KR20040026213A - Transparent soap composition - Google Patents

Transparent soap composition Download PDF

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KR20040026213A
KR20040026213A KR1020020057589A KR20020057589A KR20040026213A KR 20040026213 A KR20040026213 A KR 20040026213A KR 1020020057589 A KR1020020057589 A KR 1020020057589A KR 20020057589 A KR20020057589 A KR 20020057589A KR 20040026213 A KR20040026213 A KR 20040026213A
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weight
parts
transparent soap
soap composition
soap
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KR1020020057589A
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Korean (ko)
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김기영
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김기영
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

PURPOSE: Provided is a transparent soap composition excellent in decomposition of secretion like sebum and hydration, which has an effect on curing inflammation, pimples, and skin disease and can be used for oily, dry, and allergic skin. CONSTITUTION: The transparent soap composition contains: 100pts.wt. of a mixture containing 15-20wt% of coco fatty acid, 20-30wt% of palm fatty acid, 12-17wt% of caustic soda solution, 30-40wt% of triethanol amine, 1.0-2.0wt% of glycerine, small amounts of a soap froth accelerator, an antiseptic, and the balance being water; 1-4pts.wt. of noni juice; 0.1-1pts.wt. of mineral oil, jojoba oil, or a mixture thereof.

Description

투명비누 조성물{Transparent soap composition}Transparent soap composition

본 발명은 인체 세정용 투명비누 조성물에 관한 것으로, 보다 구체적으로는 피지 등의 분비물에 대한 분해효과 및 보습효과가 우수한 새로운 투명비누 조성물에 관한 것이다.The present invention relates to a transparent soap composition for washing the human body, and more particularly to a new transparent soap composition excellent in the decomposition and moisturizing effect on secretions such as sebum.

투명비누의 제조방법에 대해서는 과거부터 많은 제안이 있어왔다.There have been many proposals about the method of manufacturing the transparent soap from the past.

종래의 투명비누 제조방법은 휘발성용매(보통은 에탄올)중에서 비누 및 기타성분의 용액을 만든 다음, 이 용액을 몰드 또는 틀형에 주형 한 후 휘발성 용매를 증발시켜 고형화 된 바 형태의 비누를 제조하는 것이다.The conventional method for preparing a transparent soap is to prepare a solution of soap and other components in a volatile solvent (usually ethanol), and then cast the solution into a mold or a mold, and then evaporate the volatile solvent to prepare a bar-shaped soap. .

처음 주형할 때의 고화된 비누용액은 반투명이므로 투명함을 얻기 위해서는 증발에 의한 용매의 제거과정이 필요하다.Since the solidified soap solution at the time of the first casting is translucent, the removal of the solvent by evaporation is necessary to obtain transparency.

그러나 그 증발량이 보통 처음 용액의 15wt% 이상 됨으로 이에 걸리는 시간이 수개월 정도 된다.However, the evaporation usually takes more than 15wt% of the initial solution, which can take several months.

이러한 소위 주형방법은 증발 고형화 과정에서 몰드 양면으로부터 분리되어 수축되는 현상으로 인해 잘못된 형태의 바가 제조될 가능성이 있으며 이 수축은 포장후에도 계속 일어나며 또한 증발에 걸리는 시간으로 인해 제조에 드는 비용이 높다.Such a so-called mold method is likely to produce a wrong type of bar due to the shrinkage of the mold from both sides of the mold during evaporation solidification, and this shrinkage continues to occur after packaging and is expensive to manufacture due to the time required for evaporation.

더군다나 이렇게 제조된 바 형태의 비누는 투명하기는 하나 보통 불투명 비누에 비해 값이 비싸고 사용특성이 좋지 못한 경향이 있다. 특히 이러한 비누는 물과 접촉시켰을 때 보기에도 좋지 않은 끈적한 불투명 표면 층이 생기게 되며 또한 사용 시 피부건조를 유발시키는 비교적 고 알칼리성 제품이다.Furthermore, the soaps produced in this manner tend to be transparent, but they are usually more expensive and less expensive to use than opaque soaps. In particular, these soaps are relatively high alkaline products which, when contacted with water, have a sticky opaque surface layer which is unsightly and which leads to dry skin when used.

