KR20040052059A - Hair oil composition comprising camellia oil and method for preparation thereof - Google Patents
Hair oil composition comprising camellia oil and method for preparation thereof Download PDFInfo
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- KR20040052059A KR20040052059A KR1020020079783A KR20020079783A KR20040052059A KR 20040052059 A KR20040052059 A KR 20040052059A KR 1020020079783 A KR1020020079783 A KR 1020020079783A KR 20020079783 A KR20020079783 A KR 20020079783A KR 20040052059 A KR20040052059 A KR 20040052059A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
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Abstract
Description
본 발명은 두발을 위한 새로운 조성의 헤어오일 조성물 및 그 제조방법에 관한 것으로, 보다 상세하게는 모발의 큐티클 층에 도포 시 모발에 윤기와 엷은 막을 형성시켜주는 동백오일이 함유된 헤어오일 조성물 및 그 제조방법에 관한 것이다.The present invention relates to a hair oil composition having a new composition for hair and a method for manufacturing the same, and more particularly, to a hair oil composition containing camellia oil which forms a thin film and a luster on the hair when applied to the cuticle layer of the hair and It relates to a manufacturing method.
헤어 오일은 모발에 윤기를 제공하고 모발을 정돈하기 위하여 처방되어 왔으며, 종래에는 식물성 오일이나 탄화수소 오일을 주성분으로 하였으나, 현재에 이르러서는 사용감과 윤기가 우수한 실리콘을 주성분으로 하고 있다.Hair oils have been prescribed to provide shine to hair and to prepare hair. Conventionally, hair oil has been based on vegetable oils or hydrocarbon oils. However, up to now, silicone oils have excellent usability and luster.
식물성 오일이나 탄화수소 오일을 주성분으로 하는 헤어오일은 헤어스타일을 위한 모발 정돈력은 우수하지만 끈적임이 너무 많고 무거운 느낌을 주며 쉽게 먼지와 같은 이물질이 모발에 부착되어 지저분한 헤어스타일이 되는 단점이 있고, 실리콘 오일을 주성분으로 하는 헤어오일의 경우는 사용감이 매끄럽고 가벼우며 지모보수효과가 있지만 불규칙한 막의 형성과 쉽게 휘발되는 성질 때문에 빠른 시간에 그 효과가 소멸하는 문제점을 가지고 있었다.Hair oils based on vegetable oils or hydrocarbon oils have excellent hair trimming power for hairstyles, but they are too sticky and heavy. They also have the disadvantages of being attached to foreign hair such as dust, which leads to a messy hairstyle. In the case of the oil containing the oil as a main component, the feeling of use is smooth, light, and has a hair-removal effect, but the effect disappears quickly because of the irregular membrane formation and the easily volatilized property.
따라서, 두 가지 헤어오일의 단점을 보완하기 위해 혼용된 처방, 즉 실리콘오일에 식물성오일과 탄화수소오일을 혼합하는 헤어오일이 개발되기는 하였으나, 고온 보관시 유화상태가 깨지는 등 상 안정성이 좋지 않으며, 지모보수효과가 감소되는 단점을 갖고 있었다.Therefore, although mixed hair formulas have been developed to supplement the shortcomings of the two hair oils, that is, vegetable oils and hydrocarbon oils are mixed with silicone oils, they do not have good phase stability such as breakage of emulsified state at high temperature. It had the disadvantage of reducing the repair effect.
따라서, 본 발명은 이러한 종래의 문제점을 개선하고자 발명된 것으로서, 종래의 헤어오일 조성물에 동백오일을 첨가함으로서, 두발 윤기를 장기간 유지시키면서도 상안전성이 뛰어난 신규한 헤어오일 조성물을 제공하고자 하는 것이다.Accordingly, the present invention has been invented to improve such a conventional problem, by adding camellia oil to a conventional hair oil composition, to provide a novel hair oil composition excellent in phase safety while maintaining hair gloss for a long time.
