KR20050003731A - Toilet soap composition and manufacturing method thereof - Google Patents
Toilet soap composition and manufacturing method thereof Download PDFInfo
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- KR20050003731A KR20050003731A KR1020030045214A KR20030045214A KR20050003731A KR 20050003731 A KR20050003731 A KR 20050003731A KR 1020030045214 A KR1020030045214 A KR 1020030045214A KR 20030045214 A KR20030045214 A KR 20030045214A KR 20050003731 A KR20050003731 A KR 20050003731A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/08—Water-soluble compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/18—Shaping by extrusion or pressing
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/26—Drying
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
Abstract
Description
본 발명은 화장비누 조성물에 관한 것이며, 더욱 상세하게는 고농축 염화 염천수를 사용하여 피부질환 예방 및 치유효과와 체취방지 등의 효과가 있는 화장비누 조성물의 제조방법에 관한 것이다.The present invention relates to a cosmetic soap composition, and more particularly to a method for producing a cosmetic soap composition having the effect of preventing and healing skin diseases and body odor by using highly concentrated chloride salt water.
일반적으로 미용비누는 세정작용 뿐만 아니라 비누사용시 피부에 자극이 없어야 하며 피부의 탄력을 유지할 수 있어야 한다. 이를 위해 종래에 죽염, 알로에, 스쿠아렌, 한방재, 기타 순수 천연성분 등을 비누조성물에 혼합한 피부의 노화 방지 및 미백효과를 향상시키도록 하는 기능과 미용을 겸하도록 하는 화장품류 및 각종 미용비누가 널리 사용되고 있다.In general, cosmetic soaps should not only have a cleansing action but also have no skin irritation when using soap and should be able to maintain the elasticity of the skin. To this end, cosmetics and various beauty soaps that combine the function and beauty to improve the anti-aging and whitening effect of the skin, which is conventionally mixed with bamboo salt, aloe, squaraine, herbal medicine, and other pure natural ingredients in a soap composition. Is widely used.
이렇게 미백효과와 피부의 노화 방지 등의 피부 관리 기능을 하는 미용비누는, 화장품과 더불어 여성과 남성의 구분이 없이 사용되고 있으며, 특히 미용비누는 피부화장의 기준을 제시함에 따라 그 중요성이 크게 인식되고 있다.Beauty soaps that have a skin care function such as whitening effect and anti-aging of skin are used without cosmetics and men and women. Especially, beauty soaps are recognized as important because they suggest the standard of skin cosmetics. have.
특히 종래 구운 소금 및 죽염을 이용한 미용비누들이 널리 보급되어 있었음에도 고형 성분을 이용함으로 인하여 제조상의 불편과 한계를 가져왔으며, 특히 농도조절에 어려움을 겪었다.In particular, even though the soap has been widely spread using conventional baked salt and bamboo salt, the use of solid ingredients brought inconveniences and limitations in manufacturing, and in particular, had difficulty in controlling the concentration.
일반적으로 구운 소금, 소금, 죽염 등은 피부의 염증과 독기를 제거하고 오래된 노폐물을 체외로 방출시켜 인체의 자연생리기능을 강화시키며, 화상과 외상을 치료하는 효과와 피부에 대한 수분과 지방의 균형을 유지하는 효과가 있다고 알려져 있다. 그러나 상기 소금, 죽염 등을 함유한 비누의 제조방법에 있어서 고형 원료를 액상화하여 사용해야 하므로 증류수나 정수물을 끓여 용해시킨 용수를 비누화화도록 혼합하여 제조함으로써 낮은 농도로 조절되기 쉬우며, 이때는 기능성을 기대하기 힘들었다. 또한 동 원료의 농도를 높여 기능성을 갖도록 할 경우에는 비누화 반응이 잘 일어나지 않거나 비누가 굳고 갈라지며 거품이 잘 일어나지 않는 문제점이 있었다.In general, grilled salt, salt, and bamboo salt remove inflammation and poisoning of the skin, release old wastes to the body, strengthen the body's natural physiological function, treat burns and trauma, and balance water and fat on the skin. It is known to have the effect of maintaining. However, in the manufacturing method of the soap containing salt, bamboo salt, etc., since the solid raw material should be used by liquefying, it is easy to control to low concentration by mixing and preparing distilled or purified water to be saponified, and at this time, It was hard to expect. In addition, when the concentration of the raw material to increase the functionality to have a problem that the saponification reaction does not occur well or the soap is hard and cracking and foaming does not occur.
