably about 5% by weight is added (R2).

산삼배양근의 약효성분이 충분히 침출될 수 있도록 수개월 동안, 바람직하게는 약 1~3개월 동안 15~60℃의 온도에서 침출(R3)한 후 산삼배양근을 분리(R4)하여 따로 저장한다. 상기에서, 침출 기간이 1개월 미만이면 산삼 배양근의 약효 성분이 유의적으로 나타나질 않도록 약하게 우러나고, 3개월 이상이면 과침출로 인한 이취나 쓴맛이 발생할 수 있다. In order for the active ingredient of wild ginseng culture root to be sufficiently leached for several months, preferably about 1 to 3 months at a temperature of 15 ~ 60 ℃ leaching (R3) after separating the wild ginseng culture root (R4) and stored separately. In the above, if the leaching period is less than 1 month weakly so that the active ingredient of wild ginseng culture root does not appear significantly, more than 3 months may result in off-flavor or bitter taste due to over leaching.

산삼배양근이 분리된 침출원액을 주질의 조화를 위해 15~60℃의 온도에서 1년 내지 15년 동안, 오크(oak)통에 저장(R5)하여 재숙성(R6) 과정을 거친다. 오크 나무 조직에 함유돼 있는 폴리페놀(polyphenols) 성분 중 탄닌(tannin), 바닐린(vanillin) 성분이 산삼배양근 리큐르의 맛과 향에 결정적인 영향을 준다. 특히, 탄닌 성분은 산삼배양근 리큐르를 마실 때 입안에서 느낄 수 있는 전체적인 중량감(body)을 느끼는데 기여한다. 한편 바닐린 성분은 숙성과정에서 산소와의 미세한 산화작용을 거쳐 산삼배양근 특유의 향기 성분과 조화되어 은근히 향긋한 목향으로 나타나게 된다.The leachate from which the wild ginseng cultured root is separated is stored in an oak barrel (R5) for 1 to 15 years at a temperature of 15 to 60 ° C. for reconstitution of the main body and undergoes re-aging (R6). Among the polyphenols contained in oak tree tissue, tannin and vanillin have a decisive effect on the taste and aroma of wild ginseng root liqueur. In particular, the tannin component contributes to feeling the overall weight (body) that can be felt in the mouth when drinking wild ginseng cultured liqueur. On the other hand, vanillin component is finely oxidized with oxygen during the aging process and harmonizes with the unique fragrance ingredient of wild ginseng culture root and appears as a silky fragrance.

오크 나무는 다공질의 조직으로 통 속의 산삼배양근 침출액과 외부의 공기가 천천히 순환되면서 침출주에 용해되어 있는 탄산가스 등이 배출되고 산소와 침줄주 성분의 상호작용에 의해 맛이 풍부해지고 안정적인 숙성과정을 유도한다. 오크통은 다양한 종류(오크, 아카시아, 밤나무 등)의 것이 사용될 수 있으며, 바람직하게는 라이트(light) 또는 중간 토스트(medium toast)의 색깔을 지닌 오크통이 사용된다. Oak tree is a porous tissue, and the acid ginseng root leaching liquid in the barrel and the outside air are slowly circulated to release carbon dioxide dissolved in the leaching liquor. do. Oak barrels may be of various kinds (oak, acacia, chestnut, etc.), preferably oak barrels of a color of light or medium toast are used.

이렇게 장기간 침출 및 숙성 기간을 거친 산삼배양근 침출원액을 희석용 정제수를 이용하여 10~40%, 바람직하게는 20-40%로 희석, 적당하게는 25%의 원액(R7)을 제조한다. 원액 제성(R7)과정에서 추출원액을 배합탱크에 채우고, 리큐르제조에 필요한 첨가물, 예를 들면 설탕, 올리고당, 벌꿀, 구연산, 아미노산 등을 소정량, 바람직하게는 최종 희석된 리큐르를 기준으로 0.01~5중량% 첨가하여 배합(R8)하도록 한다.The acid ginseng root leaching stock solution, which has undergone a long leaching and ripening period, is diluted to 10-40%, preferably 20-40%, using a purified dilution water to prepare a stock solution (R7) of 25%. In the process of preparing the stock solution (R7), the extraction stock solution is filled into the blending tank, and additives necessary for preparing the liqueur, for example, sugar, oligosaccharide, honey, citric acid, amino acid, etc., are added in a predetermined amount, preferably based on the final diluted liqueur. 5 weight% is added to mix (R8).

