KR20040013846A - fiber products for emitting far infrared ray and method for making the same - Google Patents
fiber products for emitting far infrared ray and method for making the same Download PDFInfo
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- KR20040013846A KR20040013846A KR1020020046933A KR20020046933A KR20040013846A KR 20040013846 A KR20040013846 A KR 20040013846A KR 1020020046933 A KR1020020046933 A KR 1020020046933A KR 20020046933 A KR20020046933 A KR 20020046933A KR 20040013846 A KR20040013846 A KR 20040013846A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/001—Softening compositions
- C11D3/0015—Softening compositions liquid
Abstract
Description
본 발명은 원적외선 방출 섬유제품 및 그 제조방법에 관한 것으로서, 보다 상세하게는, 원적외선 방출체를 담요 또는 카페트 등의 섬유재에 침작시켜 형성된 원적외선 방출 섬유제품 및 그 제조방법에 관한 것이다.The present invention relates to a far-infrared emitting fiber product and a method of manufacturing the same, and more particularly, to a far-infrared emitting fiber product formed by depositing a far-infrared emitter on a fiber material such as a blanket or a carpet, and a method of manufacturing the same.
원적외선은 일정한 주파수를 갖는 전자파 및 열에너지로서, 세포를 1 분에 약 2000번씩 미세하게 흔들어주는 공진, 공명운동을 통해 세포조직의 생명활동을 보다 왕성하게 해주고 혈액순환을 촉진시켜 스트레스 및 피로 회복과 노화방지에큰 효능을 갖는다고 알려져 있다.Far-infrared rays are electromagnetic waves and thermal energy having a constant frequency.They resonate and resonately move cells about 2,000 times per minute to enhance the vitality of cell tissues and promote blood circulation, thereby relieving stress and fatigue and aging. It is known to have great efficacy in prevention.
이러한 이유로, 원적외선을 방출하는 방출체에 대한 연구가 여러 분야에서 폭 넓게 이루어지고 있는 실정이다.For this reason, studies on emitters emitting far infrared rays have been widely conducted in various fields.
원적외선 방출체의 방사에너지는 최대방사능력을 갖은 가상물질인 흑체를 기준으로 해서 각 파장에 있어서 그 원적외선 방출체의 방사에너지를 상대비율로서 나타내는 것이 일반적이다.The radiation energy of the far infrared emitter is generally represented as a relative ratio of the radiation energy of the far infrared emitter at each wavelength based on a black body, which is a virtual material having the maximum radiation ability.
도 1에는 이상물질인 흑체의 분광방사 에너지 곡선이 도시되어 있다.1 shows a spectral radiant energy curve of a black body, which is an abnormal substance.
도 1에 도시된 바와 같이, 온도가 올라가면 흑체의 방사파장 최대점이 근적외선으로 이동하는 것을 볼 수 있으며, 이는 원적외선 방사체도 비슷한 경향을 보인다.As shown in FIG. 1, it can be seen that as the temperature increases, the maximum radiation wavelength of the black body moves to the near infrared, which also shows a similar tendency to the far infrared emitter.
이는 고온에서 방사되는 원적외선 방사보다는 저온, 바람직하게는 체온 근처의 온도에서 원적외선을 쬐는 것이 인체에 더 유익하다는 것을 증명한다.This demonstrates that it is more beneficial to the human body to expose far infrared rays at low temperatures, preferably near body temperature, rather than far infrared radiation emitted at high temperatures.
따라서, 의류 또는 침구류와 같이 인체에 직접 닿는 섬유재에, 체온에 가까운 온도에서 원적외선을 방출하는 원적외선 방사체가, 도입되어질 경우, 그 효과가 더욱 커질 것으로 기대되며, 이에 따라, 섬유재에 게르마늄 원석 분말과 같은 원적외선 방사체를 침착시킨 섬유제품이 개발되었다.Therefore, when a far-infrared radiator that emits far-infrared radiation at a temperature close to the body temperature is introduced to a textile material that directly touches the human body, such as clothing or bedding, the effect is expected to be greater. Textile products have been developed which deposit far-infrared emitters such as powders.