본 발명은 상기의 문제점을 해결하기 위하여 안출된 것으로서, 고농축 염화염천수 성분이 최적의 비율과 함유된 화장비누 조성물과 그 제조방법에 관한 발명이다.The present invention has been made to solve the above problems, the present invention relates to a cosmetic soap composition containing a highly concentrated chloride salt water component in an optimal ratio and a method for producing the same.
담수와 해수의 성질을 모두 가지고 있는 고농축 염화염천수를 이용하여 염화염천수에 함유되어 있는 각종 성분들이 가져오는 피부해독 및 피부보호효과를 얻는 화장비누 조성물을 제공하는 것을 목적으로 하며, 나아가 고농축 염화염천수를 이용한 편리하고 안정적인 농도조절방법을 통하여 효율적인 화장비누 제조방법을 제공하고자 한다.It is an object of the present invention to provide a cosmetic soap composition which obtains skin detoxification and skin protection effect of various components contained in the chloride salt water by using highly concentrated chloride salt water having both fresh water and sea water. To provide an efficient cosmetic soap manufacturing method through a convenient and stable concentration control method using brine.
도 1은 본 발명에 따른 화장 비누 조성물의 제조방법을 나타내는 공정도이다.1 is a process chart showing a manufacturing method of a cosmetic soap composition according to the present invention.
본 발명은 염화 염천수를 수분증발을 차단한 상태로 가열하여 부유물을 필터로 걸러 만들어진 고농축 염화 염천수를 함유하는 화장비누 조성물 및 그 제조방법에 관한 발명이다.The present invention relates to a cosmetic soap composition containing a highly concentrated chlorine salt water produced by filtering the suspended solids water in a state of blocking the evaporation of water to filter the suspended matter and a method for producing the same.
이하 본 발명을 더욱 더 상세하게 설명하면 다음과 같다.Hereinafter, the present invention will be described in more detail as follows.
본 발명에서 사용하는 염화염천수는 해안지역 지하 870m 아래 심층수에서 채취한 것으로서 담수와 해수에 함유되는 다양한 종류의 성분을 함유하고 있다. 본 발명에 사용된 염화염천수의 성분을 한국지질자원연구원에 의뢰하여 분석한 분석시험성적서는 아래와 같다.Chloride spring water used in the present invention is taken from deep water below 870m underground and contains various kinds of components contained in fresh water and seawater. The analysis test report analyzing the components of chloride spring water used in the present invention by the Korea Institute of Geoscience and Mineral Resources is as follows.
상기 표에서 보는 바와 같이 염화염천수는 칼슘, 칼륨, 나트륨, 마그네슘, SiO2, 염소, SO4, 플루오르, 리튬, 스트론튬, 철, 망간, 구리, 납, 수은 등을 함유하고 있으며, 염수와 담수의 중간적인 성질을 갖는다. 채취된 염화 염천수를 100℃에서 약 8시간 끓이되 수분증발을 시키지 않고 철분 등의 가라앉는 부유물을 필터로 걸러서 약 3 내지 4배 농축된 고농축 정제물을 사용한다. 이때 고농축 염화 염천수를 만드는 방법은 일반적으로 수분을 증발시켜 얻는 통상의 증발 농축방법과는 차이가 있다. 이는 염화염천수의 피부에 유용한 성분을 최대한 보유하도록 하면서 정제 농축하기 위함이다.As shown in the table above, the chloride spring contains calcium, potassium, sodium, magnesium, SiO 2 , chlorine, SO 4 , fluorine, lithium, strontium, iron, manganese, copper, lead, mercury, etc. Has intermediate properties. Boil the collected chloride salt water at 100 ° C. for about 8 hours, but use a highly concentrated purified product concentrated by about 3 to 4 times by filtering out the submerged suspended matter such as iron without filtering water. At this time, the method of making highly concentrated chlorine salt water is generally different from the conventional evaporation and concentration method obtained by evaporating water. This is to concentrate the tablet while retaining the most useful ingredients for the skin of chloride salt water.