본 발명의 또 다른 목적은 상기한 헤어오일 조성물의 제조방법을 제공하고자 하는 것이다.Still another object of the present invention is to provide a method for preparing the hair oil composition.
상기한 발명의 목적을 달성하기위하여, 본 발명의 헤어오일 조성물은 모발에 광택 및 큐티클 표면에 막형성 효과를 제공하는 85-90 : 15-10 중량비의 사이클로메치콘 및 디메치코놀 실리콘 혼합물을 포함하는 종래의 헤어오일 조성물에 있어서, 동백오일, 미네랄오일 및 디메치코놀과 식물성 오일의 상안전성을 위하여 스쿠알란을 상기한 혼합물 중량과 대비 시 20~80 : 0.5~20 : 0.5~40 : 0.1~6.0 : 0.5~20.0로 포함하되 미네랄오일을 상기한 사이클로메치콘과 디메치코놀의 혼합물 중량의 1/2 이하로 포함하여, 모발의 윤기를 장시간 지속시키고 모발을 정돈시키는 효과를 제공하고 제품의 상 안정성을 증가시킨 효과를 갖는다.In order to achieve the object of the present invention, the hair oil composition of the present invention comprises a 85-90: 15-10 weight ratio of cyclomethicone and dimethiconol silicone mixtures to provide a film-forming effect on the hair and gloss and cuticle surface In the conventional hair oil composition, in the phase safety of camellia oil, mineral oil and dimethiconol and vegetable oil 20 to 80: 0.5 to 20: 0.5 to 40: 0.1 to 6.0 : Contains from 0.5 to 20.0, but contains mineral oil less than 1/2 of the weight of the mixture of cyclomethicone and dimethiconol as described above, to provide long lasting shine and to prepare hair Has the effect of increasing the phase stability of the product.
또한, 본 발명의 조성물은 중량비로 20~80 : 20~50 : 1~10: 0.5~20 : 0.5~40 : 0.1~6.0 : 0.5~20.0 의 사이클로메치콘과 디메치코놀의 혼합물, 사이클로메치콘, 페닐트리메치콘, 동백오일, 미네랄오일, 스쿠알란, 및 식물성 액상 오일 및 합성에스테르 오일에서 선택된 하나 또는 그 이상의 오일을 포함할 수 있고, 이때 미네랄오일은 사이클로메치콘과 디메치코놀의 혼합물의 중량의 1/2 이하의 범위로 포함된다. 또한, 소량의 향료와 유용성색소, 자외선 차단제, 방부제 등을 추가로 포함할 수 있다.In addition, the composition of the present invention is a mixture of cyclomethicone and dimethiconol having a weight ratio of 20 to 80:20 to 50: 1 to 10: 0.5 to 20: 0.5 to 40: 0.1 to 6.0: 0.5 to 20.0. , Cyclomethicone, phenyltrimethicone, camellia oil, mineral oil, squalane, and one or more oils selected from vegetable liquid oils and synthetic ester oils, wherein the mineral oils are cyclomethicone and dimethiconol. It is included in the range of less than 1/2 of the weight of the mixture. In addition, it may further comprise a small amount of fragrance and oil-soluble pigments, sunscreen, preservatives and the like.
동백 오일은 두발화장료 조성물이 등장하기 이전부터 꾸준히 동양인들에게 애용되어 오던 것으로서, 산화안정성이 높고, 모발에 탄력성을 부여하는 성능이 탁월하다고 할 것이나, 끈적임이 심하여, 근래에 들어서는 이를 사용하지 않고 있었다.Camellia oil has been used habitually by Asians before the hair cosmetic composition appeared, and it is said to have high oxidation stability and excellent performance to give elasticity to hair, but it is sticky and has not been used in recent years. .