이러한 문제점을 부분적으로 극복하기 위한 초기의 제안은 미국특허 제2820768호(Fromont)에 발표되었다. 1958년도 미국 제2820768호에는 투명한 알칼리금속 비누와, 유리지방산(C〉18)과 과량의 트리에탄올아민의 생성물(트리에탄올아민 대 유리지방산의 몰비는 2 : 1- 3 : 1임)의 혼합물을 함유하는 비알칼리성 투명비누에 대해 발표되어 있다. 이 비누는 다음과 같이 제조된다.An early proposal to partially overcome this problem was published in US Pat. No. 2820768 (Fromont). US Patent No. 2820768 in 1958 contains a mixture of clear alkali metal soap and a product of free fatty acids (C> 18) and excess triethanolamine (the molar ratio of triethanolamine to free fatty acids is 2: 1-3: 1). A non-alkaline clear soap has been published. This soap is made as follows.

즉 성분들을 함께 혼합한 다음, 냉각 시에도 유지되는 균질의 투명함이 얻어질때까지 또한 10% 수용액에서의 pH 값이 약 7.5가 될 때까지 이 혼합물을 100°-120℃로 가열한다.That is, the components are mixed together and then heated to 100 ° -120 ° C. until a homogeneous clarity, which is maintained even upon cooling, and until the pH value in the 10% aqueous solution is about 7.5.

이 가열된 혼합물을 틀형에 넣고 냉각, 절단, 압축하여 케이크 또는 바 형태의 제품을 만든다.The heated mixture is placed in a mold and cooled, cut and pressed to form a cake or bar product.

미국특허 제2820768호는 종래 방법에서 생기는 알칼리성 문제가 해결되고 또한 에탄올의 사용을 피함으로써 장기간을 요하는 증발 및 그로 인한 문제점이 제거된 투명비누 및 그 제조방법을 제공한다.US Patent No. 2820768 provides a transparent soap and a method for producing the same, which solves the alkalinity problem caused by the conventional method and also eliminates the long-term evaporation and its problems by avoiding the use of ethanol.

미국특허 제2820768호의 방법에 따라 제조된 비누는 "뉴트로지나(Neutrogena)"라는 이름으로 구입할 수 있다.Soaps prepared according to the method of U.S. Patent No. 2820768 may be purchased under the name "Neutrogena".

그러나 이 비누는 사용 시 여러 가지 시각적, 촉감적인 문제점을 야기시킨다.However, this soap causes many visual and tactile problems when used.

특히 물과 접촉하게 되면 비누 바는 그 표면이 끈끈하게 되며 불투명한 표면 층이 생긴다.In particular, when in contact with water, the soap bar becomes sticky and creates an opaque surface layer.

좀더 개선된 성형 투명비누를 제공하기 위해 과량의 트리에탄올아민을 사용하는 다수의 후기의 제안은 예를 들면 미국특허 제3739214호(Avon Products, Inc), 미국특허 제4206069호(Colgate-Palmolive), 미국특허 제4468338호(Purex Corporation) 및 유럽특허 제71987호(Armour Dial, Inc.)에 발표되어 있다. 이렇게 제조된 비누도 사용특성이 불량한 등의 단점이 있는 것이다.A number of later proposals using excess triethanolamine to provide more improved molded clear soaps are described, for example, in Avon Products, Inc., U.S. Pat. No. 420669 (Colgate-Palmolive), U.S.A. Patents 4468338 to Purex Corporation and European Patent 71987 to Armor Dial, Inc. Soap thus prepared also has disadvantages such as poor use characteristics.

또한 상기한 바와 같은 종래의 투명비누는 피지 등의 분비물에 대한 강력한 분해력과 높은 보습효과를 동시에 만족하지 못하는 것이 단점으로 지적되고 있다.In addition, it is pointed out that the conventional transparent soap as described above does not satisfy the strong degrading power and high moisturizing effect on secretions such as sebum.