본 발명에 사용되는 기능성 원료는 고농축 염화염천수, 미네랄 오일, 미네랄 워터이다. 기능성 원료는 고농축 염화염천수는 비누 조성물의 2 내지 4중량부, 미네랄 오일은 비누 조성물의 2 내지 4중량부, 미네랄 워터는 1 내지 2 중량부로 구성하는 것이 바람직하다.Functional raw materials used in the present invention are highly concentrated chloride spring water, mineral oil, mineral water. The functional raw material is preferably composed of 2 to 4 parts by weight of the highly concentrated chloride salt water of the soap composition, 2 to 4 parts by weight of the mineral oil, and 1 to 2 parts by weight of the mineral water.
고농축 염화염천수의 함량이 4 중량비 보다 많으면 비누가 굳고 갈라지며 거품이 잘 일어나지 않으며 피부에 대한 자극성이 유발되어 보습작용이 저하되고 피부를 다소 거칠게 할 우려가 있으며, 염화염천수의 함량이 2 중량비 보다 적으면 염화염천수의 효능인 피부보호효과를 기대할 수 없다.If the content of highly concentrated chloride spring water is more than 4 weight ratio, the soap hardens, cracks, does not foam well, causes irritation to the skin, which lowers the moisturizing effect and makes the skin somewhat rough, and the content of chloride salt water is 2 weight ratio. If it is less, the skin protection effect of chlorinated spring water cannot be expected.
미네랄 워터는 고농축 염화염천수의 농도를 조절하는 역할을 하는데, 미네랄 워터의 함량이 2 중량비보다 많으면 수분이 많아서 비누가 응고되기 힘들며, 미네랄 워터의 함량이 1 중량비보다 적으면 비누가 굳고 갈라지는 현상이 일어난다.Mineral water plays a role to control the concentration of high concentration chloride chloride water.If the content of mineral water is more than 2 weight ratio, soap is hard to coagulate due to the moisture content. If the content of mineral water is less than 1 weight ratio, the soap hardens and cracks. Happens.
미네랄 오일은 호바오일, 팜오일, 동백오일 등의 식물성 오일을 사용하고, 미네랄 오일의 함량이 4 중량비보다 많으면 염화염천수의 효과의 작용을 방해하며, 미네랄 오일의 함량이 2 중량비보다 적으면 삼투압현상에 의하여 소금기가 비누에 침투되어 비누화가 잘 일어나지 않는다.Mineral oil uses vegetable oils such as joba oil, palm oil, and camellia oil.If the content of mineral oil is more than 4 weight ratio, the effect of chloride salt water is impeded. If the content of mineral oil is less than 2 weight ratio, osmotic pressure Due to the phenomenon, salt is penetrated into soap and saponification does not occur easily.
기능성 원료의 함량은 비누중량에 대하여 농축 염화 염천수는 3중량부, 미네랄 오일은 3중량부, 미네랄 워터는 1. 5중량부인 것이 더욱 바람직하다.The content of the functional raw material is more preferably 3 parts by weight of concentrated chlorinated brine, 3 parts by weight of mineral oil, and 1.5 parts by weight of mineral water, based on the weight of soap.
상기 기능성 원료는 각각의 함량비에 따라 취하여 60 내지 65℃에서 9 내지 11시간 배합하여 자연숙성시킨다.The functional raw material is taken in accordance with the content ratio of each and blended for 9 to 11 hours at 60 to 65 ℃ natural maturation.
본 발명에 사용된 비누 베이스는 우지 또는 팜유를 80중량부, 야자유 또는 팜커널유를 20중량부 혼합하여 공지의 방법으로 가성소다와 반응시켜 생성한다.The soap base used in the present invention is produced by mixing 80 parts by weight of tallow or palm oil, 20 parts by weight of palm oil or palm kernel oil and reacting with caustic soda by a known method.
상기 비누 베이스와 상기 기능성 원료를 혼합하는 방법은 다음과 같다.The method of mixing the soap base and the functional raw material is as follows.