본 발명은 이러한 불건조 성향 및 유연효과가 뛰어난 동백오일을 기존의 실리콘 을 주성분으로 하는 헤어오일에 첨가하여 윤기의 지속효과를 장기간 유지시키고, 정돈효과를 제공하도록 하였으며, 디메치코놀과 식물성오일의 상용성을 위하여 스쿠알란을 첨가시킨 헤어오일 조성물이다.The present invention is to add a camellia oil having excellent drying properties and softening effect to the conventional hair oil containing silicone as a main component to maintain the long-lasting effect of shine, to provide a tidying effect, the dimethiconol and vegetable oil It is a hair oil composition to which squalane is added for compatibility.
본 발명의 헤어 오일 조성물의 제조방법은 하기의 단계를 포함한다.The method for producing a hair oil composition of the present invention includes the following steps.
20~80 : 10~50 : 1~10: 0.5~20 : 0.5~40 : 0.1~6.0의 중량비로 85~90 : 15~10 중량비로 혼합된 사이클로메치콘과 디메치코놀의 혼합물, 사이클로메치콘, 페닐트리메치콘, 동백오일, 미네랄오일, 및 스쿠알란을 준비하되 미네랄오일의 양을 사이클로메치콘 및 디메치코놀 혼합물의 중량대비 1/2 이하로 준비하는 단계;20 to 80: 10 to 50: 1 to 10: 0.5 to 20: 0.5 to 40: 0.1 to 6.0 in weight ratio of 85 to 90: 15 to 10 weight ratio of mixed cyclomethicones and dimethiconol, cyclomethicones Preparing phenyltrimethicone, camellia oil, mineral oil, and squalane, but preparing the amount of mineral oil in an amount less than 1/2 of the weight of the cyclomethicone and dimethiconol mixtures;
상기한 사이클로메치콘과 디메치코놀의 혼합물, 사이클로메치콘, 및 페닐트리메치콘을 혼합하고 교반하여 제 1 혼합물을 제조하는 단계;Preparing a first mixture by mixing and stirring the mixture of cyclomethicone and dimethiconol, cyclomethicone, and phenyltrimethicone;
상기한 동백오일, 미네랄오일, 및 스쿠알란을 혼합하고 교반하여 제 2혼합물을 제조하는 단계; 및Preparing a second mixture by mixing and stirring the camellia oil, the mineral oil, and squalane; And
상기한 제 1혼합물 및 제 2혼합물을 충분히 교반하여 혼합하는 단계.Mixing the first mixture and the second mixture by stirring sufficiently.
제품의 안정성이나 사용감의 조절을 위해 식물성 액상 오일 및 합성에스테르 오일에서 선택된 하나 또는 그 이상의 오일을 사이클로메치콘과 디메치코놀의 혼합물과 중량과 대비시 20-80 : 0.5~20.0으로 혼합하고 소량의 향료와 유용성색소, 자외선차단제, 방부제 등의 기타첨가물을 첨가하는 단계를 추가할 수 있다.One or more oils selected from vegetable liquid oils and synthetic ester oils are mixed with a mixture of cyclomethicone and dimethiconol to 20-80: 0.5 to 20.0 by weight and a small amount to control the stability or usability of the product. Adding fragrances and other additives such as oil soluble pigments, sunscreens, preservatives, etc. may be added.
또한, 제 1혼합물 및 제 2 혼합물은 각각 1500rpm의 속도로 30분간 교반하는 것이 가장 바람직하고, 제 1혼합물 및 제2 혼합물의 교반 시는 제 1혼합물을 1000rpm의 속도로 교반하면서 제 2혼합물을 가하여 2500rpm의 속도로 1시간 정도 교반하는 것이 가장 바람직한 물성을 갖는 조성물을 수득할 수 있다.In addition, it is most preferable that the first mixture and the second mixture are stirred for 30 minutes at a speed of 1500 rpm, respectively, and when the first mixture and the second mixture are stirred, the second mixture is added while stirring the first mixture at a speed of 1000 rpm. Stirring at a rate of 2500 rpm for about 1 hour can give a composition having the most desirable physical properties.