따라서 본 발명은 피지 등의 분비물에 대한 강력한 분해력과 높은 보습효과를 동시에 만족할 수 있는 새로운 투명비누 조성물을 제공하는 것을 기술적 과제로 한다.Therefore, the present invention is to provide a new transparent soap composition that can satisfy both the strong decomposition and high moisturizing effect on the secretion, such as sebum as a technical problem.

상기한 과제를 해결하기 위한 본 발명자의 연구에서 통상의 투명비누 조성물에 열대 도서지방에서 주로 산출되는 열매인 노니(noni) 쥬스 적당량과 기존제품에는 글세세린과 함께 첨가하지 않는 보습제인 미네랄 오일 및/또는 호호바 오일 적당량을 첨가한 결과 피지 등의 분비물에 대한 분해효과 및 보습효과가 우수한 투명비누를 제조할 수 있다는 사실을 알게되어 본 발명을 완성하게 된 것이다.In a study of the present inventors to solve the above problems, a suitable amount of nonni juice, a fruit mainly produced in tropical islands, and a moisturizing agent that is not added to the conventional product with a mineral oil and / or a conventional transparent soap composition and / or Or by adding an appropriate amount of jojoba oil was found to be able to produce a transparent soap excellent in the decomposition and moisturizing effect on the secretion, such as sebum to complete the present invention.

그러므로 본 발명에 의하면 투명비누 조성물에 있어서, 통상의 투명비누 조성물에 조성물 100중량부 기준으로 노니 쥬스 1∼4중량부, 글리세린 1∼3중량부 및 미네랄오일, 호호바 오일 또는 이들의 혼합물 0.1∼1중량부를 함유하는 것을 특징으로 하는 투명비누 조성물이 제공된다.Therefore, according to the present invention, in a transparent soap composition, 1 to 4 parts by weight of noni juice, 1 to 3 parts by weight of glycerin and mineral oil, jojoba oil, or a mixture thereof in a conventional transparent soap composition based on 100 parts by weight of the composition. Provided is a transparent soap composition comprising a weight part.

또한 본 발명에 의하면, 코코지방산 15∼20중량%, 팜지방산 20∼30중량%, 가성소다용액 12∼17중량%, 트리에탄올아민 30∼40중량%, 글리세린 1.0∼2.0중량% 미량성분으로서 비누거품촉진제, 방부제 및 잔량의 물을 함유하는 혼합물 100중량부 기준으로 노니 쥬스 1∼4중량부 및 미네랄오일, 호호바 오일 또는 이들의 혼합물 0.1∼1중량부를 함유하는 것을 특징으로 하는 투명비누 조성물이 제공된다.In addition, according to the present invention, 15 to 20% by weight of coco fatty acid, 20 to 30% by weight of palm fatty acid, 12 to 17% by weight of caustic soda solution, 30 to 40% by weight of triethanolamine, and 1.0 to 2.0% by weight of glycerin as a soap component Provided is a transparent soap composition comprising 1 to 4 parts by weight of noni juice and 0.1 to 1 parts by weight of mineral oil, jojoba oil or a mixture thereof based on 100 parts by weight of a mixture containing an accelerator, a preservative and a residual amount of water. .

이하, 본 발명을 보다 상세하게 설명하기로 한다.Hereinafter, the present invention will be described in more detail.

본 발명의 투명비누 조성물은 통상의 투명비누 조성물에 조성물 100중량부 기준으로 노니 쥬스 1∼4중량부, 글리세린 1∼3중량부 및 미네랄오일, 호호바 오일 또는 이들의 혼합물 0.1∼1중량부를 함유한다.The transparent soap composition of the present invention contains 1 to 4 parts by weight of noni juice, 1 to 3 parts by weight of glycerin, and 0.1 to 1 parts by weight of mineral oil, jojoba oil or a mixture thereof based on 100 parts by weight of the composition. .