상기 비누 베이스 70 내지 95중량부에 자연숙성된 기능성 원료 5 내지 30중량부를, 더욱 바람직하게는 비누 베이스 90 내지 95중량부에 자연숙성된 기능성 원료 5 내지 10중량부를 가미하여 교반기에서 혼합하여 60 내지 65℃에서 30분 내지 1시간 1차 숙성하고 이를 1차 압출한다. 상기 1차 압출된 것을 기능성 원료가 비누베이스에 혼합숙성되도록 60~65℃에서 30분 내지 1시간 2차 숙성하고 2차 압축한다. 같은 조건에서 숙성과 압축을 반복할 수 있다. 상기 압축된 것을 진공상태에서 수분을 증발건조시킨다. 진공건조에 따라 수분을 12 내지 15% 함유하는 비누반제품 상태가 된다. 진공건조된 것을 다시 50 내지 60℃에서 압축한다.5 to 30 parts by weight of the naturally-active functional raw material 5 to 30 parts by weight of the soap base 70 to 95 parts by weight, more preferably 5 to 10 parts by weight of the natural raw material to the 90-95 parts by weight of the soap base mixed 60 to First aged at 65 ° C. for 30 minutes to 1 hour and first extruded it. The first extruded and secondly aged for 30 minutes to 1 hour at 60 ~ 65 ℃ so that the functional raw material is mixed mature in the soap base and second compression. Aging and compression can be repeated under the same conditions. The compressed product is evaporated to dryness in a vacuum. According to the vacuum drying, the soap becomes a semi-finished product containing 12 to 15% of moisture. Vacuum dried is again compressed at 50-60 ° C.
본 발명은 기능성 원료와 비누베이스의 혼합, 압출과정에서 혼합을 용이하게 하기 위한 어떠한 화학적 촉매를 사용하지 않고, 자연숙성과정과 반복적인 숙성, 압축과정만을 거침으로써 피부에 미치는 자극을 최소화하여 화장비누로서의 피부보호효과를 높이고, 피부트러블을 방지하며, 기능성 원료의 효과를 자연스럽게 구현할 수 있으며, 공정의 단순화를 꾀할 수 있다.The present invention does not use any chemical catalyst for facilitating the mixing and extrusion of the functional raw material and soap base, and only minimizes the irritation to the skin by going through the natural ripening process, repeated aging, compression process It can enhance the skin protection effect, prevent skin troubles, can naturally realize the effect of the functional raw material, and can simplify the process.
압출된 비누 조성물에 기능성 향을 배합하여 공지의 성형기를 사용하여 봉상의 비누바를 압출하여 제조하고 적당크기와 모양으로 절단한 후 자동성형한다.Functional fragrance is blended into the extruded soap composition to produce a bar-shaped soap bar using a known molding machine, and is cut into a suitable size and shape and then automatically molded.
이하 실시예를 들어 본 발명을 더욱 상세히 설명한다.The present invention will be described in more detail with reference to the following Examples.
[실시예 1]Example 1
우지 또는 팜유를 80중량부, 야자유 또는 팜커널유를 20중량부 혼합하여 공지의 방법에 의해 가성소다와 반응시켜 비누베이스를 생성하는 한편, 염화 염천수(고농축 정제) 3중량부, 미네랄 오일 3중량부, 미네랄 워터 1.5중량부로 이루어진 기능성 원료를 60~65℃에서 약 10시간 배합한 후 자연숙성시킨다. 상기 비누베이스 92.5중량부에 상기 자연숙성된 기능성 원료 7.5중량부를 가미하여 교반기에서 혼합하여 약 30분 내지 1시간 숙성시킨다(1차 숙성). 상기 1차 교반된 비누반제품을 압출한다(1차 압출). 상기 1차 압출된 것을 기능성원료가 비누베이스에 혼합숙성되도록 60~65℃에서 30분 내지 1시간 2차 숙성후 2차 압출하며, 다시 60~65℃에서 30분 내지 1시간 3차 숙성후 3차 압출한다. 상기 압출된 것을 진공상태에서 수분을 증발 건조시켜 수분을 12 내지 15% 함유하는 비누반제품 상태로 만든다. 진공건조된 것을 다시 50 내지 60℃에서 4차 압출한다.80 parts by weight of Uji or palm oil, 20 parts by weight of palm oil or palm kernel oil are mixed and reacted with caustic soda by a known method to produce a soap base, while 3 parts by weight of chlorinated brine (highly concentrated purified), mineral oil 3 A functional ingredient consisting of parts by weight and 1.5 parts by weight of mineral water is blended at 60 to 65 ° C. for about 10 hours and then aged naturally. 92.5 parts by weight of the soap base is added to 7.5 parts by weight of the naturally matured functional raw material, mixed in a stirrer and aged for about 30 minutes to 1 hour (primary aging). The first stirred soap semi-finished product is extruded (first extrusion). After the first extruded the second time ripening at 60 ~ 65 ℃ 30 minutes to 1 hour so that the functional raw material mixed in the soap base mixed with the first extruded, and again after 30 minutes to 1 hour 3 aged at 60 ~ 65 ℃ 3 Secondary extrusion. The extruded product is evaporated to dryness in a vacuum to make a soapy semi-finished product containing 12 to 15% of moisture. The vacuum dried thing is further extruded at 50 to 60 ° C.