상기와 같이 배합탱크에서 고르게 배합된 산삼배양근 추출원액 100%가 포함된 리큐르 혼합물을 정밀 여과공정을 거쳐(R9) 미세입자를 제거한 후 제품저장 탱크로 보내어 저장된 상태에서 제품라인으로 배관을 통하여 이송된 제품에 앞 공정(R4)에서 분리 저장된 산삼배양근을 병입과정에서 총 중량의 약 1~10중량%, 바람직하게는 2-3중량%를 재투입하여(R10) 병입 및 캡핑(R11) 등의 포장과정을 거쳐 제품화 된다(R12).The liqueur mixture containing 100% of the ginseng cultured root extract extracts evenly blended in the blending tank as described above was removed by fine filtration (R9) to remove the fine particles and then sent to the product storage tank and transferred to the product line through the pipe in the stored state. In the process of bottling the wild ginseng cultured muscle separated and stored in the previous step (R4), the product is re-introduced (R10) and packaged such as bottling and capping (R11). It is commercialized through the process (R12).

이하 본 발명의 내용을 하기 실험예 및 실시예 의해 보다 상세하게 설명하기로 한다. 다만, 이들 실시예는 본 발명의 내용을 보다 쉽게 이해하기 위해 제시되는 것일 뿐 본 발명의 권리범위가 이들 실시예에 의해 한정되는 것은 아니다.Hereinafter, the content of the present invention will be described in more detail by the following experimental examples and examples. However, these examples are only presented to more easily understand the contents of the present invention, the scope of the present invention is not limited by these examples.

<실험예: 침출 기간에 따른 유효성분 추출> Experimental Example: Extraction of Active Ingredients According to Leaching Period

주정을 지하 250미터의 천연암반수로 45% 정도로 희석한 주정을 활성탄 및 백토로 정제한 후 건조 산삼배양근을 희석된 주정을 기준으로 5중량% 투입하고, 라이트 토스트 계열의 미국산 오크통에서 산삼배양근의 약효성분이 충분히 침출될 수 있는 적정 기간을 알기 위하여 15일, 1개월, 2개월, 3개월, 4개월 또는 5개월 동안 상온에서 침출한 후, 포어(pore) 사이즈 0.45㎛ 여과막을 통해 분리하여 산삼배양근 주정 침출액을 준비하였다. 침출 기간에 따른 조사포닌(crude saponins)과 진세노사이드(ginsenosides) 함량을 분석하여 표1과 같은 결과를 얻었다.  After distilling alcohol from 45% of basement with 250m underground rock, refined alcohol with activated carbon and clay, and added 5% by weight dry ginseng cultured roots based on diluted alcohol. In order to know the proper period for the components to be sufficiently leached, leaching at room temperature for 15 days, 1 month, 2 months, 3 months, 4 months or 5 months, and then separated through a pore size 0.45㎛ filtration membrane Alcohol leachate was prepared. The results of Table 1 were obtained by analyzing the contents of irradiation saponins and ginsenosides according to the leaching period.

조사포닌은 한국식품공전법에 의하여 검체를 감압농축하고 에틸에테르(ethylether)로 가열하여 탈지한 후 잔류물의 항량을 측정한 후 공전의 공식에 따라 조사포닌 양을 계산하였고, 진세노사이드 함량은 고속액체크로마토그래피(HPLC)법 (고성권 등, 한국식품과학회지, 2003, 35(3), 536-539)을 통하여 분석하였으며, 침출 원액 리터당 검출된 양(mg)으로 표기하였다.Investigation was carried out by deconcentrating the sample under reduced pressure, heating it with ethyl ether, and degreasing the sample by the Korean Food Code. It was analyzed by HPLC (HPLC) method (Goseong Kwon, et al., 2003, 35 (3), 536-539) and expressed in mg (liter) detected per liter of leaching stock solution.