이하, 실시예를 통하여, 본 발명을 상세히 설명할 것이다. 본 발명이 하기 실시예에 의하여 제한되지 않는 다는 것은 당업자에게 자명할 것이다.Hereinafter, the present invention will be described in detail through examples. It will be apparent to those skilled in the art that the present invention is not limited by the following examples.
[실시예 1]Example 1
50.0g의 사이클로메치콘과 디메치코놀의 혼합물인 DC-1401 (사이클로메치콘은 사이클로헥사실록산이고, 디메치코놀은 하이드록시기를 말단으로 하는 디메틸실록산으로 Dow Corning사에서 구입), 25.0g의 사이클로메치콘 DC-345 (사이클릭 디메칠 폴리실록산의 화합물로서 Dow Corning사에서 구입) 및 5.0g의 페닐트리메치콘 DC-556 (실록산 중합체 화합물로써 Dow Corning사에서 구입)을 혼합하여 1500rpm의 속도로 30분간 교반하여 제1혼합물을 제조하였다.DC-1401, a mixture of 50.0 g of cyclomethicone and dimethiconol (cyclomethicone is cyclohexasiloxane, dimethiconol is a dimethylsiloxane having a hydroxyl group at the end), purchased from Dow Corning, 25.0 g of cyclo Methicone DC-345 (a compound of cyclic dimethyl polysiloxane, purchased from Dow Corning) and 5.0 g of phenyltrimethicone DC-556 (available from Dow Corning as a siloxane polymer compound) were mixed at 30 rpm at a speed of 1500 rpm. Stirring for a minute gave a first mixture.
4.0g의 동백오일, 5.0g의 이소프로필미리스테이트, 10.3g의 미네랄오일, 0.5g의 스쿠알란, 및 0.2g의 향료를 혼합하여 1500rpm의 속도로 30분간 교반하여 제2혼합물을 제조하였다.4.0 g of camellia oil, 5.0 g of isopropyl myristate, 10.3 g of mineral oil, 0.5 g of squalane, and 0.2 g of fragrance were mixed and stirred for 30 minutes at a speed of 1500 rpm to prepare a second mixture.
제조된 혼합물중 제1혼합물 80g을 1000rpm의 속도로 교반하면서 제2혼합물 20g을 가한 후, 2500rpm의 속도로 1시간 교반하여 본 발명의 조성물 100g을 제조하였다.20 g of the second mixture was added while stirring the first mixture 80 g at a speed of 1000 rpm, and then stirred at a speed of 2500 rpm for 1 hour to prepare 100 g of the composition of the present invention.
[비교예 1]Comparative Example 1
60.0g의 DC-1401, 34.8g의 DC-345, 5.0g의 DC-556, 0.2g의 향료를 2500rpm의 속도로 1시간 교반하여 조성물 100g을 제조하였다.100 g of the composition was prepared by stirring 60.0 g of DC-1401, 34.8 g of DC-345, 5.0 g of DC-556, and 0.2 g of fragrance at a speed of 2500 rpm for 1 hour.
[비교 예 2][Comparative Example 2]
30.0g의 동백오일, 29.8g의 이소프로필미리스테이트, 40.0g의 미네랄오일, 0.2g의 향료를 2500rpm의 속도로 1시간 교반하여 조성물 100g을 제조하였다.100 g of the composition was prepared by stirring 30.0 g of camellia oil, 29.8 g of isopropyl myristate, 40.0 g of mineral oil, and 0.2 g of fragrance at a speed of 2500 rpm for 1 hour.