노니의 작용기전에 대해 아직까지 정확히 알려진 바는 없지만 효소, 비타민, 미네랄, 단백질, 그리고 무엇보다도 노니의 효과에 큰 역할을 하는 것으로 보이는 제로닌이란 알칼로이드가 들어있다.The mechanism of action of Noni is not yet known, but it contains enzymes, vitamins, minerals, proteins, and above all, an alkaloid called zeroin, which seems to play a major role in Noni's effects.

그리고 다른 성분들도 노니의 효과를 상승시키는 것으로 생각된다.And other ingredients are thought to increase the effectiveness of Noni.

또한 노니는 비정상적인 세포를 정상적인 세포로 만들어 주는 작용(아답토젠으로 작용)이 있는 것으로 알려져 있다. 암의 경우, 노니가 면역기능을 강화시켜주고 세포기능을 조절해주며 손상된 세포를 재생해주는 작용을 한다고 한다.In addition, Noni is known to have an action (adaptogen) to make abnormal cells normal cells. In cancer, Noni boosts immune function, regulates cellular function, and regenerates damaged cells.

본 발명에 있어서, 노니 쥬스의 함량은 통상의 투명비누조성물 100중량부 기준으로 1∼4중량부인데, 만일 노니 쥬스의 함량이 1중량부 미만이면 상기의 노니 성분을 포함하여 얻을 수 있는 효과가 충분치 못하여 함유시키는 의미가 없게 되는 문제점이 있고, 4중량부를 초과하면 노니의 성분함유량이 과다하여 비누의 성형을 저해하여 비누의 제조가 불가능하게 만드는 문제점이 있다.In the present invention, the content of noni juice is 1 to 4 parts by weight based on 100 parts by weight of the normal transparent soap composition, if the content of noni juice is less than 1 part by weight, the effect that can be obtained by including the noni component There is a problem that it does not have enough meaning to contain, and if it exceeds 4 parts by weight, there is a problem that makes the production of soap impossible by inhibiting the molding of soap due to excessive content of noni.

또한 본 조성물은 기존의 투명비누 제조 시 글리세린과 함께 첨가하지 않는 미네랄오일, 호호바 오일 또는 이들의 혼합물을 통상의 투명비누조성물 100중량부 기준으로 0.1∼1.0중량부를 배합하여야 목적하는 보습효과를 얻을 수 있게 된다.In addition, the present composition should be prepared by mixing 0.1 to 1.0 parts by weight of mineral oil, jojoba oil, or mixtures thereof, which are not added with glycerin in the preparation of conventional transparent soap, based on 100 parts by weight of a conventional transparent soap composition to obtain a desired moisturizing effect. Will be.

만일 미네랄오일, 호호바 오일 또는 이들의 혼합물의 함량이 0.1 중량부 미만이면 이들을 통해 얻을 수 있는 보습효과가 미미하여 미네랄오일, 호호바 오일 또는 이들의 혼합물을 적용하는 의미가 없게 되는 문제점이 있고, 1.0중량부를 초과하면 이 또한 비누의 적정 성형조건을 저해하여 비누의 제조가 불가능하게 되는 문제점이 있다.If the content of mineral oil, jojoba oil or mixtures thereof is less than 0.1 parts by weight, the moisturizing effect obtained through them is insignificant, and there is no problem in applying mineral oil, jojoba oil or mixtures thereof, and 1.0 parts by weight. If it exceeds this, there is also a problem that it is impossible to manufacture the soap by inhibiting the proper molding conditions of the soap.

특별히 제한하기 위한 것은 아니지만 본 발명의 투명비누 조성물은 코코지방산 15∼20중량%, 팜지방산 20∼30중량%, 가성소다용액 12∼17중량%, 트리에탄올아민 30∼40중량%, 글리세린 1.0∼2.0중량% 미량성분으로서 비누거품촉진제, 방부제 및 잔량의 물을 함유하는 혼합물 100중량부 기준으로 노니 쥬스 1∼4중량부 및 미네랄오일, 호호바 오일 또는 이들의 혼합물 0.1∼1중량부를 함유하도록 제조하는 것이 바람직하다.Although not particularly limited, the transparent soap composition of the present invention comprises 15 to 20% by weight of coco fatty acid, 20 to 30% by weight of palm fatty acid, 12 to 17% by weight of caustic soda solution, 30 to 40% by weight of triethanolamine, and 1.0 to 2.0 of glycerin. It is prepared to contain 1 to 4 parts by weight of noni juice and 0.1 to 1 parts by weight of mineral oil, jojoba oil or a mixture thereof based on 100 parts by weight of a mixture containing a soapy accelerator, a preservative and a residual amount of water as a weight% trace component. desirable.