4차 압출된 비누 조성물에 기능성 향을 배합하여 공지의 성형기를 사용하여봉상의 비누바를 압출하여 제조하고 적당크기와 모양으로 절단한 후 자동성형하였다.Functional fragrance was blended into the 4th extruded soap composition, and the bar-shaped soap bar was extruded using a known molding machine, cut into a suitable size and shape, and automatically molded.
이때의 염화 염천수는 해안지역의 지하 870m에서 뽑아낸 심층수 20ℓ를 100℃에서 약 8시간 끓이되 수분증발을 시키지 않고 철분 등의 가라앉는 부유물을 필터로 걸러서 약 3 내지 4배 농축된 고농축 정제물을 사용한다. 이때 고농축 염화 염천수를 만드는 방법은 일반적으로 수분을 증발시켜 얻는 통상의 증발 농축방법과는 차이가 있다. 이 염화 염천수는 칼슘, 칼륨, 나트륨, 마그네슘, SiO2, 염소, SO4, 플루오르, 리튬, 스트론튬, 철, 망간, 구리, 납, 수은 등을 함유하고 있으며, 염수와 담수의 중간적인 성질을 갖는다.At this time, chlorine salt water boils 20 liters of deep water extracted from 870m underground in the coastal region for about 8 hours at 100 ℃, but filters out sinking suspended solids such as iron without water evaporation. Use water. At this time, the method of making highly concentrated chlorine salt water is generally different from the conventional evaporation and concentration method obtained by evaporating water. This chloride chloride contains calcium, potassium, sodium, magnesium, SiO 2 , chlorine, SO 4 , fluorine, lithium, strontium, iron, manganese, copper, lead and mercury. Have
본 발명에 따른 고농축 염화 염천수 성분이 최적의 비율로 함유된 화장비누 조성물은 피부에 대한 보습 및 세정효과와 더불어 영양효과가 뛰어나고, 피부에 좋지 못한 이물질을 흡수, 방출시켜 부드럽고 탄력있는 피부를 유지시켜 준다. 또한 본 발명에 따른 화장비누 조성물은 피부에 유해한 독성물질과 노폐물을 체외로 방출시켜 인체의 자연생리기능을 강화시키며, 피부병과 가려움증 및 여드름, 잔주름, 반점에 대한 치료효과가 우수하다.The cosmetic soap composition containing the highly concentrated chlorinated spring water component according to the present invention has an excellent nutritional effect as well as a moisturizing and cleaning effect on the skin, and absorbs and releases foreign substances that are not good for the skin to maintain a soft and elastic skin. Let it be. In addition, the cosmetic soap composition according to the present invention releases toxic substances and wastes harmful to the skin to enhance the natural physiological function of the human body, and has an excellent therapeutic effect against skin diseases and itching and acne, fine wrinkles, spots.
또한 고농축 염화 염천수를 이용하여 효율적인 기능성 원료의 농도 조절을 가능케하였으며, 비누 베이스와 기능성 원료의 자연 숙성 혼합방법을 통하여 피부의 자극을 줄이고 기능성 원료의 자연스런 효과의 발현이 가능하다.In addition, it is possible to efficiently control the concentration of functional raw materials by using highly concentrated chlorinated spring water, and it is possible to reduce the irritation of the skin and to express the natural effect of the functional raw materials through the natural aging mixing method of the soap base and the functional raw materials.
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