침출 기간Leaching period Crude saponins (mg/L)Crude saponins (mg / L) Total ginsenosides (mg/L)Total ginsenosides (mg / L) 15일15th 331331 9999 30일30 days 478478 168168 60일60 days 520520 188188 90일90 days 587587 198198 120일120 days 589589 192192 150일150 days 608608 191191

표 1에 나타난 바와 같이, 침출 기간이 1개월 미만이면 조사포닌과 총 진세노사이드 성분이 낮은 수치로 침출되었고, 2 내지 3개월이 지나면서 부터는 급격한 증가가 이루어지지 않는 것을 알 수 있었다. 이후 부터는 오히려 과침출로 인한 이취나 쓴맛이 발생할 우려가 있는 것으로 나타났다. 따라서 침출기간은 1달 내지 3개월 정도인 것이 바람직하였다.As shown in Table 1, when the leaching period was less than 1 month, the irradiated with low values of irradiated saponinin and total ginsenosides, it can be seen that a sharp increase does not occur after 2 to 3 months. Since then, there is a possibility that odor or bitter taste may occur due to over leaching. Therefore, the leaching period is preferably about 1 month to 3 months.

<실시예> <Example>

원주정에 지하 250미터의 천연암반수를 이용하여, 45% 알코올 농도로 희석한 주정을 활성탄 및 백토로 정제한 후 시중에서 구입한 건조된 산삼배양근을 희석된 주정을 기준으로 5중량% 투입하고, 산삼 배양근의 약효성분이 충분히 침출될 수 있도록 1개월 동안 상온에서 침출한 후 산삼배양근을 분리하여 따로 저장하고, 침출원액은 여과 후 주질의 조화를 위해 일반 스테인레스 발효통(실시예 1) 또는 라이트 토스트 계열의 미국산 오크통(실시예 2 내지 8)에 충진한 후 상온에서 12개월 동안 재숙성 하였다.        After distilled alcohol with distilled alcohol at 45% alcohol concentration was refined with activated carbon and white clay, the dried wild ginseng cultured root was purchased at 5% by weight based on the diluted alcohol. After leaching at room temperature for 1 month so that the medicinal components of wild ginseng culture root can be sufficiently leached, the wild ginseng culture root is separated and stored separately. After filling in American oak barrels (Examples 2 to 8) were re-maturated for 12 months at room temperature.

이렇게 장기간 침출 및 숙성 기간을 거친 산삼배양근 침출원액을 희석용 정제수를 이용하여 25%의 원액을 제조하고, 오크통에서 숙성된 침출액 중 일부에 리큐르제조에 필요한 첨가물인 설탕 1중량% (실시예 3), 올리고당 1중량% (실시예 4), 벌꿀 1중량% (실시예 5), 설탕 1중량% + 구연산 0.2중량% (실시예 6), 또는 설탕 1중량% +구연산 0.2중량% + 복합 아미노산 0.1중량% (실시예 7)를 첨가하여 배합탱크에서 고르게 배합된 산삼배양근 침출원액이 포함된 리큐르 혼합물을 정밀 여과공정을 거쳐 미세입자를 제거한 후 미리 분리 저장된 산삼배양근을 병입 과정에서 총 중량의 3중량%를 재투입하여 병입하여 실시예들을 제조하였다.Thus, a 25% stock solution was prepared using distilled purified water from wild ginseng root leachate after a long leaching and aging period, and 1 wt% of sugar, which is an additive required for liqueur production, to some of the leach liquors aged in oak barrels (Example 3) , 1 weight% oligosaccharide (Example 4), 1 weight% honey (Example 5), 1 weight% sugar + 0.2 weight% citric acid (Example 6), or 1 weight% sugar + 0.2 weight% citric acid + complex amino acid 0.1 3% by weight of the total weight of the liqueur mixture containing the wild ginseng root leaching stock evenly mixed in the mixing tank by removing the fine particles after the fine filtration process to remove the fine particles by adding the weight% (Example 7) Examples were prepared by refeeding% and bottling.

본 실시예에서 제조된 산삼배양근 오크통 숙성 리큐르를 산삼배양근이 첨가되지 않은 25%의 희석식 소주(비교예)와 함께 성인남녀 50명을 대상으로 관능시험을 실시하여 그 결과를 다음의 표 2에 나타내었다. 관능검사는 맛, 풍미, 색깔 및 전체적인 기호도의 4개 항목에 대해 실시하였으며, 5점 만점을 기준으로 다음의 평가기준에 의하여 피시험자가 점수를 기록한 후 이의 평균을 계산하였다. Sensory test of 50 adult men and women with 25% dilute soju (comparative example) in which wild ginseng cultured oak barrel aging liqueur prepared in this example was not added, and the results are shown in Table 2 below. It was. The sensory test was conducted on four items of taste, flavor, color and overall acceptability, and the average was calculated after the test subject recorded the score according to the following evaluation criteria based on the five-point scale.