하지만, 게르마늄 원석분말로 이루어진 원적외선 방사체는, 1250~1300℃의 고온에서 소성가공후 미립자로 분쇄하는 과정을 거쳐야만 가시적인 원적외선 방사효과가 나타나므로, 제조공정이 복잡하고 비용이 많이 드는 문제점이 있었다.However, the far-infrared radiator made of germanium ore powder has a problem that the manufacturing process is complicated and costly because the visible far-infrared radiation effect only appears after the process of pulverizing into fine particles after plastic processing at a high temperature of 1250 ~ 1300 ℃.
이에 대해, 본 발명자는 저비용으로 간단하게 제조된 새로운 원적외선 방사체 분말을 예를 들면 담요 또는 카페트에 침착시켜 형성된 원적외선 방출 섬유제품을 개발하게 되었다.In response, the inventors have developed a far-infrared emitting fiber product formed by depositing a new far-infrared emitter powder, which is simply produced at low cost, on a blanket or carpet, for example.
따라서, 본 발명의 목적은, 원적외선 방출요소인 세레늄(Se), 합성실리카(SiO2), 알루미나(Al2O3), 산화철(Fe2O3), 산화칼슘(CaO), 산화마그네슘(MgO), 산화칼륨(K2O), 산화나트륨(Na2O) 및 산화티타늄(TiO2)을 최적의 조성비로 혼합하여 원적외선 방사능이 극대화된 원적외선 방사체를, 섬유재에 침착하여 제조된 새로운 형태의 원적외선 방출 섬유제품 및 그 제조방법을 제공하는 것을 그 목적으로 한다.Therefore, an object of the present invention, the far-infrared emitting element selenium (Se), synthetic silica (SiO 2 ), alumina (Al 2 O 3 ), iron oxide (Fe 2 O 3 ), calcium oxide (CaO), magnesium oxide (MgO ), A new type of far-infrared radiator that maximizes far-infrared radiation by mixing potassium oxide (K 2 O), sodium oxide (Na 2 O) and titanium oxide (TiO 2 ) in an optimal composition ratio It is an object of the present invention to provide a far infrared ray emitting fiber product and a method of manufacturing the same.
도 1은 이상물질인 흑체의 분광방사 에너지 곡선을 도시한 그래프.1 is a graph showing the spectral radiant energy curve of a black body as an ideal substance.
도 2는 아크릴 수지의 원적외선 특성을 나타내는 그래프.2 is a graph showing the far infrared ray characteristics of an acrylic resin.
도 3은 본 발명의 실시예에 따라 제조된 시편의 5~20㎛ 파장에 대한 원적외선 방출 에너지를 도시한 그래프.Figure 3 is a graph showing the far infrared emission energy for the wavelength of 5 ~ 20㎛ of the specimen prepared according to the embodiment of the present invention.
도 4는 본 발명의 실시예에 따른 원적외선 방출 섬유제품의 제조방법을 도시하는 순서도.Figure 4 is a flow chart showing a method of manufacturing a far infrared ray emitting fiber product according to an embodiment of the present invention.
상술한 목적을 달성하기 위해, 본 발명에 따른 원적외선 방출 섬유제품은, 합성실리카(SiO2) 52~55.2 중량%, 알루미나(Al2O3) 24~27.0 중량%, 산화칼륨(K2O)8.0~9.7중량%, 세레늄(Se) 4~6 중량%를 주성분으로 하고, 나머지는 산화칼슘(CaO), 산화마그네슘(MgO), 산화티타늄(TiO2)인 혼합물이 포함된 수용액을 600~770℃ 온도로 가열하여 결합력을 강화시키고, 이렇게 얻어진 원적외선 방사체 분말을 10~15%로 희석시켜, 그 희석된 희석액을 섬유유연재와 3:1~6:1로 혼합하여, 그 혼합액에 섬유재를 침지하여 형성되는 것을 특징으로 한다.In order to achieve the above object, the far-infrared emitting fiber product according to the present invention, synthetic silica (SiO 2 ) 52 ~ 55.2% by weight, alumina (Al 2 O 3 ) 24 ~ 27.0% by weight, potassium oxide (K 2 O) 8.0 to 9.7% by weight, 4 to 6% by weight of selenium (Se), the remainder is 600 to 770 an aqueous solution containing a mixture of calcium oxide (CaO), magnesium oxide (MgO), titanium oxide (TiO 2 ) The bonding strength is enhanced by heating to a temperature of 0 ° C., and the far-infrared radiator powder thus obtained is diluted to 10 to 15%, and the diluted dilution is mixed with the fiber soft material at 3: 1 to 6: 1, and the fiber material is added to the mixed solution. It is characterized by being formed by dipping.