[비교 예 3][Comparative Example 3]
20.0g의 DC-1401, 30.0g의 DC-345, 5.0g의 DC-556을 1500rpm의 속도로 30분간 교반하여제 1 혼합물을 제조하고, 따로 10.0g의 동백오일, 34.8g의 미네랄오일, 0.2g의 향료를 1500rpm의 속도로 30분간 교반하여 제 2혼합물을 제조한 후 한 후, 제1혼합물 55g을 1000rpm의 속도로 교반하면서 제2혼합물 45g을 가하고 2500rpm의 속도로 1시간 교반하여 조성물100g을 제조하였다.20.0 g of DC-1401, 30.0 g of DC-345 and 5.0 g of DC-556 were stirred at a speed of 1500 rpm for 30 minutes to prepare a first mixture, separately 10.0 g of camellia oil, 34.8 g of mineral oil, 0.2 After stirring the fragrance of g for 30 minutes at a speed of 1500rpm to prepare a second mixture, 45g of the second mixture was added while stirring the 55g of the first mixture at a speed of 1000rpm and stirred for 1 hour at a speed of 2500rpm to give 100g of the composition. Prepared.
[실험 예 1]Experimental Example 1
상기의 실시 예 1 및 비교 예 1, 2, 3의 결과 제조된 조성물의 성상(외부상태), 상안전성, 모발상태를 관찰하기위하여 모발가닥에 일정량을 도포하여 관능적으로 시험하였고, 그 결과는 표 1과 같다.In order to observe the properties (external state), phase safety, and hair condition of the prepared composition as a result of Example 1 and Comparative Examples 1, 2, and 3, a sensory test was carried out by applying a certain amount to the hair strands, and the results are shown in Table Same as 1.
표 1Table 1
* 상기한 표에서 모발상태의 관능평가 중 끈적임은 수치가 클수록 끈적이는 것이며, 윤기지속성은 수치가 클수록 오래 지속되는 것이고, 감촉은 수치가 클수록 부드럽고 매끄러운 것이며, 젖은 상태에서 빗질은 수치가 클수록 빗질이 잘 되는 것이다.* In the above table, stickiness of the sensory evaluation of hair condition is sticky as the value is larger, gloss persistence lasts longer as the value is higher, texture is softer and smoother as the value is higher, and combing is better when combing in the wet state. Will be.
이상에서 살펴본 바와 같이, 본 발명의 헤어오일 조성물은 실리콘을 주성분으로 하는 종래의 헤어오일에 불건조성향이 있고 유연효과가 뛰어난 동백오일 등을 첨가한 새로운 조성물로서, 실리콘 검 혼합물의 우수한 사용감 뿐만 아니라, 큐티클 보수기능, 윤기지속효과 및 모발정돈력이 향상된 효과를 갖는다. 또한, 스쿠알란을 포함함으로서 상온에서 분리.석출 되지 않고 우수한 상안정성을 갖는다.As described above, the hair oil composition of the present invention is a new composition in which a conventional hair oil containing silicone as a main ingredient is added with camellia oil having an undrying tendency and excellent softening effect. , Cuticle repair function, gloss lasting effect and hair trimming power are improved. Also, by including squalane, it is not separated and precipitated at room temperature and has excellent phase stability.
Claims (5)
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KR101219645B1 (en) * | 2006-09-26 | 2013-01-08 | 주식회사 엘지생활건강 | Non-aqueous wax-type hair cosmetic composition |
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KR100290591B1 (en) * | 1993-12-22 | 2001-09-17 | 손 경 식 | Hair cosmetic composition |
GB9404550D0 (en) * | 1994-03-09 | 1994-04-20 | Unilever Plc | Hair conditioning composition |
EP1531491A2 (en) * | 1996-04-18 | 2005-05-18 | Matsushita Electric Industrial Co., Ltd. | SiC device and method for manufacturing the same |
KR19980015484A (en) * | 1996-08-22 | 1998-05-25 | 한옥수 | How to make rinse with camellia oil |
KR19980015483A (en) * | 1996-08-22 | 1998-05-25 | 한옥수 | How to make shampoos based on camellia oil |
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KR101219645B1 (en) * | 2006-09-26 | 2013-01-08 | 주식회사 엘지생활건강 | Non-aqueous wax-type hair cosmetic composition |
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