5: 아주 좋다 (거부감의 경우 전혀 없다), 4: 좋다 (거부감의 경우 없다), 3: 보통 2: 나쁘다 내지는 좋지 않다 (거부감의 경우 약간 있다), 1: 아주 나쁘다 (거부감의 경우 있다).5: Very good (no rejection at all), 4: Good (no rejection), 3: Normal 2: Bad or not good (some rejections), 1: Very bad (some rejections).

flavor 풍미zest 색깔Color 전체적인 기호도Overall preference 비교예Comparative example 2.92.9 2.92.9 3.53.5 3.13.1 실시예 1(일반 발효통 숙성)Example 1 (General fermentation barrel ripening) 3.63.6 3.43.4 3.93.9 3.73.7 실시예 2(오크통 숙성)Example 2 (oak aging) 3.93.9 3.83.8 4.04.0 3.93.9 실시예 3(오크통/설탕)Example 3 (Oat Bucket / Sugar) 4.14.1 3.83.8 4.04.0 4.04.0 실시예 4(오크통/올리고당)Example 4 (Oil Bucket / Oligo Sugar) 4.04.0 3.73.7 4.04.0 3.83.8 실시예 5(오크통/벌꿀)Example 5 (Oil Bucket / Honey) 4.34.3 3.83.8 3.93.9 4.24.2 실시예 6(오크통/설탕+구연산)Example 6 (Oat Bucket / Sugar + Citric Acid) 4.34.3 4.04.0 4.14.1 4.14.1 실시예 7(오크통/설탕+구연산+아미노산)Example 7 oak / sugar + citric acid + amino acid 4.24.2 4.04.0 4.14.1 4.14.1

표 2의 결과로부터 알 수 있듯이, 본 발명의 산삼배양근을 함유한 오크 숙성 리큐르는 첨가제 종류에 따른 관능적 차이는 크지 않았으나, 비교예에 비하여 맛, 풍미, 색깔 및 전체적인 기호도에서 우월한 점수를 보였으며, 오크통 숙성이 아닌 일반 발효통 숙성과 비교하여도 높은 관능 점수를 나타내어, 오크통 숙성에 따른 유의적 관능차이를 나태내는 것으로 나타났다. 특히 오크통 숙성에 의하여 산삼배양근 특유의 맛이 더욱 조화롭게 느껴지고 주정취와 불쾌한 맛을 효과적으로 제거한다는 묘사분석 결과가 많았다.As can be seen from the results of Table 2, oak aged liqueur containing the ginseng cultured root of the present invention did not have a large sensory difference according to the type of additives, but showed superior scores in taste, flavor, color and overall preference compared to the comparative example, Compared with the fermentation barrel aging, but not the oak barrel aging, it showed a high sensory score, indicating a significant sensory difference according to the oak barrel ripening. In particular, there were many descriptive analysis results that the characteristic taste of wild ginseng root was more harmonized by oak barrel aging and effectively removed the main odor and unpleasant taste.