여기에서, 용어 "섬유재"는 완전한 원적외선 방출 섬유제품이 이루어지기 전의 섬유를 의미하는 것으로, 이는 담요, 카페트, 의류 등을 폭넓게 포함하는 것이다.As used herein, the term "fiber material" refers to the fiber before the complete far-infrared emitting fiber product is made, which broadly includes blankets, carpets, clothing, and the like.
여기에서, 합성 실리카(SiO2)는 약 6㎛부터 전파장에 걸쳐 가장 큰 원적외선 방출에너지를 내는 요소이며, 약 8~10㎛의 파장에서는 비교적 원적외선 방출에너지가 떨어지며, 그 함량이 52 중량% 미만일 경우, 원적외선 방출 섬유제품은 원적외선 방출 에너지가 전파장에 걸쳐 상당히 떨어짐을 실험을 통해 알 수 있었다.Here, the synthetic silica (SiO 2 ) is the element that emits the largest far-infrared emission energy over the full-wavelength from about 6 μm, and the far-infrared emission energy falls at a wavelength of about 8 to 10 μm, and its content is less than 52% by weight. In the case of the far-infrared emitting fiber products, the experiment showed that the far-infrared emission energy dropped considerably over the electric field.
또한, 알루미나는 약 8㎛부터 전파장에 걸쳐 원적외선을 방출하는 요소로서, 특히, 8~10㎛에서 원적외선 방출에너지가 가장 높은 요소이다.In addition, alumina is an element that emits far infrared rays from about 8 μm to a radio wave field, and particularly, an element having the highest far infrared ray emission energy at 8 to 10 μm.
이러한 알루미나의 함량이 24 중량% 미만인 경우, 제조된 원적외선 방출 섬유제품은 약 8~10㎛의 파장 범위에서 원적외선 방출에너지가 상당히 크게 떨어진다.When the content of such alumina is less than 24% by weight, the far-infrared emission fiber product produced has a considerable drop in far-infrared emission energy in the wavelength range of about 8-10 m.
또한, 산화칼륨(K2O), 세레늄(Se), 산화칼슘(CaO), 산화마그네슘(MgO) 및 산화티타늄(TiO2)은 합성실리카 및 알루미나의 원적외선 방출율이 적은 파장범위 약 4~6㎛의 파장범위에서 원적외선 방사효과가 있는 요소이며, 특히 , 산화칼륨(K2O)의 함량이 8.0 중량% 미만인 경우, 원적외선 방사효과가 감소됨을 실험을 통해 알 수 있었다.In addition, potassium oxide (K 2 O), selenium (Se), calcium oxide (CaO), magnesium oxide (MgO), and titanium oxide (TiO 2 ) have a wavelength range of about 4-6 μm in which far infrared ray emission rate of synthetic silica and alumina is low. The far-infrared radiation effect in the wavelength range of, especially, when the content of potassium oxide (K 2 O) is less than 8.0% by weight, the infrared radiation effect was found through experiments.