이하 본 발명을 실시예의 방법으로 설명하기로 한다.Hereinafter, the present invention will be described by way of examples.

[실시 예][Example]

다음의 조성으로 투명비누 조성물을 준비하였다.A transparent soap composition was prepared with the following composition.

기본조성물Basic composition

코코지방산 20중량%,20% by weight of coco fatty acid,

팜지방산 25중량%,25% by weight of palm fatty acid,

가성소다용액 15중량%,Caustic soda solution 15% by weight,

트리에탄올아민 35중량%,35% by weight of triethanolamine,

미량성분으로서 비누거품촉진제, 방부제 및 잔량의 물Soap bubbles accelerator, preservative and residual water as trace ingredients

첨가성분Ingredient

기본 조성물 100중량부 기준으로Based on 100 parts by weight of the base composition

노니 쥬스 1∼4중량부Noni juice 1-4 weight part

상기의 조성물을 1차 교반 탱크에 투입하여 70∼80℃에서 1시간 동안 혼합하고 얻어진 혼합물을 2차 교반 탱크에 상기 기본조성물 100중량부 기준으로 미네랄오일 0.6중량부, 글리세린 1.7중량부 및 향료와 함께 투입한 후 약 30분 정도 혼합하였다.The composition was added to a primary stirring tank, mixed at 70 to 80 ° C. for 1 hour, and the resulting mixture was mixed with a secondary stirring tank with 0.6 parts by weight of mineral oil, 1.7 parts by weight of glycerin, and flavoring based on 100 parts by weight of the basic composition. After putting together, the mixture was mixed for about 30 minutes.

얻어진 혼합물을 용기에 넣어 굳힌 후 일정크기로 절단하고 성형하여 투명비누를 제조하였다.The obtained mixture was hardened in a container, cut into a predetermined size, and molded to prepare a transparent soap.

제조된 투명비누는 염증치료 및 여드름, 피부질환치료에 탁월한 효능을 나타냈고, 지성, 건성, 알레르기성 피부에 사용이 가능하였다.The prepared transparent soap showed excellent efficacy in treating inflammation, acne, and skin diseases, and could be used for oily, dry, and allergic skin.

특히, 청소년기의 남녀를 대상으로 여드름 치료에 사용한 결과 99% 이상의 효과를 보였으며, 손바닥 습진같이 피부 표피의 벗겨짐 등에 2∼3주 사용 후 깨끗이 없어지는 효과도 있음을 실험결과 확인할 수 있었다.In particular, the results of the acne treatment in adolescents and men showed more than 99% effect, and the experimental results showed that there is also a clearing effect after 2 to 3 weeks of use such as peeling of the skin epidermis, like palm eczema.

또한 아토피성 피부질환에 탁월한 효능이 있으며 피곤하면 화장이 뜨는 여성들이 클린싱 크림을 사용하는 대신에 본 비누를 사용하게 되면 화장이 곱게 잘되는 효과도 있고, 무좀치료에도 효과가 있었다.In addition, it has an excellent effect on atopic dermatological diseases and when the tired women leave the makeup, they use the soap instead of using the cleansing cream.

또한 피지 등과 같은 피부 분비물에 대한 분해효과가 탁월하여 세정 시 때를 밀지 않아도 피부를 청결하게 하는 효과도 있고, 미백 효과가 있어서 희고 깨끗한 피부를 만드는 효과도 있었다.In addition, it has an excellent decomposition effect on skin secretions, such as sebum, and also has the effect of cleaning the skin without pushing the time when washing, and has the effect of making the skin white and clean because of the whitening effect.