이상에서 상세히 설명하고 입증하였듯이, 본 발명에 의한 산삼배양근을 함유한 오크 숙성 리큐르의 제조방법 및 이를 이용한 주류는 건강을 지향하는 기능성 식음료를 추구하는 소비자들의 욕구를 만족시킬 수 있는 새로운 형태의 기능성 리큐르 주류 제품으로서, 종래의 주류에 부가가치를 높인 신기능성 주류에 해당한다. 산삼배양근이 가지고 있는 약리성분 효과를 리큐르 형태에 최적으로 적용하기 위해, 산삼배양근 침출원액을 오크통 숙성과정을 통해 산삼배양근 특유의 향미를 부드럽게 조화시키고, 침출 후 분리 보관됐던 산삼배양근을 재투입하여 병입에 의해 애음자로부터 시각적 효과를 통해 신뢰성과 재활용의 기회를 부여할 수 있으며, 결과적으로 알코올 성분과 함께 산삼배양근 침출물로부터 흡수된 산삼배양근의 유용한 약리 성분으로 인하여 간 및 위에 부담을 덜 주고 음용할 때 느끼는 산삼배양 근의 특유의 향미로 인해 주정취와 숙취감을 극복할 수 있을 뿐 아니라, 산삼배양근 특유의 향으로 인해 부드러움을 함께 느낄 수 있는 새로운 형태의 기능성 리큐르 제품으로 차별화 될 수 있다. As described and demonstrated in detail above, the method for producing oak-aged liqueur containing wild ginseng cultured root according to the present invention and the liquor using the same are a new type of functional liqueur that can satisfy the needs of consumers pursuing health-oriented functional food and beverage. As a liquor product, it corresponds to the new functional liquor which added value added to the conventional liquor. In order to optimally apply the pharmacological effects of wild ginseng roots to liqueur form, the wild ginseng root leaching solution was blended with oak barrel aging process to smoothly blend the flavors of wild ginseng roots and re-injected the wild ginseng root which was separated and stored. It can provide the reliability and recycling opportunity through visual effects from the sounder, and consequently the alcohol and the beneficial pharmacological components of wild ginseng cultured roots absorbed from wild ginseng root leachate, together with the alcohol, will make the liver and stomach less burdened and drinkable. Due to the unique flavor of wild ginseng cultured roots, it can not only overcome the main mood and hangover, but also differentiate it into a new type of functional liqueur product that can feel softness due to the unique aroma of wild ginseng cultured.

Claims (3)

(a) 산삼배양근을 탈취 과정을 거친 42~48% 증류식 소주에 투입하여 1~3개월간 침출 및 1차숙성시키는 단계,(a) fermenting wild ginseng cultured roots into 42 ~ 48% distilled soju after deodorization and leaching and primary ripening for 1-3 months, (b) 추출된 산삼배양근을 분리하여 따로 저장하는 단계,(b) separating and storing the extracted wild ginseng cultured root, (c) 산삼배양근이 제거된 주정 침출액을 오크통에 저장하여 2차숙성하는 단계,(c) storing the alcoholic liquor from which the wild ginseng culture root has been removed in an oak barrel for secondary ripening; (d) 2차숙성된 산삼배양근 주정 침출액을 여과하고 20~40% 알코올 농도로 희석한 후 정밀 여과하는 단계, 및 (d) filtering the second aged wild ginseng root alcohol leachate, diluting to 20-40% alcohol concentration, and then fine filtration, and (e) 상기 (b)단계에서 분리하여 저장된 추출된 산삼배양근을 병입 과정에서 다시 투입하여 밀봉 포장하는 단계를 포함하는 산삼배양근을 함유한 오크통 숙성 리큐르의 제조방법. (e) a method for producing an aged oak barrel liqueur containing wild ginseng cultured root comprising the step of sealing and packing the extracted wild ginseng cultured root separated and stored in step (b) in the bottling process. 제1항에 있어서, The method of claim 1, 상기 (d)단계에서 희석된 산삼배양근 주정 침출액에 설탕, 올리고당, 벌꿀, 구연산 및 아미노산으로 이루어지는 그룹에서 선택되는 하나 이상을 추가로 배합하는 것을 특징으로 하는 산삼배양근을 함유한 오크통 숙성 리큐르의 제조방법.Method for producing an aged oak barrel liqueur containing wild ginseng cultured, characterized in that further blending at least one selected from the group consisting of sugar, oligosaccharides, honey, citric acid and amino acids in the wild ginseng root alcohol leachate diluted in step (d) . 제1항 또는 제2항의 제조방법에 따라 생산되는 것을 특징으로 하는 산삼 배양근을 함유한 오크통 숙성 리큐르를 이용하는 주류.Liquor using oak barrel aging liqueur containing wild ginseng cultured root, characterized in that produced according to the method of claim 1 or 2.
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KR100648000B1 (en) * 2006-08-28 2006-11-23 (주)충북소주 Manufacturing method of the liquors comprising cultured root of wild ginseng and alcoholic liquors using the same

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KR20190040567A (en) 2017-10-11 2019-04-19 제천한약영농조합법인 Manufacturing method of liquors
KR20190049967A (en) 2017-10-31 2019-05-10 롯데칠성음료주식회사 A distilled liquor with improved flavor by aging with oak and a method for preparing thereof
WO2019112112A1 (en) * 2017-12-08 2019-06-13 주식회사 움트리 Method for extracting wasabi extract

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