세레늄은 본 발명의 가장 큰 특징을 이루는 요소로서, 약 4~6 중량%가 첨가되어지는 것이 바람직하다, 세레늄은 그 자체로도 원적외선 방사효과를 갖는 것은 물론이고, 외부의 열을 자체 내에 저장하여 그 열로써 원적외선 방출체의 원적외선방출을 일으키는 역할을 한다.Serenium is the most characteristic element of the present invention, it is preferable that about 4 to 6% by weight is added, the selenium itself has a far-infrared radiation effect, as well as by storing external heat in itself The heat acts to cause far-infrared emission of the far-infrared emitter.
이하, 본 발명의 바람직한 실시예가 도면을 참조로 하여 상세히 설명될 것이다.Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the drawings.
<실시예><Example>
하기 표 1의 함량을 갖는 혼합물의 수용액을 수용액을 600~770℃ 온도로 가열하여 결합력을 강화시키고, 가열되어 얻어진 원적외선 방사체 분말을 10~15%로 희석한 후, 그 희석된 희석액을, 희석액: 섬유유연제=5:1로 혼합한 용액에 아크릴 섬유로 만들어진 담요를 약 40시간 침지한 후, 이를 완전히 건조하여 원적외선 방출 섬유제품, 바람직하게는 원적외선 방출 담요를 제조하였다.The aqueous solution of the mixture having the content of the following Table 1 was heated to 600 ~ 770 ℃ temperature of the aqueous solution to enhance the bonding strength, and diluted 10 ~ 15% of the far-infrared radiator powder obtained by heating, the diluted diluted solution, diluent: After immersing a blanket made of acrylic fiber in a solution mixed with a fiber softener = 5: 1 for about 40 hours, it was completely dried to prepare a far infrared ray emitting fiber product, preferably a far infrared ray emitting blanket.
여기에서, 상기 언급된 아크릴 섬유는 아크릴 수지로 제조되는 것으로서, 그 아크릴 수지는, 도 2에 도시된 바와 같이, 원적외선에 특성이 양호함을 알 수 있다.Here, the above-mentioned acrylic fiber is made of an acrylic resin, the acrylic resin, as shown in Figure 2, it can be seen that the characteristics of the far infrared is good.
또한, 섬유유연제는 섬유재에 원적외선 방사체를 침착시키기 위해 유연하게 만드는 용도로서, 그 섬유유연제는 일반적으로 제조 판매되는 것을 사용하고 그 성분이 이미 공지되어 있으므로, 본 명세서에서는 그 설명이 생략되어졌다.In addition, the fabric softener is an application for making it flexible for depositing a far-infrared radiator on a fiber material, and the fabric softener is generally manufactured and sold, and its components are already known, and thus the description thereof is omitted.
<실험예>Experimental Example
상술한 제 1 실시예에 의해 제조된 원적외선 방출 섬유제품을 30mm×30mm의 시편으로 채취하여, 파장범위 5~20㎛, 온도 40℃의 실험조건에서, 원적외선 방사율및 원적외선 방사에너지를 원적외선 방출시험(FT-IR)으로 측정하여 하기 표 2에 나타내고, 이상물질인 흑체와 함께, 파장에 대한 원적외선 방사에너지 그래프를 도 3에 도시하였다. 참고로, 원적외선 방출 섬유제품은 약 40℃의 온도 및 5~20㎛의 파장 범위 내에서 이상 물질인 흑체와 가까운 양상을 보일 수록 우수하다 할 것이다.The far-infrared emission fiber product prepared according to the first embodiment was taken with a 30 mm × 30 mm specimen, and the far-infrared emissivity and far-infrared radiation energy were tested for far-infrared emissivity and far-infrared radiation energy under the experimental conditions of a wavelength range of 5 to 20 μm and a temperature of 40 ° C. FT-IR) is shown in Table 2 below, and the far-infrared radiation energy graph with respect to the wavelength is shown in FIG. For reference, the far-infrared emitting fiber product may be superior as it exhibits a close appearance to a black body which is an abnormal substance within a temperature of about 40 ° C. and a wavelength range of 5 to 20 μm.