또한 본 비누는 잔류 향이 오랫동안 지속되어 아로마 요법으로 치료한 것과 같은 효과도 얻을 수 있었다.The soap also lasted for a long time, giving the same benefits as aromatherapy.

또한 피부 분비물에 대한 분해효과가 탁월하여 처음 사용시 약간 당김을 느낄 수 있으나, 보습효과가 탁월하여 10여분 지나면 피부가 촉촉하게 되었다.In addition, due to the excellent decomposition effect on the skin secretion, you may feel a little pull on the first use, but the moisturizing effect was excellent, and after 10 minutes the skin became moist.

Claims (2)

투명비누 조성물에 있어서, 통상의 투명비누 조성물에 조성물 100중량부 기준으로 노니 쥬스 1∼4중량부, 글리세린 1∼3중량부 및 미네랄오일, 호호바 오일 또는 이들의 혼합물 0.1∼1중량부를 함유하는 것을 특징으로 하는 투명비누 조성물.In the transparent soap composition, containing 1 to 4 parts by weight of noni juice, 1 to 3 parts by weight of glycerin and 0.1 to 1 parts by weight of mineral oil, jojoba oil or a mixture thereof in a conventional transparent soap composition based on 100 parts by weight of the composition. Transparent soap composition characterized in that. 제 1 항에 있어서, 코코지방산 15∼20중량%, 팜지방산 20∼30중량%, 가성소다용액 12∼17중량%, 트리에탄올아민 30∼40중량%, 글리세린 1.0∼2.0중량% 미량성분으로서 비누거품촉진제, 방부제 및 잔량의 물을 함유하는 혼합물 100중량부 기준으로 노니 쥬스 1∼4중량부 및 미네랄오일, 호호바 오일 또는 이들의 혼합물 0.1∼1중량부를 함유하는 것을 특징으로 하는 투명비누 조성물.The soap bubble according to claim 1, wherein 15 to 20% by weight of coco fatty acid, 20 to 30% by weight of palm fatty acid, 12 to 17% by weight of caustic soda solution, 30 to 40% by weight of triethanolamine, and 1.0 to 2.0% by weight of glycerin A transparent soap composition comprising 1 to 4 parts by weight of noni juice and 0.1 to 1 parts by weight of mineral oil, jojoba oil or a mixture thereof based on 100 parts by weight of a mixture containing an accelerator, a preservative and a residual amount of water.
KR1020020057589A 2002-09-23 2002-09-23 Transparent soap composition KR20040026213A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR860008772A (en) * 1985-05-13 1986-12-18 더 프록터 앤드 갬블 캄파니 Super soft skin cleaning composition
KR970010945A (en) * 1995-08-17 1997-03-27 이범익 Transparent gold soap with pure vegetable oil and its manufacturing method
KR19990083850A (en) * 1999-08-19 1999-12-06 변성진 A Manufacturing prosess of toilet soap contain from natural Matter
KR20000068900A (en) * 1999-05-04 2000-11-25 스즈키 츠네시 Transparent solid soap and transparent soap stock
JP2001199871A (en) * 2000-01-24 2001-07-24 Kanebo Ltd Cosmetic
JP2001213752A (en) * 2000-01-28 2001-08-07 Kanebo Ltd Cosmetic

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR860008772A (en) * 1985-05-13 1986-12-18 더 프록터 앤드 갬블 캄파니 Super soft skin cleaning composition
KR970010945A (en) * 1995-08-17 1997-03-27 이범익 Transparent gold soap with pure vegetable oil and its manufacturing method
KR20000068900A (en) * 1999-05-04 2000-11-25 스즈키 츠네시 Transparent solid soap and transparent soap stock
KR19990083850A (en) * 1999-08-19 1999-12-06 변성진 A Manufacturing prosess of toilet soap contain from natural Matter
JP2001199871A (en) * 2000-01-24 2001-07-24 Kanebo Ltd Cosmetic
JP2001213752A (en) * 2000-01-28 2001-08-07 Kanebo Ltd Cosmetic

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