표 2 및 도 3으로 알 수 있는 바와 같이, 본 발명에 따라 제조된 원적외선 방출 섬유제품은 원적외선 방출효과가 체온 근처의 온도인 약 40 ℃의 온도에서 매우 큼을 알 수 있다.As can be seen from Table 2 and Figure 3, it can be seen that the far-infrared emission fiber product produced according to the present invention is very large at a temperature of about 40 ℃, the temperature near the body temperature.
이제, 도 4를 참조로 하여, 본 발명에 따른 원적외선 방출 섬유제품의 제조방법에 대한 설명이 이루어질 것이다.Referring now to FIG. 4, a description will be made of a method for producing a far infrared ray emitting fiber product according to the present invention.
상술한 원적외선 방출 섬유제품의 제조 방법은, 합성실리카(SiO2) 52~55.2 중량%, 알루미나(Al2O3) 24~27.0 중량%, 산화칼륨(K2O) 8.0~9.7중량%, 세레늄(Se) 4~6 중량%와, 나머지는 산화칼슘(CaO), 산화마그네슘(MgO), 산화티타늄(TiO2)의 혼합물이 포함된 수용액을 600~770℃의 온도로 가열하여 원적외선 방사체 분말을 얻는 단계(S10)와, 상기 단계(S10)에서 얻어진 원적외선 방사체 분말을 10~15%로 희석한 후, 그 희석된 희석액을 액상의 섬유유연제 용액과 혼합하여 침치액을 제조하는 침지액 조성단계(S11)와, 상기 침지액에 섬유재, 바람직하게는 아크릴 섬유재를침지하는 침지단계(S12)와, 상기 침지단계(S12)를 거친 원적외선 방출 섬유재를 건조하는 단계(S13)를 포함한다.The method for producing the far-infrared emitting fiber product described above includes 52 to 55.2 wt% of synthetic silica (SiO 2 ), 24 to 27.0 wt% of alumina (Al 2 O 3 ), 8.0 to 9.7 wt% of potassium oxide (K 2 O), and selenium (Se) 4 to 6% by weight, and the remainder of the far-infrared radiator powder by heating an aqueous solution containing a mixture of calcium oxide (CaO), magnesium oxide (MgO), titanium oxide (TiO 2 ) to a temperature of 600 ~ 770 ℃ Dipping solution composition step of obtaining a step (S10) and the far-infrared radiator powder obtained in the step (S10) to 10 to 15%, and then mixing the diluted diluent with a liquid fibrous softener solution ( S11), and an immersion step (S12) of immersing a fibrous material, preferably an acrylic fiber material, in the immersion liquid, and a step (S13) of drying the far-infrared emitting fiber material passed through the immersion step (S12).
여기에서, 침지액 조성단계(S11)에서 조성된 원적외선 방출체를 포함한 침지액은 약 캐티온(cation)의 성질을 가짐으로써 섬유재에 침착되기에 용이하다.Here, the immersion liquid including the far-infrared emitter formed in the immersion liquid composition step (S11) is easy to be deposited on the fiber material by having a property of about cation (cation).
이상에서 살펴본 바와 같이, 본 발명은 종래의 원적외선 방출 섬유제품에 비해 저렴한 가격으로 제조되면서도, 그 원적외선 방출 특성이 우수하여, 인체의 건강에 매우 이로운 기능을 하는 효과를 갖는다.As described above, the present invention is produced at a lower price than the conventional far-infrared emitting fiber products, it is excellent in the far-infrared emission characteristics, has the effect of having a very beneficial function to the health of the human body.
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| US9556063B2 (en) | 2014-07-17 | 2017-01-31 | Unifrax I Llc | Inorganic fiber with improved shrinkage and strength |
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| US10882779B2 (en) | 2018-05-25 | 2021-01-05 | Unifrax I Llc | Inorganic fiber |
| KR102216896B1 (en) * | 2020-10-23 | 2021-02-18 | 김용선 | Method for processing fiber that radiates far-infrared rays using powder, and fabric using fibers processed thereby |
| US11203551B2 (en) | 2017-10-10 | 2021-12-21 | Unifrax I Llc | Low biopersistence inorganic fiber free of crystalline silica |
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